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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 丁健芳 | zh_TW |
| dc.contributor.advisor | Chien-Fang Ding | en |
| dc.contributor.author | 張宇 | zh_TW |
| dc.contributor.author | Yu Chang | en |
| dc.date.accessioned | 2025-08-19T16:11:06Z | - |
| dc.date.available | 2025-08-20 | - |
| dc.date.copyright | 2025-08-19 | - |
| dc.date.issued | 2025 | - |
| dc.date.submitted | 2025-08-07 | - |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/98783 | - |
| dc.description.abstract | 近年來，乙醯氨基酚（Acetaminophen, APAP）在臨床診斷之研究日益增多。本研究旨在開發一種快速、靈敏且具成本效益的電化學感測元件，目標為偵測液體中之APAP。本感測器以CO₂雷射誘導聚醯亞胺（Polyimide, PI）薄膜生成石墨烯（Laser-induced graphene, LIG），再修飾於玻璃碳電極（Glassy carbon electrode, GCE）表面，形成 LIG/GCE 感測面。材料特性透過四點探針（Four-point probe）、場發射掃描式電子顯微鏡（Field emission scanning electron microscope, FESEM）、拉曼光譜儀（Raman spectrometer）、X 光光電子能譜儀（X-ray photoelectron spectroscopy, XPS）與X射線繞射（X-ray diffractometer, XRD）進行驗證，以評估其微觀結構、化學組成與結晶性。在電化學性能分析方面，本研究採用循環伏安法（Cyclic voltammetry, CV）與方波伏安法（Square wave voltammetry, SWV）進行測試。結果顯示，LIG/GCE 靈敏度（Sensitivity）為0.157 µA·µM⁻¹·cm⁻²、檢測極限（Limit of detection, LOD）為3.95 µM，寬廣的線性範圍（Linear range）5–120 µM，並展現出優異的抗干擾能力與選擇性。本研究展示 LIG 技術在感測APAP領域的潛力，具備快速製備與低成本等優勢，可望應用於人類尿液中對APAP的偵測。 | zh_TW |
| dc.description.abstract | In recent years, acetaminophen (APAP) has attracted growing attention in clinical diagnostics monitoring. This study aims to develop a rapid, sensitive, and cost-effective electrochemical sensor for APAP detection in aqueous media. The sensor uses laser-induced graphene (LIG), fabricated by CO₂ laser irradiation of a polyimide (PI) film, to modify a glassy carbon electrode (GCE), forming a LIG/GCE sensing platform. The structural and chemical properties of LIG were characterized via Four-point probe, FESEM, Raman spectroscopy, XPS, and XRD. Electrochemical performance was evaluated using cyclic voltammetry and square wave voltammetry. Results show the LIG/GCE electrode exhibits a sensitivity of 0.157 µA·µM⁻¹·cm⁻²,a limit of detection (LOD) of 3.95 µM, and a broad linear range of 5–120 µM. The sensor demonstrates excellent selectivity and anti-interference capability, making it suitable for complex matrices. This study demonstrates the potential of LIG technology for APAP sensing, offering advantages such as rapid fabrication and low cost, and shows promise for application in detecting APAP in human urine. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2025-08-19T16:11:06Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2025-08-19T16:11:06Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | 致謝 i
摘要 ii Abstract iii 目次 iv 圖次 viii 表次 x 第一章 緒論 1 1.1 研究背景與動機 1 1.2 研究目的 2 1.3 研究架構 2 第二章 文獻回顧 4 2.1 乙醯氨基酚 4 2.1.1 乙醯氨基酚藥理作用與潛在危害 4 2.1.2 乙醯氨基酚檢測方法 5 2.1.2.1 氣相色譜-質譜法 5 2.1.2.2 電泳法 5 2.1.2.3 分光光度法 6 2.1.2.4 電化學法 6 2.2 石墨烯 7 2.2.1 石墨烯的製備方法 8 2.2.1.1 化學氣相沉積法 8 2.2.1.2 氧化還原法 9 2.2.1.3 機械剝離法 9 2.2.1.4 電化學剝離法 10 2.2.1.5 化學剝離法 10 2.2.1.6 雷射誘發石墨烯 10 2.3 電化學方法之乙醯氨基酚感測件 11 2.4 小結 12 第三章 研究方法 14 3.1 實驗材料與藥品 14 3.2 實驗設備 15 3.2.1 雷射系統 15 3.2.2 電化學分析系統 16 3.2.3 去離子水系統 19 3.2.4 超音波震盪機 20 3.2.5 精密天秤 20 3.3 實驗流程 21 3.4 實驗分析儀器 23 3.4.1 四點探針 23 3.4.2 場發射掃描式電子顯微鏡 25 3.4.3 拉曼光譜儀 27 3.4.4 X 光光電子能譜儀 28 3.4.5 X 射線繞射儀 30 3.5 雷射誘發石墨烯修飾玻璃碳電極製備 32 3.6 電化學感測方法 33 3.6.1 循環伏安法 33 3.6.2 方波伏安法 34 3.6.3 乙醯氨基酚感測實驗 35 3.6.4 干擾物測試 37 第四章 結果與討論 38 4.1 雷射誘發石墨烯之結果分析 38 4.1.1 雷射誘發石墨烯之外觀 38 4.1.2 雷射誘發石墨烯之四點探針片電阻率分析 38 4.1.3 雷射誘發石墨烯之 FESEM 表面形貌分析 39 4.1.4 雷射誘發石墨烯之拉曼光譜分析 44 4.1.5 雷射誘發石墨烯之 XPS 化學性質分析 46 4.1.6 雷射誘發石墨烯之 XRD 分析 50 4.1.7 最佳雷射能量密度之綜合評估與選擇 51 4.2 電化學之乙醯氨基酚感測結果與分析 52 4.2.1 LIG 修飾於 GCE 之循環伏安量測 52 4.2.2 LIG 修飾於 GCE 之方波伏安量測 55 4.2.3 干擾物測試 59 第五章 結論與未來展望 60 5.1 結論 60 5.2 未來展望 60 參考文獻 63 附錄 A — Abbreviation 74 A.1 Abbreviation 74 | - |
| dc.language.iso | zh_TW | - |
| dc.subject | PI 薄膜 | zh_TW |
| dc.subject | 乙醯氨基酚 | zh_TW |
| dc.subject | 石墨烯 | zh_TW |
| dc.subject | CO₂雷射 | zh_TW |
| dc.subject | graphene | en |
| dc.subject | Acetaminophen | en |
| dc.subject | CO₂ laser | en |
| dc.subject | PI film | en |
| dc.title | 雷射誘導石墨烯修飾玻璃碳電極於乙醯氨基酚檢測之研究 | zh_TW |
| dc.title | Detection of Acetaminophen Using a Glassy Carbon Electrode Modified with Laser-induced Graphene | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 113-2 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.oralexamcommittee | 陳林祈;廖英志;陳盈君;李旻軒 | zh_TW |
| dc.contributor.oralexamcommittee | Lin-Chi Chen;Ying-Chih Liao;Ying-Chun Chen;Min-Hsuan Lee | en |
| dc.subject.keyword | PI 薄膜,CO₂雷射,石墨烯,乙醯氨基酚, | zh_TW |
| dc.subject.keyword | PI film,CO₂ laser,graphene,Acetaminophen, | en |
| dc.relation.page | 75 | - |
| dc.identifier.doi | 10.6342/NTU202504072 | - |
| dc.rights.note | 同意授權(限校園內公開) | - |
| dc.date.accepted | 2025-08-13 | - |
| dc.contributor.author-college | 生物資源暨農學院 | - |
| dc.contributor.author-dept | 生物機電工程學系 | - |
| dc.date.embargo-lift | 2025-08-20 | - |
| 顯示於系所單位： | 生物機電工程學系 | |
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