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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/81919完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 黃耀輝(Yaw-Huei Hwang) | |
| dc.contributor.author | Chia-Hsin Liu | en |
| dc.contributor.author | 劉佳欣 | zh_TW |
| dc.date.accessioned | 2022-11-25T03:06:37Z | - |
| dc.date.available | 2024-12-25 | |
| dc.date.copyright | 2021-11-09 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-09-26 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/81919 | - |
| dc.description.abstract | "鑒於人工奈米二氧化鈦（TiO2-ENPs）在各種消費性產品中的使用量日益增加，可能會對環境和人類造成未知的風險，因此對環境中的TiO2-ENPs量化有其必要性。為了正確量化TiO2-ENPs的質量濃度，TiO2-ENPs與天然含鈦奈米微粒之間不同的顆粒組成是區分彼此的關鍵。當在研究環境中測得的鈦與天然追蹤劑(如釩和釔)的元素比高於天然背景的元素比時，則表明有TiO2-ENPs排放的可能。本研究使用多元素單粒子感應耦合電漿質譜儀探討臺灣北部和南部的主要河川水源新店溪流域和高屏溪流域中TiO2-ENPs的分布和含鈦奈米微粒的特徵。 結果顯示，相較於鈦/釩元素比，從臺灣地質條件和不受人為活動干擾的角度來看，釔具有更穩定的特性，因此鈦/釔元素比更適合用來識別含鈦奈米微粒的來源。在兩個流域中普遍檢測到含鈦奈米微粒，其中高屏溪的含鈦奈米微粒主要歸因於人為活動的貢獻。另一方面，新店溪在高河川流量季節時，顯示含鈦奈米微粒來源與天然貢獻有較大關聯，但是，在低河川流量季節時，新店溪侵蝕岩石的能力下降，導致天然來源的含鈦奈米微粒減少，進而增加TiO2-ENPs的貢獻比例。 高屏溪中，經量測推算的TiO2-ENPs質量濃度、含鈦奈米微粒的數目濃度和最常見粒徑範圍分別為0.03-7.43 ng/mL、8.63×10^3-1,643×10^3 part./mL和46-60 nm; 而新店溪中，在高河川流量季節，它們分布範圍分別在 ND-0.325 ng/mL、11.2×10^3-134×10^3 part./mL和 32-52 nm 之間變化，在低河川流量季節，它們分別在 ND-0.268 ng/mL、7.33×10^3-76.4×10^3 part./mL 和 38-58 nm 之間波動。本研究提供了一種可靠的奈米微粒檢測方法，透過顆粒形式含鈦奈米微粒量測來量化TiO2-ENPs的質量濃度，同時可以提供含鈦奈米微粒的數目濃度和顆粒大小的特徵。此外，這些數據對於未來的TiO2-ENPs暴露風險評估甚至是水質控制都是至關重要的。" | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-25T03:06:37Z (GMT). No. of bitstreams: 1 U0001-2509202118074100.pdf: 3547850 bytes, checksum: 071d7590c397d5b4373f8ba75183ed21 (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | 中文摘要 i ABSTRACT ii CONTENTS iv LIST OF FIGURES vii LIST OF TABLES ix Chapter 1 Introduction 1 1.1 Background 1 1.2 Study objectives 2 Chapter 2 Literature Review 4 2.1 Information on nanoparticles 4 2.1.1 Definition 4 2.1.2 Classification 4 2.1.3 TiO2-ENPs 5 2.2 Environmental release pathways and the fate of TiO2-ENPs 6 2.3 Concentrations of Ti-containing NPs/TiO2-NPs in the surface water 9 2.3.1 Ti-containing NPs/TiO2-NPs 9 2.3.2 Anthropogenic vs natural origin of Ti-containing NPs 13 2.4 Toxicity of TiO2-ENPs 18 Chapter 3 Materials and Methods 21 3.1 Description of the study area 21 3.1.1 Gaoping River 21 3.1.2 Xindian River 24 3.2 Sample collections 25 3.2.1 Materials and equipment 25 3.2.2 Sampling strategy 25 3.3 Multi-element sp-ICPMS measurement 28 3.3.1 Nanomaterials and reagents 28 3.3.2 Sample pretreatment 28 3.3.3 sp-ICPMS analysis 29 3.3.4 Calibration curve 32 3.3.5 QA/QC and detection limits 34 3.4 Particle composition 36 3.4.1 Ti/V and Ti/Y 36 3.4.2 Calculation of TiO2-ENPs mass concentration 36 3.5 Statistical analysis: R 37 Chapter 4 Results 38 4.1 Evolution of water chemistry along the rivers 38 4.2 Elemental ratios of Ti with V and Y 45 4.2.1 Gaoping River 45 4.2.2 Xindian River 54 4.3 Spatial distributions of TiO2-ENPs mass concentration along the rivers 61 4.3.1 Gaoping River 61 4.3.2 Xindian River 67 4.4 Number concentrations and size distributions of Ti-containing NPs 72 4.4.1 Gaoping River 72 4.4.2 Xindian River 77 Chapter 5 Discussion 79 5.1 Contributing sources of Ti-NNPs and TiO2-ENPs along the rivers 79 5.1.1 Discerning Ti-containing NPs sources with the elemental ratio 79 5.1.2 Occurrence of TiO2-ENPs and their origins 81 5.1.3 Seasonal changes in mass concentration of Ti-NNPs 85 5.1.4 Comparison of TiO2-ENP mass concentrations in the present work with previous studies 86 5.2 Possible factors governing particle size 91 5.3 Environmental implications 98 5.4 Limitations and analytical perspectives 101 Chapter 6 Conclusions 104 REFERENCES 106 APPENDICES 117 | |
| dc.language.iso | en | |
| dc.subject | 元素比 | zh_TW |
| dc.subject | 多元素單粒子感應耦合電漿質譜儀 | zh_TW |
| dc.subject | 人工奈米二氧化鈦 | zh_TW |
| dc.subject | 天然來源 | zh_TW |
| dc.subject | 地表水 | zh_TW |
| dc.subject | multi-element sp-ICPMS | en |
| dc.subject | TiO2 engineered nanoparticle | en |
| dc.subject | natural source | en |
| dc.subject | elemental ratio | en |
| dc.subject | surface water | en |
| dc.title | 利用元素比區分新店溪和高屏溪流域中含鈦奈米微粒來源 | zh_TW |
| dc.title | Differentiation of Ti-containing Engineered Nanoparticles from Natural Sources in the Xindian River and the Gaoping River Basins with Elemental Ratios | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 吳章甫(Hsin-Tsai Liu),陳美蓮(Chih-Yang Tseng) | |
| dc.subject.keyword | 人工奈米二氧化鈦,天然來源,元素比,地表水,多元素單粒子感應耦合電漿質譜儀, | zh_TW |
| dc.subject.keyword | TiO2 engineered nanoparticle,natural source,elemental ratio,surface water,multi-element sp-ICPMS, | en |
| dc.relation.page | 121 | |
| dc.identifier.doi | 10.6342/NTU202103359 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2021-09-27 | |
| dc.contributor.author-college | 公共衛生學院 | zh_TW |
| dc.contributor.author-dept | 環境與職業健康科學研究所 | zh_TW |
| dc.date.embargo-lift | 2024-12-25 | - |
| 顯示於系所單位： | 環境與職業健康科學研究所 | |
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