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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/92967完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳錦地 | zh_TW |
| dc.contributor.advisor | Chin-Ti Chen | en |
| dc.contributor.author | 圖爾西 | zh_TW |
| dc.contributor.author | TULSIRAM MOODALA BEED PRASANNAKUMAR | en |
| dc.date.accessioned | 2024-07-09T16:10:14Z | - |
| dc.date.available | 2024-07-10 | - |
| dc.date.copyright | 2024-07-09 | - |
| dc.date.issued | 2024 | - |
| dc.date.submitted | 2024-07-08 | - |
| dc.identifier.citation | [1] S.G. Benka, The Energy Challenge, Physics Today 55(4) (2002) 38-39. https://doi.org/10.1063/1.1480780.
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/92967 | - |
| dc.description.abstract | 在本博士論文的第一部分，三碘化鉛甲基銨 (MAPbI3，其中MA代表甲基銨) 鈣鈦礦太陽能電池（PVSCs）的穩定性透過以下方法進行仔細的檢測：氧化鋅-硫化鎘核殼 (ZnO@CdS) 奈米顆粒材料嵌入環氧樹脂膜（EP-ZC膜 具有不同比例的 CdS 殼層厚度，即 EP-ZC1、EP-ZC3 和 EP-ZC6）、元件封裝（玻璃片和紫外線固化凝膠）、以及在不同溫度條件下（10°C、室溫（無溫控）、65°C）進行測試。EP-ZC膜用於屏蔽短波長的太陽光線（紫外線、近紫外線、紫光和深藍光），這些短波長的光線會導致MAPbI3產生光降解，進而降低PVSCs的轉換效率（PCE）。此外，在連續500小時的光照測試中，也記錄了部分元件的外部量子效率（EQE）光譜、與電流密度（J）-電壓（V）的測量結果。此外，透過飛行時間-二次離子質譜法（TOF-SIMS）的分析，來定量比較有、無使用具有光遮蔽功能的EP-ZC膜之鈣態礦封裝元件因MAPbI3降解所產生的碘化物，分別在溫度10°C和65°C下之差異。EP-ZC6膜經10°C、連續500小時光浸潤後之封裝PVSCs元件中，仍維持了98%的初始元件效率，展現出最佳的保護效果。從本研究連續光照的研究結果中來看，我們可以優先考量濕度、溫度和光對PVSCs穩定性的影響。
而本論文的第二部分則集中在多晶和單晶的鈣態礦元件穩定性的比較分析。我們成功地透過擴散輔助空間限制生長法製備了單晶薄膜的鈣態礦元件。在短期元件穩定性的結果中揭示了無論是否使用EP-ZC6膜、或有無元件封裝，單晶鈣態礦元件的穩定性皆比多晶鈣態礦元件更為優良。這些發現指出，穩定、且高效的單晶鈣態礦元件，在產業邁向商業化過程中是一個很有前途的候選者。 | zh_TW |
| dc.description.abstract | In the first part of this Ph.D. thesis, the stability of MAPbI3-based (MA stands for methylammonium) perovskite solar cells (PVSCs) have been carefully examined by ZnO@CdS nanoparticle-embedded epoxy films (EP-ZC films with varying ratios of CdS shell layer thickness i.e., EP-ZC1, EP-ZC3, and EP-ZC6), device encapsulation (of glass sheet and UV-curing gel), and in different temperatures, 10 oC, room temperature (no temperature control), and 65 oC. EP-ZC films are used for shielding the short wavelength of the sunlight (UV, near UV, violet, and deep blue) which causes the photodegradation of MAPbI3 and hence the decline of power conversion efficiency (PCE) of PVSCs. Some external quantum efficiency (EQE) spectra of the device have been recorded alongside of the 500 hr continuous light soaking measurement of current density (J)voltage (V) of the devices. The time-of-flight secondary ion mass spectroscopy (TOF-SIMS) analysis has been performed for a quantitative comparison of the iodide derived from the degradation of MAPbI3 in the encapsulated devices with or without the light-shielding EP-ZC films at 10 oC and 65 oC, respectively. The EP-ZC6 film shows the best protection for encapsulated PVSCs with a 98% of the initial PCE at 10°C after 500 hr continuous light soaking. In this study, from the continuous light soaking results we can prioritize the moisture, temperature, and light in the influence of the stability of PVSCs.
The second portion of the Ph.D. thesis is centered around a comparative analysis between the stability of polycrystalline and single crystal MAPbI3 PVSCs. We have successfully fabricated thin-film single crystal-based MAPbI3 PVSCs using the diffusion-assisted space-confined growth method. Short-term stability results with or without the EP-ZC6 film and with or without encapsulation reveal that single-crystal-based PVSCs are more stable than their polycrystalline counterparts. These findings indicate that single-crystal-based PVSCs are a promising candidate for stable and efficient PVSCs as the industry moves towards commercialization. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2024-07-09T16:10:14Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2024-07-09T16:10:14Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | Table of Contents
Chinese Abstract iii Abstract v Acknowledgements vii Table of contents ix List of Figures xii List of Tables xix List of Abbreviations xxii Chapter 1 Introduction 1 1.1 Solar energy background 1 1.2 Photovoltaic Technologies 1 1.3 Comparison of first, second, and third generation solar cells 4 1.4 Organic inorganic hybrid perovskite structure 5 1.5 Perovskite solar cells device architecture 6 1.6 Deposition techniques of perovskite films 8 1.7 Stability of perovskite solar cells 9 1.7.1 Moisture effect 10 1.7.2 Temperature effect 14 1.7.3 Light effect 16 1.7.4 Oxygen effect 19 1.7.5 Interaction with metallic electrode material 19 1.7.6 Comparison of literature reported stability data of MAPbI3 based PVSCs 21 1.7.7 Single crystal perovskite solar cells 25 1.7.8 Growth of perovskite single crystal thin film (SCTF) 27 1.8 Motivation 32 Chapter 2 Materials and Methods 35 2.1 Materials 35 2.1.1 Synthesis of ZnO QDs 36 2.1.2 Synthesis of ZnO@CdS QDs 36 2.1.3 Preparation of ZnO@CdS (ZC1, ZC3, and ZC6) embedded epoxy films (EP-ZC films) 37 2.1.4 Synthesis of methylammonium iodide (MAI), CH3NH3I 37 2.1.5 Growth of MAPbI3 based thin film single crystal 38 2.2 Physical characterization and instrumentation 38 2.2.1 UV-Vis absorption: Hawlett Packard 8453 / HALO DB-20 Dynamica 38 2.2.2 X-ray diffractometer (XRD): Bruker D8 Advance X-ray Diffractometer 39 2.2.3 Surface profiler (α - step): Detak 150 39 2.2.4 Field-Emission Scanning Electron Microscope (FE-SEM): Ultra Plus Carl Zeiss 40 2.2.5 High-Resolution Transmission Electron Microscope (HR-TEM): JEM-2100F 40 2.2.6 Energy Dispersive X-ray Spectrometer (EDS): Oxford INCA Energy system 41 2.2.7 Solar simulator: Newport 94043A 41 2.2.8 External Quantum Efficiency: Newport 41 2.2.9 Time-of-Flight Secondary Ion Mass Spectroscopy (TOF-SIMS): PHI TRIFT V nano-TOF (ULVAC-PHI, Japan) 42 2.3 Solar cell device fabrication and photovoltaic characterization 43 2.3.1 Fabrication of inverted MAPbI3 polycrystalline thin-film PVSCs 43 2.3.2 Modification to the polycrystalline thin film PVSCs device architecture 45 2.3.3 Fabrication of MAPbI3 thin-film single crystal PVSCs 46 2.3.4 500 hr continuous light-soaking J-V and EQE measurement set-up at 25 °C 48 2.3.5 500 hr continuous light-soaking J-V measurement set-up at 10 °C 49 2.3.6 500 hr continuous light-soaking J-V measurement set-up at 65 °C 50 2.3.7 Perovskite thin-film single crystal device J-V measurement set-up 51 Chapter 3 Mitigating the degradation of MAPbI3 perovskite solar cells under continuous light soaking with ZnO@CdS:epoxy short-wavelength-sunlight shield films 53 3.1 Introduction 53 3.2 Results and discussions 55 3.2.1 Structure and morphology of ZnO@CdS NPs and the optical properties of EP-ZC films 55 3.2.2 Device architecture for 500 hr continuous light soaking 58 3.2.3 Device stability influenced by light 59 3.2.4 Device stability influenced by temperature (heat) 68 3.2.5 Comparing device stability influenced by moisture, temperature (heat), light, or oxygen 91 Chapter 4 MAPbI3 single crystal thin-film solar cell: a short-term stability comparison study 103 4.1 Introduction 103 4.2 Results and discussion 104 4.2.1 Characterization of perovskite thin-film single crystals 104 4.2.2 Solar cell performance analysis 105 4.2.3 Stability study 106 Chapter 5 Conclusions and future outlook 110 5.1 Conclusions 110 5.2 Future outlook 111 References 112 Appendix 155 | - |
| dc.language.iso | en | - |
| dc.title | 三碘化鉛甲基銨之鈣鈦礦太陽能電池的穩定性研究 | zh_TW |
| dc.title | Stability study on MAPbI3 based Perovskite Solar Cells | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 112-2 | - |
| dc.description.degree | 博士 | - |
| dc.contributor.coadvisor | 陳貴賢 | zh_TW |
| dc.contributor.coadvisor | Kuei-Hsien Chen | en |
| dc.contributor.oralexamcommittee | 王立義;王俊凱;陶雨臺 | zh_TW |
| dc.contributor.oralexamcommittee | Lee-Yih Wang;Juen-Kai Wang;Yu-Tai Tao | en |
| dc.subject.keyword | 三碘化鉛甲基銨,多晶薄膜鈣鈦礦太陽能電池,工作穩定性,光遮蔽,連續光浸潤,薄膜單晶生長,單晶鈣鈦礦太陽能電池, | zh_TW |
| dc.subject.keyword | Methylammonium lead triiodide,Polycrystalline thin-film perovskite solar cells,Operational stability,Light shielding,Continuous light soaking,Thin-film single crystal growth,Single-crystal perovskite solar cells, | en |
| dc.relation.page | 157 | - |
| dc.identifier.doi | 10.6342/NTU202401557 | - |
| dc.rights.note | 同意授權(限校園內公開) | - |
| dc.date.accepted | 2024-07-08 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 分子科學與技術國際研究生博士學位學程 | - |
| dc.date.embargo-lift | 2029-07-08 | - |
| 顯示於系所單位： | 分子科學與技術國際研究生博士學位學程 | |
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