請用此 Handle URI 來引用此文件：
http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/43321完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 馬小康 | |
| dc.contributor.author | Kuo-Lun Tseng | en |
| dc.contributor.author | 曾國倫 | zh_TW |
| dc.date.accessioned | 2021-06-15T01:49:27Z | - |
| dc.date.available | 2014-07-14 | |
| dc.date.copyright | 2009-07-14 | |
| dc.date.issued | 2009 | |
| dc.date.submitted | 2009-07-06 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/43321 | - |
| dc.description.abstract | 本研究為二氧化鈦(TiO2)在染料敏化太陽能電池(dye-sensitized solar cells, DSSCs)上之應用，利用預混式燃燒器火焰，添加鈦系化合物C12H28O4Ti(TTIP)，並以氣相燃燒合成奈米級TiO2顆粒，討論其晶相純度及粒徑大小，當O2/N2=30/70、Φ=1.0、TTIP=0.89%，時，粉末粒徑約為50nm，Anatase晶相含量為67%，由於改變收集方式，因此此數據與本實驗室先前所製作之Anatase晶相含量為97.7%相比較差，將本實驗製作之顆粒應用在染料敏化太陽能電池上可得到最佳光電轉換效率1.17%。
DSSCs之製備主要探討電池之工作電極之TiO2薄膜厚度、兩電極間距離以及電解液調配方式等數個研究方向。工作電極方面以刮刀成膜法(doctor blade method)製做，討論TiO2膜厚度，結果發現使用4克的P25 TiO2粉末加上15毫升去離子水，0.5毫升乙醯丙酮與0.5毫升界面活性劑(X-100)，塗佈三層TiO¬2薄膜厚度之DSSCs效率最佳；兩電極間厚度以100μm為最佳；在電解液的選用上，使用濃度為0.5M-0.05M 之LiI-I2，溶劑為體積比Propylene carbonate：Acetonitrile為9：1之電解液，再加入濃度為0.5M之 4-tert-butylpyridine(TBP)，最佳光電轉換效率可達2.115%。 | zh_TW |
| dc.description.abstract | Flame synthesis of nanosized titanium oxide particles with the precursor titanium isopropoxide (TTIP) were used in dye-sensitized solar cells (DSSCs). In this study, particles collected in the premixed flames were studied for their morphology, crystal phase purity, and size. Results from X-ray diffraction (XRD) analyses show that TiO2 crystal phase purity and the size of TiO2 nanoparticles may be effectively controlled by the oxygen concentration and equivalence ratio(Φ). As a result, the anatase purity and the size of TiO2 particle can be 67% and 50nm. TiO2 nanoparticles are formed under the conditions of O2/N2=30/70,Φ=1.0, and TTIP=0.89%. Because of the different collected mothod, this particle anatase purity is lower than 97.7% that collected before. However, DSSCs are developed by using a dye-sensitized nanocrystalline TiO2 film display the photo-energy efficiency of 1.17%.
DSSC is an alternative method for the development of a new generation of photovoltaic devices. DSSC is a combination of several materials, consisting of a transparent electrode coated with a dye-sensitized mesoporous film of nanocrystalline particles of TiO2, an electrolyte containing a suitable redox-couple and a platinum coated counter-electrode. Ruthenium 535-bis TBA (N719) is used as the dyesensitizers. The photo-energy conversion efficiency of DSSCs depends on the properties of its components. The photo-energy conversion efficiency of DSSCs can be optimized up to 2.115%, when the anode electrode made by doctor blade method with three layers. Furthermore, the spacer thickness is 100μm, and the electrolyte condition become [LiI]-[ I2] is 0.5M-0.05M in volume ratio Propylene Carbonate(PC)：Acetonitrile is 9：1 with 0.5M 4-tert-butylpyridine(TBP). | en |
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| dc.description.tableofcontents | 第一章 緒論1
1.1 前言 1 1.2 研究背景2 1.3 太陽能電池3 1.3.1 單晶矽4 1.3.2 多晶矽5 1.3.3 非晶矽5 1.3.4 化合物半導體II-VI 族(CdS, CdTe, CuInSe2)5 1.3.5 化合物半導體III-V 族(GaAs, InP, InGaP) 6 1.3.6 染料敏化太陽能電池6 1.3.7 塑膠太陽能電池6 1.3.8 奈米碳管太陽能電池7 1.4 奈米顆粒7 1.5 研究動機與目的9 第二章 TiO2文獻回顧與理論基礎12 2.1 TiO2基本介紹 12 2.1.1 Anatase/Rutile 晶相之介紹12 2.1.2 光觸媒Photocatalyst13 2.2 奈米微粒的製備14 2.2.1 奈米微粒子的物理製備方法15 2.2.2 奈米微粒子的化學製備方法15 2.3 文獻回顧17 第三章 DSSCs文獻回顧與理論基礎24 3.1 DSSCs發展24 3.2 DSSCs構造24 3.3 DSSCs光電轉換原理29 3.4 光電轉換特性 30 3.5 DSSCs文獻回顧 31 第四章 奈米微粒子實驗研究與方法35 4.1 實驗基本架構與參數定義 35 4.1.1 實驗基本架構35 4.1.2 實驗參數定義35 4.2 TTIP介紹36 4.3 實驗設備36 4.3.1 燃燒器系統 36 4.3.2 氣體流量與燃料輸送系統37 4.3.3 其他設備37 4.4 實驗步驟38 4.4.1 實驗前準備 38 4.4.2 流量計與熱電偶之校正 39 4.4.3 實驗操作條件41 4.4.4 火焰之定量量測及定性觀察41 4.4.5 燃燒產物的收集與分析 42 第五章 DSSCs實驗研究與方法 45 5.1 材料準備45 5.2 實驗設備46 5.3 敏化太陽能電池各部之製備46 5.3.1 工作電極製備46 5.3.2 對電極製備47 5.3.3 敏化染料的配製48 5.3.4 電解液的配置48 5.4 DSSCs組裝與測試48 第六章 結果與討論 50 6.1 燃燒法粉末分析50 6.1.1 火焰的量測與觀察50 6.1.2 產物晶相分析結果51 6.1.3 產物粒徑之分析53 6.1.4 燃燒合成TiO2粉末於敏化太陽能電池之應用 54 6.2 改變DSSCs之變因討論55 6.2.1 薄膜厚度對DSSCs所產生的影響55 6.2.2 兩電極間距離對DSSCs之影響57 6.2.3 不同電解液對於DSSCs之影響57 第七章 結論與建議 60 7.1 結論 60 7.2 建議 61 參考文獻 63 附表72 附圖77 | |
| dc.language.iso | zh-TW | |
| dc.title | TiO2奈米顆粒應用於DSSCs之研究 | zh_TW |
| dc.title | Experimental study on the dye-sensitized solar cells using TiO2 nanoparticles | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 97-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 王興華,顏溪成 | |
| dc.subject.keyword | 奈米,敏化太陽能電池,二氧化鈦,TTIP,燃燒合成, | zh_TW |
| dc.subject.keyword | Nanoparticles,TiO2,Synthesis,TTIP,DSSC, | en |
| dc.relation.page | 105 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2009-07-06 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 機械工程學研究所 | zh_TW |
| 顯示於系所單位： | 機械工程學系 | |
文件中的檔案：
| 檔案 | 大小 | 格式 | |
|---|---|---|---|
| ntu-98-1.pdf 目前未授權公開取用 | 9.33 MB | Adobe PDF |
系統中的文件，除了特別指名其著作權條款之外，均受到著作權保護，並且保留所有的權利。