請用此 Handle URI 來引用此文件：
http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/36596完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 楊哲人 | |
| dc.contributor.author | Mei-Chuan Lin | en |
| dc.contributor.author | 林美娟 | zh_TW |
| dc.date.accessioned | 2021-06-13T08:07:07Z | - |
| dc.date.available | 2005-07-27 | |
| dc.date.copyright | 2005-07-27 | |
| dc.date.issued | 2005 | |
| dc.date.submitted | 2005-07-21 | |
| dc.identifier.citation | 參考文獻
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Cohen, The Strengthening of Steel, Trans TSM-AIME, Vol 224, 1962, p638. 15. Roberts, C.S., Trans. AIME, Vol 197, 1953, p.203. 16. Bain, E. C., Trans. AIME, 70 25(1924). 17. G. Wasserman, Mitt. Kaiser-Wilhelm-Inst. Eseinforch, Dusseldorf, 17(1935),149. 18. F.J. Schone, et al., Metall. Trans., 2(1971), 2489. 19. R.F. Mehl, et al., Trans, AIME, 105(1933), 215. 20. A.B. Greninger, A.R. Triano, Trans. AIME, 140(1940), 307. 21. H.K.D.H Bhadeshia, Worked Examples in the Geometry of Crystals, The Institute of Metals, 1987, p.26. 22. H.K.D.H Bhadeshia, Worked Examples in the Geometry of Crystals, The Institute of Metals, 1987, p.9. 23. J.K. Mackenzie, Aust.J.Phys., 1957, vol.10, p.103. 24. H.K.D.H Bhadeshia, Worked Examples in the Geometry of Crystals, The Institute of Metals, 1987, p.59. 25. P.M. Kelly and J. Nutting, JISI., 197(1961), 199. 26. G. Krauss, STEELS﹕Heat Treatment and Processing Principles, 1990, p.351. 27. R W K Honeycombe & H K D H Bhadeshia STEELS﹕Microstructure and Properties 2nd edition 1995, p.38. 28. M. Cohen, The Strengthening of Steel, Trans TSM-AIME, Vol 224, 1962, p638. 29. Roberts, C.S., Trans. AIME, Vol 197, 1953, p.203. 30. Bain, E. C., Trans. AIME, 70 25(1924). 31. G. Wasserman, Mitt. Kaiser-Wilhelm-Inst. Eseinforch, Dusseldorf, 17(1935),149. 32. F.J. Schone, et al., Metall. Trans., 2(1971), 2489. 33. R.F. Mehl, et al., Trans, AIME, 105(1933), 215. 34. A.B. Greninger, A.R. Triano, Trans. AIME, 140(1940), 307. 35. H.K.D.H Bhadeshia, Worked Examples in the Geometry of Crystals, The Institute of Metals, 1987, p.26. 36. H.K.D.H Bhadeshia, Worked Examples in the Geometry of Crystals, The Institute of Metals, 1987, p.9. 37. J.K. Mackenzie, Aust.J.Phys., 1957, vol.10, p.103. 38. H.K.D.H Bhadeshia, Worked Examples in the Geometry of Crystals, The Institute of Metals, 1987, p.59. 39. P.M. Kelly and J. Nutting, JISI., 197(1961), 199. 40. R.L. Patterson and C.M. Wayman, Acta Met., 1966, vol.14, p.347. 41. T. MAKI and C. M. WAYMAN, Transmission Electron Microscopy Studies of Thin Foil Martensite In Fe-Ni and Fe-Ni–C Alloys, Acta Metallurgica. Vol. 25. pp681 693. Pergamon Press. 1977. 42. M.A. Grossmann and E.C. Bain, Principles of Heat Treatment, Amerucan Society for Metals, Metals Park, OH, 1964. 43. K.E. Thelning, Steel and its Heat Treatment, 1974. 44. K.H. Jack, Structural Transformations in the Tempering of High Carbon Martensitic Steel, JISI, Vol 169, 1951, p.26. 45. C.S. Robert, B.L. Averbach, and M. Cohen, The Mechanism and Kinetics of the First Stage of Tempering, Trans ASM, Vol 45,1953,p.576. 46. G.B. Olson and W.S. Owen, Martensite, ASM International, p.576. 47. K.A. Taylor, unpublished research, Massachusetts Institute of Technology, 1985. 48. S. Nagakura, Y. Hirotsu, M. Kusunoki, T. Suzki, and Y. Nakamura, Tempering of Martenstitic Steel Studied by Electron Microscopy and Diffraction, Sci. Red. RITU, Vol A29 (Suppl 1), 1981, p.7. 49. G.B. Olson and W.S. Owen, Martensite, ASM International, p.262. 50. G.R. Speich, Tempering of Low-Carbon Martensite, Trans TMSAIME, Vol 245,1969, p.2552. 51. 王旨玄，板片麻田散鐵及沃斯鐵在440C合金鋼之回火相變態研究，2003，p.14. 52. S.W.K. Shaw and A.G. Quarrell, Ibid., 185, 1975, p.10. 53. Harue Wada, Meta. Trans. A, vol.17A, 1986, p.1585. 54. 佐藤忠雄，熱處理，Vol 13, No.1, 1973,p.2. 55. Hsu Tzu-yao, Chang Wen-Chen, Science Record, New Ser, 1(1957),(3),p.59. 56. 徐祖耀，北京鋼鐵學會學報，1958(5),p.57. 57. D.P. Koistinen and R.E. Marburger, Acta Metall., 7(1959),p.59. 58. X. Changsheng, S. P.,Z. J.,W. Y., Effects of preheating treatment on repeated martensitic transformation under cyclic heating and cooling, Journal of Materials science, 29 (1994) 4051-4055. 59. 張華榮，AISI 440C 不銹鋼之麻田散鐵相變態顯微組織研究，2000，p.75. 60. K.W. Andrew, JISI., 203(1965), p.721. 61. G. Krauss, STEELS﹕Heat Treatment and Processing Principles, 1990, p.43. 62. 王旨玄，板片麻田散鐵及沃斯鐵在440C合金鋼之回火相變態研究，2003，p.51. 63. T.N. Durlu, Structure of the Martensite Midrib in Fe-24% Ni-0.45% C Alloy, Journal of Materials science letters 16(1997) 1307-1308. 64. A.R. Marder and A.O. Benscoter, Trans. ASM, 1968, Vol.61, p293. 65. T. Kakeshita and K. Shimizu: Mem. Inst. Sci.Ind. Res.,Osaka Univ.,Vol. 14, pp. 1067-1070, 1980. | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/36596 | - |
| dc.description.abstract | 摘 要
AISI 440C麻田散鐵系不銹鋼，其成份主要為高含量的碳及鉻元素，使其硬化能很高，均質化處理後採用空冷即可避過肥粒鐵的相線區，但也導致其Ms溫度低於室溫，故需以深冷處理方能相變得到麻田散鐵組織，但基底仍殘有大量沃斯田鐵，故再施以回火處理消除殘留沃斯田鐵，並改善麻田散鐵相變後之韌性與機械性質，期望能得到最佳的性質。 本次實驗著重在深冷後的板片狀麻田散鐵組織及回火處理後的回火板片狀麻田散鐵組織，逐一觀察各項處理後所形成之組織變化，並以穿透式電子顯微鏡分析各相微觀組織。觀察後發現板片狀麻田散鐵基地是由雙晶所組成，有中脊面(midrib)的痕跡及伴隨大量的疊差區；回火板片狀麻田散鐵基地除了雙晶和中脊面外，有多種的合金碳化物得析出，並發現部分中脊面兩側的雙晶有小角度的轉折。除此之外，回火麻田散鐵板片週圍所觀察到的中低碳區麻田散鐵板條狀組織，來推斷殘留沃斯田鐵分解後基底重新分配後的相變結果。 | zh_TW |
| dc.description.abstract | Abstract
AISI 440C is an important alloy steel and is widely applied in medical appliances, cutting tools and turbine blades. The steel typically contains 1 wt% carbon and 17% Cr, so that the MS Temperature is expected to be much lower than the room temperature. After quenching into liquid nitrogen, It gives plate martensite, which has a burst formation with Zig-Zag morphology. There is still remaining a great quantity of retained austenite in the matrix. In order to deliminate the retained austenite, the tempering treatment is necessarily carried out. In the study, plate martensite and tempered martemsite has been examined after different cycles of tempering. The orientation relationship between the twins within the plate martensite has been investigated through the electron diffraction of TEM. In addition, it has found that after multi-tempering cycles the MS temperature gradually rises with increasing the repeated cycling numbers, and that austenite transforms into ferrite and carbides, step by step. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-13T08:07:07Z (GMT). No. of bitstreams: 1 ntu-94-R92527034-1.pdf: 9031577 bytes, checksum: 2c1726ab1ba47bd47b6e06e62033b299 (MD5) Previous issue date: 2005 | en |
| dc.description.tableofcontents | 目 錄
第1章 前言˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙1 第2章 文獻回顧˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙2 2.1 不銹鋼及麻田散鐵系不銹鋼…………………………………….2 2.1.1 AISI 440C不銹鋼……………………………………………...3 2.2 麻田散鐵相變化………………………………………………….4 2.2.1 麻田散鐵的特徵………………………………………………5 2.2.2 麻田散鐵的晶體結構…………………………………………6 2.2.3 麻田散鐵的結晶學……………………………………………7 2.2.4 麻田散鐵的形態學…………………………………………..12 2.2.4.1 板條狀麻田散鐵………………………………………….12 2.2.4.2 板片狀麻田散鐵………………………………………….13 2.3 回火……………………………………………………………...14 2.3.1 回火四階段…………………………………………………..15 2.3.2 回火碳化物…………………………………………………..16 2.3.3 回火與循環回火對基地相變化之影響……………………..17 第3章 材料製備及使用儀器˙˙˙˙˙˙˙˙˙˙˙˙˙˙35 3.1 實驗材料………………………………………………………...35 3.3.1 材料的前製程………………………………………………..35 3.2 實驗流程………………………………………………………...36 3.3 熱模擬儀器……………………………………………………...36 3.4 金相製備………………………………………………………...37 3.5 硬度測試………………………………………………………...37 3.6 電子顯微鏡試片製作及觀察…………………………………...37 第4章 AISI 440C不銹鋼麻田散鐵回火相變態研究˙˙˙˙42 4.1 均質化組織觀察………………………………….…...….……..42 4.1.1 OM之觀察……………………………………..…..…………42 4.2均質化後深冷處理之組織觀察…..………….…..…………...…43 4.2.1 OM之觀察………………………………………….….……..43 4.2.2 SEM之觀察…………………………….…….………..……..44 4.2.3 TEM之觀察………………………………..………..………..45 4.3 相同溫度持溫短時間與長時間回火處理之比較………....…...46 4.3.1 OM之觀察……………………………………………..……..46 4.3.2 SEM之觀察…………………………………………………..48 4.3.3 TEM之觀察………………………………………....………..48 4.4 相同溫度下多次回火處理之比較………………………....…...50 4.4.1 OM之觀察……………………………….……………….…..50 4.4.2 SEM之觀察…………………………….………….……..…..51 4.4.3 TEM之觀察…………………………………………………..52 4.5 硬度值的觀察…………………………………………………...55 4.6 熱膨脹儀曲線的觀察…………………………………………...56 第5章 結論˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙100 第6章 建議未來工作˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙102 第7章 參考文獻˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙˙103 | |
| dc.language.iso | zh-TW | |
| dc.title | AISI 440C不銹鋼深冷及隨後回火相變態之電子顯微鏡微結構研究 | zh_TW |
| dc.title | The study of the microstructure of AISI 440C steel's transformation by deep-cooling and tempering. | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 93-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 鄭國華,侯春看,林招松,林新智 | |
| dc.subject.keyword | 440C不銹鋼,板片狀麻田散鐵,雙晶,中脊面(midrib), | zh_TW |
| dc.subject.keyword | 440C stainless steel,plate martensite,twins,midrib, | en |
| dc.relation.page | 106 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2005-07-21 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 材料科學與工程學研究所 | zh_TW |
| 顯示於系所單位： | 材料科學與工程學系 | |
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