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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78359完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳建彰(Jian-Zhang Chen) | |
| dc.contributor.author | Jui-Chen Hsin | en |
| dc.contributor.author | 辛睿宸 | zh_TW |
| dc.date.accessioned | 2021-07-11T14:52:57Z | - |
| dc.date.available | 2023-07-30 | |
| dc.date.copyright | 2020-08-03 | |
| dc.date.issued | 2020 | |
| dc.date.submitted | 2020-07-24 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78359 | - |
| dc.description.abstract | 此研究主要是使用碳纖維布作為軟性超級電容的電極，使用氮氣電弧式常壓噴射電漿在基板溫度520℃將碳纖維布表面處理30秒後，網印塗覆上還原氧化石墨烯-聚苯胺-殼聚醣的奈米複合材料，再使用氬氣介電質放電噴射電漿，在不同處理次數與基板溫度40℃下，對表面材料進行改質，最後均勻塗覆上凝膠態硫酸電解液，製作成一組超級電容。另外，亦有研究以發泡鎳與纖維素紙作為基材之超級電容。經由掃描式電子顯微鏡 (SEM)，可以觀察到還原氧化石墨烯、聚苯胺、殼聚醣的奈米複合材料皆均勻分布在碳纖維布上，而由X-射線繞射儀 (XRD)與拉曼光譜儀 (Raman spectroscopy)觀測到在氬氣介電質放電噴射電漿處理後，材料本身之結構皆沒有明顯的改變。由X-射線光電子能譜儀 (XPS)分析處理前後材料表面的化學組成，利用水接觸角儀 (WCA)測量後，可以發現到在氬氣介電質放電噴射電漿處理後，材料表面之親水性鍵結增加，使得親水性上升，可與凝膠態硫酸電解液有更好的接合，進而提升超級電容之容量。另外，亦有探討電漿處理與熱效應對於碳纖維布之親水性影響。在恆電流充電放電測量法 (Galvanostatic Charge-Discharge Test)與循環伏安法（Cyclic Voltammetry Test）下，可以得到在經過氬氣介電質放電噴射電漿處理後，超級電容具有較大之電雙層電容及法拉第電容，電容值皆提高了150 ~ 300%左右，而在機械式彎曲測試與長時間充放電的實驗下，軟性超級電容經過五百次曲率半徑5 mm的機械彎曲與1萬次充放電後，電容值沒有明顯的降低，顯示出軟性超級電容具有良好的機械穩定性和長時間充放電穩定性。經由此研究的結果顯示，在沒有給予樣品加熱處理下，單純以低溫(~40°C)氬氣介電質放電噴射電漿的高反應性離子，便可以改變碳纖維布上還原氧化石墨烯-聚苯胺-殼聚醣複合材料的性質，使軟性超級電容之性能有進一步的提升。 | zh_TW |
| dc.description.abstract | We used carbon fiber cloth as the electrodes of the flexible supercapacitors. The carbon cloth was treated by nitrogen arc atmospheric-pressure plasma jet (APPJ) at a substrate temperature of 520℃ for 30 s. Following which reduced graphene oxide (rGO)-polyaniline (PANI)-chitosan (CS) pastes was screen-printed on APPJ-treated carbon cloth. Ar dielectric barrier discharge jet (DBDjet) was used to modify the material at a substrate temperature of ~40° C with zero, one, and two scans. Through the scanning electron microscopy, it can be observed that the nanocomposite materials of rGO-PANI-CS are uniformly distributed on the carbon cloth. The structure of the rGO-PANI-CS did not change significantly after the Ar DBDjet treatment. Improved hydrophilicity after DBDjet treatment increased capacity of the supercapacitor, as evidenced by X-ray photoelectron spectroscopy and water contact angle measurement. Galvanostatic charging-discharging (GCD) and cyclic voltammetry (CV) results indicate that Ar DBDjet treatment improves the capacitance by 150 ~ 300%. The flexible supercapacitor shows good stability under the mechanical bending test and long-term charging and discharging experiments. Our results show that without substantial heating, only reactive plasma species of Ar DBDjet can substantially alter the properties of rGO-PANI-CS nanocomposites on carbon cloth to improve the performance of supercapacitors | en |
| dc.description.provenance | Made available in DSpace on 2021-07-11T14:52:57Z (GMT). No. of bitstreams: 1 U0001-2407202013150800.pdf: 10045190 bytes, checksum: 68929f64d4291dbb73122edaae742b9e (MD5) Previous issue date: 2020 | en |
| dc.description.tableofcontents | 口試委員審定書 I 誌謝 II 中文摘要 III ABSTRACT IV 總目錄 V 圖目錄 IX 表目錄 XV 第一章 緒論 1 1.1 前言 1 1.2 研究動機 3 1.3 論文大綱 4 第二章 基本原理與文獻回顧 5 2.1 超級電容 5 2.1.1 超級電容之介紹 5 2.1.2 超級電容之儲能型式 9 2.1.3 超級電容之組成 15 2.2 常壓電漿 18 2.2.1 電漿之介紹 18 2.2.2 電漿之工作原理 18 2.2.3 常壓電漿之種類與其應用 24 2.3 材料特性 30 2.3.1 石墨烯之介紹 30 2.3.2 聚苯胺之介紹 34 2.3.3 殼聚醣之介紹 38 2.3.4 石墨烯-聚苯胺超級電容之文獻回顧 39 第三章 實驗方法與步驟 42 3.1 實驗材料與量測儀器 42 3.2 實驗步驟 45 3.2.1 製備超級電容電極之漿料 45 3.2.2 製備凝膠態電解液 46 3.2.3 製備還原氧化石墨烯-聚苯胺-殼聚醣之電極 46 3.2.4 氮氣直流脈衝常壓噴射電漿 47 3.2.5 網版印刷法 49 3.2.6 氬氣介電質放電電漿 50 3.2.7 製備軟性超級電容 51 3.3 量測儀器介紹 52 3.3.1 掃描式電子顯微鏡 (Scanning Electron Microscope) 52 3.3.2 光放射光譜儀 (Optical Emission Spectroscopy) 55 3.3.3 水接觸角儀 (Water contact angle instrument) 55 3.3.4 X射線繞射儀 (X-ray diffractometer) 57 3.3.5 拉曼光譜儀 (Raman spectroscopy) 58 3.3.6 X射線光電子能譜儀 (X-ray photoelectron spectroscopy) 60 3.3.7 電化學量測 (electrochemical measurement) 61 第四章 實驗結果與討論 65 4.1 氮氣直流脈衝常壓噴射電漿處理碳纖維布之溫度分析 65 4.2 氮氣直流脈衝常壓噴射電漿定點處理碳纖維布之光譜分析 66 4.3 碳纖維布之表面型態 67 4.4 碳纖維布之水接觸角量測 69 4.5 氬氣介電質放電電漿掃描處理還原氧化石墨烯-聚苯胺-殼聚醣複合材料之溫度分析 73 4.6 氬氣介電質放電電漿掃描處理還原氧化石墨烯-聚苯胺-殼聚醣複合材料之光譜分析 74 4.7 還原氧化石墨烯-聚苯胺-殼聚醣複合材料之表面型態 75 4.8 還原氧化石墨烯-聚苯胺-殼聚醣複合材料之水接觸角量測 77 4.9 還原氧化石墨烯-聚苯胺-殼聚醣複合材料之晶體結構分析 78 4.10 還原氧化石墨烯-聚苯胺-殼聚醣複合材料之拉曼光譜分析 79 4.11 還原氧化石墨烯-聚苯胺-殼聚醣複合材料之表面化學型態分析 81 4.12 還原氧化石墨烯-聚苯胺-殼聚醣軟性超級電容之循環伏安法量測 86 4.13 還原氧化石墨烯-聚苯胺-殼聚醣軟性超級電容之定電流充放電法量測 89 4.14 還原氧化石墨烯-聚苯胺-殼聚醣軟性超級電容之彎曲穩定性測試 91 4.15 還原氧化石墨烯-聚苯胺-殼聚醣軟性超級電容之多循環次數充放電穩定性測試 94 4.16 還原氧化石墨烯-聚苯胺-殼聚醣軟性超級電容之點亮LED實驗 95 4.17 還原氧化石墨烯-聚苯胺-殼聚醣軟性超級電容之能量密度與功率密度分析 96 第五章 結論與未來展望 98 附錄 實驗A 電泳還原氧化石墨烯於發泡鎳電極之超級電容應用 100 A.1 摘要 100 A.2 實驗步驟 100 A.3 實驗結果與討論 101 A.3.1發泡鎳超級電容之循環伏安法量測 101 A.3.1發泡鎳超級電容之定電流充放電法量測 103 A.3.1發泡鎳之表面型態 104 A.4 結論 106 附錄 實驗B以纖維素紙作為電極之超級電容應用 107 B.1 摘要 107 B.2 實驗步驟 107 B.3 實驗結果與討論 108 B.3.1纖維素紙超級電容之循環伏安法量測 108 B.3.2纖維素紙之表面型態 109 B.4 結論 110 參考文獻 111 | |
| dc.language.iso | zh-TW | |
| dc.subject | 還原氧化石墨烯 | zh_TW |
| dc.subject | 聚苯胺 | zh_TW |
| dc.subject | 常壓噴射電漿 | zh_TW |
| dc.subject | 超級電容 | zh_TW |
| dc.subject | 介電質放電噴射電漿 | zh_TW |
| dc.subject | 殼聚醣 | zh_TW |
| dc.subject | Reduced graphene oxide | en |
| dc.subject | Supercapacitor | en |
| dc.subject | Polyaniline | en |
| dc.subject | Dielectric barrier discharge | en |
| dc.subject | Atmospheric-pressure plasma | en |
| dc.subject | Chitosan | en |
| dc.title | 常壓介電質放電噴射電漿改質聚苯胺-石墨烯-殼聚醣軟性超級電容及紙基超級電容製程開發 | zh_TW |
| dc.title | Atmospheric-pressure dielectric-barrier-discharge jet modified polyaniline-reduced graphene oxide-chitosan flexible supercapacitors and fabrication process development of paper-based supercapacitors | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 108-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 陳奕君(I-Chun Cheng),徐振哲(Cheng-Che Hsu),李岳聯(Yueh-Lien Lee) | |
| dc.subject.keyword | 超級電容,聚苯胺,還原氧化石墨烯,殼聚醣,介電質放電噴射電漿,常壓噴射電漿, | zh_TW |
| dc.subject.keyword | Supercapacitor,Polyaniline,Reduced graphene oxide,Chitosan,Dielectric barrier discharge,Atmospheric-pressure plasma, | en |
| dc.relation.page | 120 | |
| dc.identifier.doi | 10.6342/NTU202001821 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2020-07-24 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 應用力學研究所 | zh_TW |
| dc.date.embargo-lift | 2023-07-30 | - |
| 顯示於系所單位： | 應用力學研究所 | |
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