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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳建彰(Jian-Zhang Chen) | |
| dc.contributor.author | Jung-Hsien Chang | en |
| dc.contributor.author | 張榮憲 | zh_TW |
| dc.date.accessioned | 2022-11-25T05:34:24Z | - |
| dc.date.available | 2024-07-31 | |
| dc.date.copyright | 2021-08-18 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-07-22 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/82031 | - |
| dc.description.abstract | " 本研究利用常壓電漿(Atmospheric Pressure Plasma Jet, APPJ)合成碳材-金屬氧化物複材並用於儲能元件。首先在碳布電極上網印石墨烯-氯化亞錫(rGO-SnCl2)前驅體，並透過大氣電漿製備石墨烯-二氧化錫(rGO-SnO2)電極，最後組裝成對稱型超級電容。實驗比較了氮氣及二氧化碳電漿製程的差異性。 第一部分先使用穩定且成熟的氮氣常壓噴射電漿來進行，並證實複合材料用於儲能的可行性。透過各項分析得以證實最佳製程時間僅需300秒。在材料分析上，由掃描式電子顯微鏡發現石墨烯表面有大量奈米顆粒形成，因此更進一步透過X射線光電子能譜儀鑑定材料化學結構，證實奈米顆粒是來自於二氧化錫的形成，X射線繞射儀也可見二氧化錫的晶相。亦進行了能量色散X光譜儀、拉曼光譜儀等完整材料分析。在實際應用於軟性超級電容時，以定電流充放電，電流0.25 mA的條件量測，其面積電容值達47.52 mF/cm2。在Trasatti plots分析中，電雙層電容(EDLC)及擬電容(PC)貢獻各佔約50%。 證實了氮氣常壓電漿於材料製備的可行性後，接著使用二氧化碳龍捲風式常壓噴射電漿來製備rGO-SnO2電極。在顯微分析及化學鑑定有類似於氮氣電漿實驗的結果。而在電化學分析中，本部分聚焦於電漿系統對碳布及石墨烯-二氧化錫石墨烯-二氧化錫超級電容個別的影響。以指數率分析可見碳布表現出電雙層電容行為；石墨烯-二氧化錫表現出擬電容行為。碳布的儲能效果較不明顯，主要仍來自石墨烯-二氧化錫複合材料，製備的軟性超級電容之面積電容值達37.17 mF/cm2，且保持理想的穩定性，也成功證實驅動外部發光二極體的可行性。" | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-25T05:34:24Z (GMT). No. of bitstreams: 1 U0001-2007202123222500.pdf: 11227898 bytes, checksum: 41c43b97c60ed69bca4196607926cc63 (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | 誌謝 i 摘要 ii Abstract iii 第一章 緒論 1 1.1 前言 1 1.2 研究動機 2 1.3 論文大綱 4 第二章 理論與文獻回顧 5 2.1 超級電容介紹 5 2.1.1 超級電容與其他能源元件之特性比較 5 2.1.2 超級電容架構與儲能機制 6 2.1.3 超級電容活性材料 10 2.1.4 超級電容電解液 15 2.2 石墨烯與二氧化錫 17 2.2.1 石墨烯 17 2.2.2 二氧化錫 19 2.2.3 石墨烯-二氧化錫合成法回顧 20 2.3 常壓電漿 23 2.3.1 電漿介紹 23 2.3.2 常壓電漿介紹以及超級電容的製程應用 24 第三章 實驗流程及儀器介紹 27 3.1 實驗材料及儀器 27 3.2 實驗步驟 29 3.2.1 還原氧化石墨烯-氯化亞錫前驅漿料製備 29 3.2.2 還原氧化石墨烯-二氧化錫電極之製備 29 3.2.3 調配凝膠態電解液 32 3.2.4 軟性超級電容全元件製備 32 3.3 分析儀器介紹 33 3.3.1 光放射光譜儀 33 3.3.2 掃描式電子顯微鏡及能量色散X射線譜 34 3.3.3 拉曼光譜儀 35 3.3.4 X射線光電子能譜儀 36 3.3.5 X射線繞射儀 38 3.3.6 電化學分析 39 第四章 結果與討論 43 4.1 實驗一 氮氣常壓噴射電漿於石墨烯-二氧化錫超級電容 43 4.1.1 氮氣常壓電漿基礎物理性質 43 4.1.2 氮氣常壓電漿製程時間對電極表面形貌之影響 46 4.1.3 氮氣常壓電漿製程時間對電極親疏水性之影響 50 4.1.4 氮氣常壓電漿製程時間對電極之拉曼光譜分析 50 4.1.5 氮氣常壓電漿製程對電極材料之結晶性影響 52 4.1.6 氮氣常壓電漿製程時間對電極化學表徵之影響 53 4.1.7 以循環伏安分析氮氣常壓電漿對石墨烯-二氧化錫超級電容之影響 61 4.1.8 以恆電流充放電評估氮氣常壓電漿製程對石墨烯-二氧化錫超級電容之性能 63 4.1.9 以Trasatti plot分析氮氣常壓電漿製備之石墨烯-二氧化錫超級電容 64 4.1.10 氮氣常壓電漿製備之石墨烯-二氧化錫超級電容穩定度量測 66 4.1.11 氮氣常壓電漿製備之石墨烯-二氧化錫超級電容點亮LED 67 4.2 實驗二 二氧化碳龍捲風式常壓噴射電漿於石墨烯-二氧化錫超級電容 68 4.2.1 二氧化碳龍捲風式常壓噴射電漿基礎物理性質 68 4.2.2 二氧化碳常壓電漿處理次數對材料表面形貌之影響 70 4.2.3 二氧化碳常壓電漿處理次數對電極親疏水性之影響 73 4.2.4 二氧化碳常壓電漿製程時間對電極化學表徵之影響 74 4.2.5 以循環伏安分析二氧化碳常壓電漿對碳布及石墨烯-二氧化錫超級電容之性能影響 82 4.2.6 以恆電流充放電評估二氧化碳常壓電漿製程對碳布及石墨烯-二氧化錫超級電容之性能 85 4.2.7 以Trasatti plot分析二氧化碳常壓電漿製備之石墨烯-二氧化錫超級電容 88 4.2.8 二氧化碳常壓電漿製備之石墨烯-二氧化錫超級電容穩定性分析 91 4.2.9 二氧化碳常壓電漿製備之石墨烯-二氧化錫超級電容點亮LED 93 4.2.10 以Ragone plot比較氮氣及二氧化碳電漿製程製備之石墨烯-二氧化錫超級電容 93 第五章 結論 95 附錄A: 利用常壓電漿改質石墨氈 96 A.1 摘要 96 A.2 實驗流程 96 A.3 以X射線光電子能譜分析改質之石墨氈 97 參考文獻 99 | |
| dc.language.iso | zh-TW | |
| dc.subject | 石墨烯 | zh_TW |
| dc.subject | 二氧化碳 | zh_TW |
| dc.subject | 超級電容 | zh_TW |
| dc.subject | 常壓電漿 | zh_TW |
| dc.subject | 二氧化錫 | zh_TW |
| dc.subject | 氮氣 | zh_TW |
| dc.subject | Reduced graphene oxide | en |
| dc.subject | Supercapacitor | en |
| dc.subject | Tin oxide | en |
| dc.subject | Carbon dioxide | en |
| dc.subject | Nitrogen | en |
| dc.subject | Atmospheric pressure plasma process | en |
| dc.title | 二氧化碳龍捲風式常壓噴射電漿於石墨烯-氧化錫超級電容之應用 | zh_TW |
| dc.title | Applications of CO2 tornado-type atmospheric pressure plasma jet in reduced graphene oxide-tin oxide supercapacitor | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 陳奕君(Hsin-Tsai Liu),徐振哲(Chih-Yang Tseng),趙宇強 | |
| dc.subject.keyword | 常壓電漿,氮氣,二氧化碳,石墨烯,二氧化錫,超級電容, | zh_TW |
| dc.subject.keyword | Atmospheric pressure plasma process,Nitrogen,Carbon dioxide,Reduced graphene oxide,Tin oxide,Supercapacitor, | en |
| dc.relation.page | 112 | |
| dc.identifier.doi | 10.6342/NTU202101614 | |
| dc.rights.note | 同意授權(限校園內公開) | |
| dc.date.accepted | 2021-07-22 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 應用力學研究所 | zh_TW |
| dc.date.embargo-lift | 2024-07-31 | - |
| 顯示於系所單位： | 應用力學研究所 | |
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