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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 童心欣(Hsin-Hsin Tung) | |
| dc.contributor.author | TRAN THI PHUONG QUYNH | en |
| dc.contributor.author | 陳氏芳瓊 | zh_TW |
| dc.date.accessioned | 2022-11-24T03:11:52Z | - |
| dc.date.available | 2021-11-05 | |
| dc.date.available | 2022-11-24T03:11:52Z | - |
| dc.date.copyright | 2021-11-05 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-10-24 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/80653 | - |
| dc.description.abstract | "異丙醇(Isopropyl alcohol, IPA)為半導體製程廠廢水中廣泛常見的污染物，因此本研究利用微波強化高級氧化處理(Microwave-enhanced advanced oxidation processes, MW-enhanced AOPs)並結合過氧化氫(H2O2)，比較在微波催化劑對異丙醇降解效率的影響。在 MW/H2O2 系統中反應90 分鐘內可將IPA完全降解，相較之下，單獨使用微波照射、單獨使用H2O2氧化，或以加熱(Thermal, TH)合併H2O2的系統，其去除IPA的效率分別為4.8%、6.1%和68.2%。IPA降解動力學在MW/H2O2和TH/H2O2系統中遵循擬一階動力反應，而其他系統為擬零階動力反應。在特定H2O2劑量下，降解效率隨著H2O2劑量增加而上升，過量的過氧化氫會捕捉氫氧自由基 而抑制IPA的氧化。MW/H2O2系統降解IPA的中間產物包含丙酮與短鏈有機酸等分別進行定性與定量分析，並以總有機碳的質量平衡來進行確認降解途徑。 對於此微波異相催化氧化系統，H2O2和活性碳(AC)的角色分別為氧化劑和微波吸收劑。本研究另外對於操作參數(過氧化氫濃度-[H2O2]、IPA初始濃度-[IPA]i、催化劑量- AC dosage)對 IPA 礦化的影響以Design-Expert® software version 12設計最佳化操作並以反應曲面方法論（Response surface methodology, RSM）進行優化。本研究所獲得最佳設計條件為：[H2O2] = 0.132 M, 活性碳劑量 = 108 - 123 g/L, [IPA]i = 36.82 - 100 mM, 照射時間= 4 min和照射溫度= 80°C，結果顯示活性碳劑量和初始 IPA濃度為主要去除IPA的影響因子。反應變化曲線中回歸線的R2 = 0.9948 和調整後的R2 = 0.9902顯示模式符合二次式適配。以MW/AC/H2O2組合反應系統相較於其他組合系統去除IPA效率最高和最快。最後，本研究針對高濃度IPA污水設計一上流式連續流微波催化反應器。" | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-24T03:11:52Z (GMT). No. of bitstreams: 1 U0001-2010202114501700.pdf: 5710474 bytes, checksum: e16c066c796c411be51c0b8362bca0d2 (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | "Certificate of dissertation approval from the oral defense committee/國立臺灣大學博士學位論文 i Acknowledgements ii Abstract (Chinese)/ 摘要 iii Abstract (English) v Table of content vii List of tables x List of figures xii List of abbreviation xvi Chapter 1 Introduction 1 1.1 Background/Problem statement 1 1.2 Research objectives 3 1.3 Dissertation organization 3 Chapter 2 Literature review 5 2.1 Characteristics of isopropyl alcohol and its applications 5 2.2 Treatment of IPA-containing wastewater from the semiconductor industry 6 2.3 Microwave-enhanced advanced oxidation processes in organic wastewater treatment 17 2.3.1 Advanced oxidation processes 17 2.3.2 Microwave theory and mechanism 19 2.3.3 Application of MW-enhanced AOPs in organic wastewater treatment 21 2.4 Novelty of the study 27 Chapter 3 Materials and methods 29 3.1 Chemicals and materials 30 3.2 Batch microwave-assisted oxidation experiments 31 3.2.1 Experimental details 31 3.2.2 IPA degradation in real wastewater 33 3.2.3 Kinetic analysis 33 3.3 Batch microwave-assisted heterogeneous catalytic oxidation experiments 36 3.3.1 Experimental details 36 3.3.2 Central composite design and response surface methodology study 38 3.4 Continuous-flow mode microwave-assisted heterogeneous catalytic oxidation experiments 39 3.4.1 Apparatus 39 3.4.2 Experimental details 40 3.5 Analytical methods 43 3.5.1 Identification and quantification of IPA and its metabolites 43 3.5.2 Determination of total organic carbon concentration 43 3.5.3 Determination of chemical oxygen demand concentration 44 3.5.4 Determination of hydrogen peroxide concentration 44 3.5.5 Brunauer-Emmett-Teller (BET) specific surface area analysis 44 Chapter 4 Results and discussion 46 4.1 Microwave-assisted oxidation process – Batch study 46 4.1.1 Degradation kinetics of IPA in the MW-assisted oxidation process 46 4.1.2 Evolution of degradation products over the course of the MW-assisted oxidation process 53 4.1.3 Possible degradation pathways of IPA in the MW-assisted oxidation process 57 4.2 Microwave-assisted heterogeneous catalytic oxidation process – Batch study 62 4.2.1 Preliminary tests - Heterogeneous catalyst screening 62 4.2.2 Mathematical model construction for optimization of IPA degradation in MW/AC/H2O2 system 64 4.2.3 Effect of selected variables 69 4.2.4 Optimization of MW-assisted heterogeneous catalytic oxidation process using RSM approach 75 4.2.5 Comparison of different treatment processes on TOC removal 76 4.2.6 Possible degradation mechanism of IPA in the MW/AC/H2O2 system 77 4.3 Microwave-assisted heterogeneous catalytic oxidation – Continuous flow study 80 4.3.1 Investigation of influencing factors 80 4.3.2 MW-assisted regeneration of AC catalyst 86 Chapter 5 Significance, conclusions and suggestions 90 5.1 Research significance 90 5.2 Conclusions 91 5.3 Suggestions 93 References 94 Appendix I. Degradation products study 110 Appendix II. Continuous flow study 116" | |
| dc.language.iso | en | |
| dc.subject | 降解途徑 | zh_TW |
| dc.subject | 異丙醇 | zh_TW |
| dc.subject | 微波 | zh_TW |
| dc.subject | 高級氧化處理 | zh_TW |
| dc.subject | 中央複合設計 | zh_TW |
| dc.subject | 反應曲面方法論 | zh_TW |
| dc.subject | 降解動力學 | zh_TW |
| dc.subject | microwave | en |
| dc.subject | degradation kinetics | en |
| dc.subject | central composite design and response surface methodology | en |
| dc.subject | advanced oxidation process | en |
| dc.subject | isopropyl alcohol | en |
| dc.subject | degradation pathways | en |
| dc.title | 以微波強化高級氧化處理異丙醇廢水 | zh_TW |
| dc.title | Microwave-enhanced advanced oxidation processes for isopropyl alcohol wastewater treatment | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 博士 | |
| dc.contributor.oralexamcommittee | 闕蓓德(Hsin-Tsai Liu),于昌平(Chih-Yang Tseng),侯嘉洪,林伯勳 | |
| dc.subject.keyword | 異丙醇,微波,高級氧化處理,中央複合設計,反應曲面方法論,降解動力學,降解途徑, | zh_TW |
| dc.subject.keyword | isopropyl alcohol,microwave,advanced oxidation process,central composite design and response surface methodology,degradation kinetics,degradation pathways, | en |
| dc.relation.page | 117 | |
| dc.identifier.doi | 10.6342/NTU202103927 | |
| dc.rights.note | 同意授權(限校園內公開) | |
| dc.date.accepted | 2021-10-25 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 環境工程學研究所 | zh_TW |
| 顯示於系所單位： | 環境工程學研究所 | |
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