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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/81835完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 李篤中(Duu-Jong Lee) | |
| dc.contributor.author | Tzu-Chieh Lin | en |
| dc.contributor.author | 林子傑 | zh_TW |
| dc.date.accessioned | 2022-11-25T03:04:43Z | - |
| dc.date.available | 2023-07-24 | |
| dc.date.copyright | 2021-08-20 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-07-24 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/81835 | - |
| dc.description.abstract | 本文對改質棉布應用在油水分離提供了觀點回顧。 首先描述了棉布表面疏水性的原理並介紹了產生超疏水表面的基礎理論。 然後對親水性棉布改質為疏水性棉布的製備方法進行了回顧和討論。本文提出了根據文獻結論設計出的新製備方法、總結測試方法、全面技術經濟以及永續性分析的必要性。棉布測試展示了流體和表面相互作用在不同應用場景下對確定油水混合物分離效率的重要關鍵。 POSS改質棉布又稱為POSS-CT是通過硫醇-烯加成反應合成，表現出粗糙與水接觸角為142.82±1.17°的疏水表面。POSS-CT用於清除浮油具有0.96 g/g的吸油能力幾乎是純棉布的 3 倍。 單步驟製備的TA-ODA、TA-HDA 和 TA-TDA 是用單寧酸 (TA) 與十八烷基胺 (ODA)、十六烷基胺 (HDA) 和十四烷基胺 (TDA)透過麥可加成/希夫鹼反應分別鍵結。 此外，用 5mM CuSO4 和 19.6mM H2O2 改質 60 分鐘表現出142.87±0.53°、135.99±1.15°和133.27±1.15°的水接觸角，水接觸角隨著烷基胺長度的減少而降低。 TA-ODA、TA-HDA和TA-TDA擁有1.01 g/g、1.00 g/g和0.96 g/g吸油量表現出和POSS改質棉布一樣出色的浮油清除能力。 與POSS-CT相比，單寧酸改質棉布成本低、製造流程簡單、合成溶劑具永續性，更適合於實際應用。 | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-25T03:04:43Z (GMT). No. of bitstreams: 1 U0001-2007202123263100.pdf: 4895991 bytes, checksum: 15f207e54b48171fd9dcc75e4e7bacb6 (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | "口試委員審定書 ⅰ ACKNOWLEDGEMENTS ⅱ ABSTRACT ⅲ 摘要 ⅴ Content ⅵ List of Figures ⅹ List of Tables ⅻⅰ Chapter 1 Introduction 1 Chapter 2 Literature review 5 2.1 Hydrophobicity 5 2.2 The evaluation of surface energy of hydrophobicity 6 2.3 The characteristic of cotton 8 2.4 Hydrophobicity modification of cotton fabric for oil/water separation 9 2.5 Natural inspired method 10 2.6 Michael addition reaction 15 2.7 Schiff base reaction 15 2.8. CuSO4/H2O2-triggered reaction 16 2.9. Thiol-ene click reaction 18 2.10. Polyhedral oligomeric silsesquioxane (POSS) 19 Chapter 3 Material and Experiment methods 21 3.1. Material 21 3.2. Preparation of as-preprared cotton fabric 22 3.3. Fabrication of POSS-modified cotton fabric 22 3.4. Fabrication of tannic acid-modified cotton fabrics 22 3.5. Characterization and instrumentation 24 3.5.1 Fourier Transform Infrared Spectroscopy (FTIR) 24 3.5.2 Nuclear Magnetic Resonance (NMR) 24 3.5.3 X-ray Photoelectron Spectroscopy (XPS) 24 3.5.4 Field-emission Scanning Electron Microscope (FE-SEM) 24 3.5.5 Static Contact angle measurement 25 3.5.6 Ultraviolet-visible spectroscopy (UV-vis) 25 3.5.7 Absorption capacity 25 3.5.8 Oil absorption capacity 25 Chapter 4 Result and discussion 27 4.1 POSS-modified cotton fabric 27 4.1.1 The functional groups of cotton fabric, SH-CT and POSS-CT 27 4.1.2 The structure of POSS, MPTES and POSS-CT 28 4.1.3 The binding energy of cotton, SH-CT and POSS-CT 29 4.1.4 The morphology of surface for cotton fabric, SH-CT and POSS-CT 31 4.1.5 Contact angle measurements 32 4.1.6 Water contact angle for POSS-CT 33 4.1.7 Oil absorption capacity 35 4.2 Tannic acid-modified cotton fabrics 37 4.2.1 The functional groups of cotton fabric and tannic acid-modified cotton fabrics 37 4.2.2 The structure of tannic acid, long chain alkyl amine and tannic acid-modified cotton fabrics 38 4.2.3 The binding energy of cotton fabric, TA-TDA, TA-HDA and TA-ODA 41 4.2.4 The morphology of surface for fabrics 43 4.2.5 Contact angle measurements 45 4.2.6 Anti-wetting ability 48 4.2.7 Effects of reaction parameters for alkylamine grafting 49 4.2.8 Oil absorption capacity 52 4.3 The comparison of reaction conditions and performance for TA-ODA and POSS-CT 55 Chapter 5 Conclusions 56 References 58 List of Figures Figure 2-1. The image (a) of the lotus leaf effect [31]. SEM image of 6 lotus-leaf-like structures (b) from carbon nanotubes [31] and rose –petal-like structure (c) of modified surface [32]. Figure 2-2. Schematic of three phase contact line 6 Figure 2-3. The chemical structure of cotton 8 Figure 2-4. Schematic of fabrication of superhydrophobic cotton fabric 10 via dip coating [60] Figure 2-5. Schematic of formation of hierarchical structure by grafting long chain alkyl compound 10 Figure 2-6. The structure of tannic acid 12 Figure 2-7. Schematic of complexation and Michael addition/Schiff base 13 reaction for tannic acid Figure 2-8. Mechanism of Michael addition/Schiff base reaction between tannic acid and amine 13 Figure 2-9. Schematic of hierarchical structure for tannic acid hybrid coating 14 Figure 2-10. Schematic of secondary reaction for tannic acid-modified hydrophobic cotton fabrics [28, 108, 109] 14 Figure 2-11. Schematic of Michael addition reaction [113] 15 Figure 2-12. Schematic of Schiff base reaction [127] 16 Figure 2-13. Schematic of CuSO4/H2O2-triggered oxidation of dopamine 17 Figure 2-14. Schematic of CuSO4/H2O2-triggered oxidation of tannic acid 18 Figure 2-15. Schematic of thiol-ene click reaction 19 Figure 2-16. The chemical structure of POSS 20 Figure 3-1. Schematic of two stage fabrication process of POSS-CT 23 Figure 3-2. Schematic of the adopted reactions in this work. The two step 23 reactions were performed in the same reactor to establish one-pot modification Figure 3-3. The absorption test (a) Test I (b) Test II 26 Figure 4-1. The FTIR spectra of cotton fabric, SH-CT and POSS-CT 27 Figure 4-2. The 1H NMR spectra of POSS, MPTES nad POSS-CT 28 Figure 4-3. The XPS spectra of POSS-CT. (a) wide scanning; (b) binding energy for C1s 30 Figure 4-4. FE-SEM images (a-c) and EDS spectra (d-f) of cotton fabrics. (a, d) cotton fabric; (b, e) SH-CT; (c, f) POSS-CT 31 Figure 4-5. The wetting envelope of POSS-CT, PTFE, and those for water, gasoline, diesel, and kerosene 32 Figure 4-6. Effects of reaction parameters on water contact angles for POSS-CT.(a) Effects of POSS concentration on water contact angles for 1 hr reaction time; (b) effects of reaction time to water contact angle with 1.6% w/w POSS concentration; (c) effects of contact time on water contact angle. POSS-CT modified by 1.6% w/w POSS for 1 hr 34 Figure 4-7. The FTIR spectra of cotton fabric, TA-TDA, TA-HDA, TA-ODA 37 Figure 4-8. The 1H NMR spectra of TDA, HDA, ODA and tannic acid 39 Figure 4-9. The 1H NMR spectra of TA-TDA, TA-HDA and TA-ODA 40 Figure 4-10. The XPS spectra of C1s for cotton fabric (a), TA-TDA (b), TA-HDA (c) and TA-ODA (d) 42 Figure 4-11. FE-SEM images (a-d) and EDS spectra (e-h) of cotton fabrics. 44 (a,e) Pristine; (b,f) TA-TDA; (c,g) TA-HDA; (d,h) TA-ODA. Figure 4-12. The wetting envelope of TA-ODA, TA-HDA and TA-TDA cotton fabrics, PTFE, and those for water, gasoline, diesel, and kerosene 46 Figure 4-13. The wetting resistance of TA-ODA, TA-HDA and TA-TDA 48 Figure 4-14. Effects of reaction parameters on contact angles water droplets on the modified cotton fabrics. (a) 5 mM CuSO4, 19.6 mM H2O2, pH 8.5; (b) no CuSO4, no H2O2, pH 8.5 (c) TA-ODA, no CuSO4, pH 8.5; (d) TA-ODA, 19.6mM H2O2, pH 8.5; (e) TA-ODA, 5 mM CuSO4, 19.6 mM H2O2 51 List of Tables Table 1. The comparison of price for dopamine hydrochloride and tannic acid 3 Table 2. The comparison of reaction conditions for TA grafting modification tests 3 Table 3. The comparison of price for long chain alkyl compound, POSS, and MPTES 4 Table 4 Measurement results and calculations for POSS-CT fabrics 36 Table 5. The binding energy value of C1s for pristine and modified cotton fabrics 42 Table 6. The contact angles of modified cotton fabrics with water and 47 diiodomethane droplets. Table 7. The absorption capacity of fabrics for water and hexane in Test I 54 and Test II. Table 8. The absorption capacity of fabrics modified with 5mM/19.6mM of 54 CuSO4/H2O2 in 10 min for water and hexane in Test II Table 9. The absorption capacity of fabrics modified with no CuSO4/H2O2 in 54 10 min for water and hexane in Test II Table 10. The comparison of reaction condition and performance for TA-ODA and POSS-CT 55 Table 11. The comparison of price for tannic acid, alkylamine, POSS and MPTES 57 " | |
| dc.language.iso | en | |
| dc.subject | 棉布 | zh_TW |
| dc.subject | 疏水性 | zh_TW |
| dc.subject | 烷基胺 | zh_TW |
| dc.subject | POSS | zh_TW |
| dc.subject | 油水分離 | zh_TW |
| dc.subject | 單寧酸 | zh_TW |
| dc.subject | 測試 | zh_TW |
| dc.subject | testing | en |
| dc.subject | Cotton fabrics | en |
| dc.subject | hydrophobicity | en |
| dc.subject | tannic acid | en |
| dc.subject | alkylamine | en |
| dc.subject | POSS | en |
| dc.subject | oil/water separation | en |
| dc.title | 單寧酸/多面體矽氧烷寡聚物改質疏水化棉布進行油水分離 | zh_TW |
| dc.title | Hydrophobicity modification for cotton fabrics by tannic acid/POSS for oil/water separation | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 賴君義(Hsin-Tsai Liu),黃志彬(Chih-Yang Tseng),朱曉萍 | |
| dc.subject.keyword | 棉布,疏水性,單寧酸,烷基胺,POSS,油水分離,測試, | zh_TW |
| dc.subject.keyword | Cotton fabrics,hydrophobicity,tannic acid,alkylamine,POSS,oil/water separation,testing, | en |
| dc.relation.page | 81 | |
| dc.identifier.doi | 10.6342/NTU202101615 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2021-07-26 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 化學工程學研究所 | zh_TW |
| dc.date.embargo-lift | 2023-07-24 | - |
| 顯示於系所單位： | 化學工程學系 | |
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