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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/79908完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 童世煌(Shih-Huang Tung) | |
| dc.contributor.author | Kai-Pin Chang | en |
| dc.contributor.author | 張鎧馪 | zh_TW |
| dc.date.accessioned | 2022-11-23T09:16:15Z | - |
| dc.date.available | 2021-08-06 | |
| dc.date.available | 2022-11-23T09:16:15Z | - |
| dc.date.copyright | 2021-08-06 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-08-02 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/79908 | - |
| dc.description.abstract | 在靜電紡絲的過程中引入相分離法產生多孔纖維，可以進一步提升其比表面積並增加應用性。然而，受限於溶劑的選擇，高極性的高分子只能紡出緻密的中型孔洞而無法形成巨孔纖維，不過仍有許多應用需要用到高極性材料製成的巨孔纖維，例如空氣懸浮微粒的吸附。為了同時提升極性並產生巨孔纖維，本研究使用包含高、低極性單元的4-乙烯基吡啶-苯乙烯共聚物 (S4VP) 作為材料，並以氯苯 (CB) 與二甲基亞碸 (DMSO) 混和為共溶劑探討其可電紡性與形貌變化。我們發現改變CB/DMSO的比例會使相分離由不同機制主導，包括呼吸圖法 (breath figure)、非溶劑誘導與水蒸氣誘導相分離法，並產生豐富的形貌，例如內外相連的巨孔 (macroporous)、緻密中型孔洞 (mesoporous) 與中空纖維等。為了再提高極性，我們將P4VP混摻到S4VP/CB/DMSO中，不過孔洞形貌也會因此被改變，並且在P4VP量少的時候可以適度增加孔洞尺寸；P4VP較多則會使孔洞合併變成巨大的溝槽或樹洞狀。最後，我們將S4VP/P4VP混摻的巨孔纖維應用於空氣懸浮微粒的吸附。纖維因為同時達到高極性以及巨孔的條件，相較於其他低極性與表面平滑的纖維，吸附速率與三小時內的吸附量有顯著的上升。 | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-23T09:16:15Z (GMT). No. of bitstreams: 1 U0001-2907202112552800.pdf: 6331817 bytes, checksum: a9a94f60762dafa5ba0f4b7cbd932a7f (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | 誌謝 i 摘要 ii Abstract iii 目錄 iv 圖目錄 vii 表目錄 x 第一章 緒論 1 1.1前言 1 1.2研究動機 1 第二章 文獻回顧 3 2.1電紡絲技術介紹 3 2.1.1概述 3 2.1.2電紡過程與原理 3 2.1.3參數條件 7 2.1.4共聚物(Copolymer)與高分子混摻(Polymer blend)之電紡 9 2.2相分離製造孔洞的技術介紹 11 2.2.1Breath Figure法 11 2.2.2蒸氣誘導相分離法(Vapor-Induced Phase Separation) 13 2.2.3熱誘導相分離法(Thermal-Induced Phase Separation) 14 2.2.4非溶劑誘導相分離法(Nonsolvent-Induced Phase Separation) 15 2.3空氣懸浮微粒的吸附 17 2.3.1空氣淨化的方法 17 2.3.2影響吸附過濾效率的因素 17 第三章 實驗方法與儀器 20 3.1實驗材料 20 3.1.1高分子 20 3.1.2溶劑 21 3.1.3鹽類 22 3.2實驗方法 23 3.2.1 S4VP/CB/DMSO三相圖繪製 23 3.2.2 S4VP/P4VP/CB/DMSO三相圖繪製 23 3.2.3電紡流程與參數設定 23 3.2.4纖維截面製備 24 3.2.5纖維直徑、孔洞大小量測 24 3.2.6接觸角測試 25 3.2.7空氣懸浮微粒定時吸附量測試 25 3.2.8空氣懸浮微粒吸附前後形貌觀察 26 3.2.9空氣懸浮微粒吸附速率測試 26 3.3實驗儀器與原理 28 3.3.1場發射掃描式電子顯微鏡 (SEM) 28 3.3.2白金濺鍍機 29 3.3.3接觸角測定器 29 3.3.4分光光譜儀 29 3.3.5熱重分析儀 (TGA) 29 第四章 結果與討論 31 4.1相圖 31 4.2電紡性 33 4.2.1高分子濃度的影響 34 4.2.2 DMSO比例的影響 35 4.3孔洞形貌 37 4.3.1孔洞形成機制 37 4.3.2 DMSO比例的影響 39 4.3.3高分子濃度的影響 46 4.4混摻P4VP的影響 49 4.4.1混摻對相圖的影響 49 4.4.2混摻對電紡性的影響 51 4.4.3混摻對孔洞形貌的影響 53 4.5空氣懸浮微粒過濾之應用 57 4.5.1材料極性與形貌 57 4.5.2吸附量之比較 61 4.5.3吸附速率之比較 68 第五章 結論 72 參考資料 74 附錄 80 | |
| dc.language.iso | zh-TW | |
| dc.subject | 電紡絲 | zh_TW |
| dc.subject | 多孔纖維 | zh_TW |
| dc.subject | 呼吸圖法 | zh_TW |
| dc.subject | 非溶劑誘導相分離 | zh_TW |
| dc.subject | 水蒸氣誘導相分離 | zh_TW |
| dc.subject | 空氣懸浮微粒吸附 | zh_TW |
| dc.subject | Breath figure | en |
| dc.subject | Vapor-induced phase separation | en |
| dc.subject | Nonsolvent-induced phase separation | en |
| dc.subject | Electrospinning | en |
| dc.subject | Aerosol adsorption | en |
| dc.subject | Porous fibers | en |
| dc.title | 4-乙烯基吡啶-苯乙烯共聚物孔洞纖維的製備以及其在空氣懸浮微粒吸附之應用 | zh_TW |
| dc.title | Preparation of Poly(4-vinylpyridine-co-styrene) Porous Fibers for Aerosol Adsorption | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 賴偉淇(Hsin-Tsai Liu),楊大毅(Chih-Yang Tseng),邱昱誠 | |
| dc.subject.keyword | 電紡絲,多孔纖維,呼吸圖法,非溶劑誘導相分離,水蒸氣誘導相分離,空氣懸浮微粒吸附, | zh_TW |
| dc.subject.keyword | Electrospinning,Porous fibers,Breath figure,Nonsolvent-induced phase separation,Vapor-induced phase separation,Aerosol adsorption, | en |
| dc.relation.page | 90 | |
| dc.identifier.doi | 10.6342/NTU202101888 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2021-08-03 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 高分子科學與工程學研究所 | zh_TW |
| 顯示於系所單位： | 高分子科學與工程學研究所 | |
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