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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/89657完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 施養信 | zh_TW |
| dc.contributor.advisor | Yang-hsin Shih | en |
| dc.contributor.author | 王芸珍 | zh_TW |
| dc.contributor.author | Yun-Chen Wang | en |
| dc.date.accessioned | 2023-09-15T16:07:00Z | - |
| dc.date.available | 2023-09-16 | - |
| dc.date.copyright | 2023-09-15 | - |
| dc.date.issued | 2022 | - |
| dc.date.submitted | 2002-01-01 | - |
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Yu, F., Yang, C., Huang, G., Zhou, T., Zhao, Y., Ma, J., 2020b. Interfacial interaction between diverse microplastics and tetracycline by adsorption in an aqueous solution. Sci Total Environ 721, 137729. Zhang, H., Liu, P., Feng, Y., Yang, F., 2013. Fate of antibiotics during wastewater treatment and antibiotic distribution in the effluent-receiving waters of the Yellow Sea, northern China. Marine pollution bulletin 73, 282-290. Zhang, H., Wang, J., Zhou, B., Zhou, Y., Dai, Z., Zhou, Q., Chriestie, P., Luo, Y., 2018. Enhanced adsorption of oxytetracycline to weathered microplastic polystyrene: Kinetics, isotherms and influencing factors. Environ Pollut 243, 1550-1557. Zhang, Y., 2017. Sorption of Polycyclic Aromatic Hydrocarbons in Microplastic Polystyrene. Zhuang, W.R., Wang, Y., Cui, P.F., Xing, L., Lee, J., Kim, D., Jiang, H.L., Oh, Y.K., 2019. Applications of pi-pi stacking interactions in the design of drug-delivery systems. J Control Release 294, 311-326. | - |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/89657 | - |
| dc.description.abstract | 廢棄塑膠顆粒及人工合成的新興有機化合物常共同存在許多水相環境中，然而對於塑膠顆粒與有機化合物間的吸附作用尚不完全清楚。本研究採用十二種塑膠顆粒進行吸附試驗，並藉由比表面積分析儀、X光繞射儀 (X-Ray diffraction, XRD)、衰減全反射傅立葉紅外線光譜儀 (attenuated total reflectance-fourier transform infrared spectrophotometer, ATR-FTIR) 等儀器進行塑膠材料特徵分析，瞭解比表面積、平均孔隙直徑、結晶度及顆粒表面官能基等特性，發現本研究採用的塑膠顆粒尺寸大及比表面積小，導致本研究採用的塑膠顆粒吸附有機化合物量較小，幾乎偵測不到高密度聚乙烯(high-density polyethylene, HDPE)、低密度聚乙烯(low-density polyethylene, LDPE)、線型低密度聚乙烯(linear low density polyethylene, LLDPE)、單聚聚丙烯(mono-material polypropylene, Mono PP)及通用級聚苯乙烯(general purpose polystyrene, GPPS)塑膠顆粒發生吸附作用，並使得吸附平衡時間長達至少14天以上。另其中軟質聚氯乙烯(flexible PVC, FPVC)及修飾型聚苯乙烯(modified PS, MPS)兩種材料具有不同於典型塑膠的單體結構，如C=O官能基及O-H官能基。探討bisphenol A (BPA)、phenol (PEN)及sulfamethoxazole (SMX)三種有機化合物與乙烯-醋酸乙烯酯共聚物(ethylene vinyl acetate copolymer, EVA)、Nylon 6、Nylon 66及FPVC四種塑膠顆粒進行靜置條件及震盪條件下的25℃吸附動力學結果，發現震盪條件會相對於靜置條件縮短吸附平衡時間。其中除了SMX無法偵測到被EVA吸附外，擬一階模型適用於SMX吸附速率，依序為Nylon 6 (0.550 day-1) > Nylon 66 (0.484 day-1) > FPVC (0.254 day-1)。擬二階模型則適用於BPA的吸附速率，排序為EVA (0.066 g/mg·day) > Nylon 66 (0.044 g/mg·day) > Nylon 6 (0.038 g/mg·day) > FPVC (0.025 g/mg·day)。而在phenol則在兩種模型具相同吸附速率的推測，排序皆為EVA > FPVC > Nylon 6 > Nylon 66。另進行不同塑膠顆粒對九種弱疏水性芳香族有機化合物的25℃等溫吸附平衡實驗，可觀察到在本研究採用的初濃度範圍內之等溫吸附曲線平衡曲線圖皆呈高度線性相關，Linear模型具高相關性(相關係數範圍0.899~0.998)，判定大部分吸附機制皆發生以凡德瓦爾力所主導的分配作用。並利用線性模型估算的Kd值作為吸附親和性的比較發現，塑膠顆粒對於有機化合物的吸附會強於河川底泥或土壤等環境基質。其中影響吸附親和性的塑膠特性主要為比表面積及極性，而有機化合物則主要為疏水性質。最終藉由多參數線性自由能關係 (polyparameter linear free energy relationships, pp-LFER)的吸附劑物化參數，表述塑膠顆粒在吸附作用中發生的不同交互作用力，以本研究的實驗結果分析可知，EVA、Nylon 6、Nylon 66、FPVC及MPS五種塑膠顆粒的v值皆具最大正值，Nylon 6、Nylon 66及FPVC的a值為較大負值，EVA的s值為正值而b值為較大負值。 | zh_TW |
| dc.description.abstract | Waste plastic particles and synthetic emerging organic compounds often coexist in many aqueous environments, but the sorption between plastic particles and organic compounds is not completely clear. In this study, 12 kinds of plastic particles were used for sorption test, and specific surface area analyzer, X-Ray diffraction (XRD), Attenuated Total Reflection-Fourier Transform Infrared Spectrometer (ATR-FTIR) were used to analyze the characteristics of plastic materials, and the characteristics of specific surface area, average pore diameter, crystallinity and functional groups of particles were known. It is found that the plastic particles used in this study have large size and small specific surface area, which leads to the small amount of organic compounds adsorbed by the plastic particles used in this study. The sorption of high-density polyethylene (HDPE), low-density polyethylene (LDPE), linear low density polyethylene (LLDPE), mono-material polypropylene (Mono PP) and general purpose polystyrene (GPPS) can hardly be detected, and the sorption equilibrium time is at least 14 days. In addition, flexible PVC (FPVC) and modified PS (MPS) have different monomer structures from typical plastics, such as C=O functional group and O-H functional group. The sorption kinetics of bisphenol A (BPA), phenol (PEN), sulfamethoxazole (SMX) with ethylene vinyl acetate copolymer (EVA), Nylon 6, Nylon 66 and FPVC at 25℃ under static condition and shaking condition was discussed. It was found that shaking condition could shorten the sorption equilibrium time compared with static condition. Except that SMX can't be detected by EVA, the pseudo-first-order model is suitable for SMX sorption rate, and the order is Nylon 6 (0.550day-1) > Nylon 66 (0.484day-1) > FPVC (0.254day-1). The pseudo-second order model is suitable for the sorption rate of BPA, and the order is EVA (0.066g/mg day) > Nylon 66 (0.044g/mg day) > Nylon 6 (0.038g/mg day) > FPVC (0.025g/mg day). On the other hand, PEN has the same sorption rate in the two models, and the order is EVA > FPVC > Nylon 6 > Nylon 66. In addition, the isotherm experiment of nine weakly hydrophobic aromatic organic compounds by different plastic particles at 25℃ shows that the equilibrium curves of isotherm in the initial concentration range used in this study are highly linearly correlated, and the linear model has high correlation (correlation coefficient range 0.899~0.998), which indicates that most sorption mechanisms have partition dominated by van der waals force. The Kd value estimated by the linear model is used as the comparison of sorption affinity. It is found that the sorption of organic compounds by plastic particles is stronger than that of environmental substrates such as river sediment or soil. Among them, the characteristics of plastics that affect sorption affinity are mainly specific surface area and polarity, while organic compounds are mainly hydrophobic. Finally, according to the physical and chemical parameters of the adsorbent with polyparameter linear free energy relationships (pp-LFER), the different interaction forces of plastic particles in sorption are expressed. According to the analysis of the experimental results of this study, The v values of EVA, Nylon 6, Nylon 66, FPVC and MPS all have maximum positive values, and the a values of Nylon 6, Nylon 66 and FPVC are relatively negative, while the s values of EVA are positive and the b values are relatively negative. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2023-09-15T16:07:00Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2023-09-15T16:07:00Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | 誌謝 I 中文摘要 II Abstract III 目錄 V 表目錄 IX 圖目錄 XI Abbreviations XVI 第一章 前言 1 1.1 塑膠的危害 1 1.2 研究背景 1 1.3 研究目的 2 第二章 文獻回顧 3 2.1 常見的塑膠 3 2.1.1 PE 3 2.1.2 PP 3 2.1.3 EVA 3 2.1.4 PA 4 2.1.5 PVC 4 2.1.6 PS 4 2.2 環境水域中常見的新興有機化合物 5 2.2.1 Bisphenol A 5 2.2.2 Phenol 6 2.2.3 Sulfamethoxazole 6 2.2.4 Tebuconazole 6 2.2.5 Ofloxacin 6 2.2.6 Pindolol 7 2.2.7 Trimethopreim 7 2.2.8 Vinclozolin 7 2.2.9 Triclosan 8 2.3 塑膠顆粒對於有機化合物的吸附 8 2.3.1 吸附作用 8 2.3.2 吸附動力學 8 (一) 擬一階模型及擬二階模型 9 (二) 顆粒內擴散模型 10 (三) 薄膜擴散模型 10 2.3.3 等溫吸附曲線 10 (一) 線性模型 10 (二) Freundlich吸附模型 11 (三) 塑膠顆粒吸附有機化合物的研究 12 2.3.4 影響吸附的因素 14 (一) 有機化合物的極性(logKow) 14 (二) 粒徑與比表面積 14 (三) 結晶度 16 (四) 不同塑膠種類的表面官能基 16 2.3.5 塑膠顆粒對有機化合物的吸附之常見機制及作用力 17 (一) 分配效應 17 (二) 孔隙填充機制 17 (三) 疏水相互作用 17 (四) π-π相互作用 18 (五) 氫鍵及鹵素鍵 18 2.3.6 多參數線性自由能關係(pp-LFER) 18 第三章 實驗材料與方法 20 3.1 材料 20 3.1.1 實驗藥品 20 3.1.2 吸附劑 20 3.1.3 吸附質 21 3.2 實驗方法 23 3.2.1 吸附劑的表徵分析 23 (一) X光繞射 23 (二) 傅立葉紅外線光譜 23 (三) 比表面積分析 23 3.2.2 吸附動力學及等溫吸附實驗 24 第四章 結果與討論 31 4.1 塑膠顆粒特性分析 31 4.1.1 塑膠顆粒之粒徑、比表面積及平均孔徑 31 4.1.2 塑膠顆粒的結晶度 34 4.1.3 塑膠顆粒的表面官能基 37 (一) LDPE及LLDPE 37 (二) Mono PP 38 (三) EVA 38 (四) Nylon 6及Nylon 66 39 (五) Flexible PVC 40 (六) GPPS 41 (七) Modified PS 41 4.2 塑膠顆粒吸附各種有機化合物之動力學 42 4.2.1 Triclosan 42 4.2.2 Bisphenol A 43 4.2.3 Phenol 44 4.2.4 Sulfamethoxazole 44 4.2.5 Tebuconazole 46 4.2.6 Ofloxacin 46 4.2.7 Pindolol 47 4.2.8 Trimethoprim 47 4.2.9 Vinclozolin 48 4.2.10 吸附質及吸附劑的量對於吸附平衡時間之關係 49 4.3 吸附動力學之分析 51 4.3.1 Bisphenol A的吸附動力學分析 52 4.3.2 Phenol的吸附動力學分析 54 4.3.3 Sulfamethoxazole的吸附動力學分析 56 4.3.4 同種塑膠顆粒對於不同有機化物的吸附動力學分析 57 4.4 等溫吸附曲線 59 4.4.1 同種有機化合物在不同塑膠顆粒的等溫吸附曲線 59 (一) 七種塑膠顆粒吸附triclosan的等溫吸附 59 (二) 四種塑膠顆粒吸附bisphenol A的等溫吸附 63 (三) 五種塑膠顆粒吸附phenol的等溫吸附 66 (四) 四種塑膠顆粒吸附sulfamethoxazole的等溫吸附 69 (五) 四種塑膠顆粒吸附tebuconazole的等溫吸附 72 (六) 一種塑膠顆粒吸附ofloxacin的等溫吸附 75 (七) 兩種塑膠顆粒吸附pindolol的等溫吸附 76 (八) 兩種塑膠顆粒吸附trimethoprim的等溫吸附 78 (九) 四種塑膠顆粒吸附vinclozolin的等溫吸附 80 4.5 同種有機化合物在不同塑膠顆粒上的吸附分析 82 4.5.1 Triclosan 82 4.5.2 Bisphenol A 83 4.5.3 Phenol 84 4.5.4 Sulfamethoxazole 85 4.5.5 Tebuconazole 86 4.5.6 Pindolol 87 4.5.7 Trimethoprim 88 4.5.8 Vinclozolin 88 4.6 pp-LFER估計Kd與吸附實驗線性擬合Kd結果之比較 90 4.7 同種塑膠顆粒對於不同有機化合物的吸附親和性分析 95 4.7.1 EVA對不同有機化合物的吸附 95 4.7.2 Nylon 6對不同有機化合物的吸附 96 4.7.3 Nylon 66對不同有機化合物的吸附 97 4.7.4 Flexible PVC對不同有機化合物的吸附 98 4.7.5 Modified PS對不同有機化合物的吸附 100 第五章 結論 102 附錄 104 參考資料 129 | - |
| dc.language.iso | zh_TW | - |
| dc.title | 塑膠顆粒吸附水中有機化合物之研究 | zh_TW |
| dc.title | Sorption of Organic Compounds in Plastic Particles in Water | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 110-2 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.oralexamcommittee | 郭大孚 | zh_TW |
| dc.contributor.oralexamcommittee | Chin-Yun Chen;Meei-Ling Chang;Dave KUO | en |
| dc.subject.keyword | 塑膠顆粒,有機化合物,吸附,動力學,等溫吸附曲線, | zh_TW |
| dc.subject.keyword | Plastic particles,Organic compounds,Sorption,Kinetics,Isotherm, | en |
| dc.relation.page | 142 | - |
| dc.identifier.doi | 10.6342/NTU202204167 | - |
| dc.rights.note | 同意授權(全球公開) | - |
| dc.date.accepted | 2022-09-29 | - |
| dc.contributor.author-college | 生物資源暨農學院 | - |
| dc.contributor.author-dept | 農業化學系 | - |
| 顯示於系所單位： | 農業化學系 | |
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