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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/7945完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 童國倫 | |
| dc.contributor.author | Minh Hien Le | en |
| dc.contributor.author | 黎恆明 | zh_TW |
| dc.date.accessioned | 2021-05-19T17:59:47Z | - |
| dc.date.available | 2021-09-13 | |
| dc.date.available | 2021-05-19T17:59:47Z | - |
| dc.date.copyright | 2016-09-13 | |
| dc.date.issued | 2016 | |
| dc.date.submitted | 2016-07-18 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/7945 | - |
| dc.description.abstract | The purpose of this study is using an in-situ assisted acetic acid procedure to prepare a MIL-101 as filler in ceramic membrane. The MIL-101 membrane is firstly applied for organic solvent nanofiltration. In this study, the effects of synthetic conditions are investigated to get an invisible defect membrane and nanofiltration performance is also checked to prove the feasible application of MIL-101 membrane.
Incorporation of metal organic framework (MIL-101) as filler on ceramic membrane is firstly investigated. In-situ method assisted by acid modular is utilized to synthesize uniform and defect-free MIL-101 membrane. Effect of additives such as NaOH, HF, CH3COOH and concentration of reactants are surveyed to find out the optimal synthetic conditions. Synthesis of MIL-101 membrane by using in-situ acetic acid-assisted method is proved as efficient way to prepare a compact and dense MIL-101 layer compared to other methods as thermal seeding method, layer by layer seeding method. The MIL-101 membranes are characterized by using a variety of different techniques, including X-ray thin film diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy EDX. MIL-101 is chosen as material filler for membrane in nanofiltration application because of its ability to form the largest pore size in the MOFs’ family and a number of its prominent properties for molecular separation applications such as high surface area and well-defined pore size. Besides, MIL-101 and ceramic substrate are inorganic materials, so they are able to be stable in harsh solvent such as N-methyl-2-pyrrolidone (NMP), dimethyl sulfoxide (DMSO), dimethylacetamide (DMAc), those usually dissolve common polymers. The MIL-101 membranes are applied in organic solvent nanofiltration (OSN) by testing separation of Rose Bengal (RB) from NMP, DMSO, DMAc and ethanol. The MIL-101 membranes show a significantly high rejection but lower permeance compared to bare ceramic membrane. The best flux and rejection of MIL-101 membrane with RB ethanol solution are 1.65 lm-2h-1bar-1 and 99.7% respectively where ratio of chromium nitrate, benzendicarboxylic acid and water is 1:1:277, respectively and 0.8 ml of CH3COOH. The MIL-101 membranes also exhibit the stability under harsh solvent with high rejection of RB and constant flux within 3 hours. | en |
| dc.description.provenance | Made available in DSpace on 2021-05-19T17:59:47Z (GMT). No. of bitstreams: 1 ntu-105-R03524099-1.pdf: 4511501 bytes, checksum: 69e2ae09a971fdefbf3fe0c762e86433 (MD5) Previous issue date: 2016 | en |
| dc.description.tableofcontents | ACKNOWLEDGEMENT i
ABSTRACT ii LIST OF FIGURES vi LIST OF TABLE ix Chapter 1 - Introduction 1 1.1 General overview 1 1.2 Objective 3 Chapter 2 - Literature review 5 2.1 Nanofiltration 5 2.2 Organic Solvent Nanofiltration 8 2.2.1 Classification of organic solvent nanofiltration 9 2.2.2 Membrane characterization 11 2.2 3. System design 13 2.2.4 OSN material and ceramic membrane for OSN 15 2.2.5 Challenges and future development 22 2.3 Metal organic framework – MIL-101 and MOF membranes 24 2.3.1 Metal organic framework 24 2.3.2 MIL-101 26 2.3.3 Metal organic framework composite membranes 35 Chapter 3 - Experimental methods and equipment 54 3.1 Experimental materials 54 3.1.1 Supports 54 3.1.2 Chemicals for MIL-101 particles and MIL-101 membranes 55 3.1.3 Chemical for OSN performance 55 3.2 Experiment 56 3.2.1 Synthesis of MIL-101 particles 56 3.2.2 Synthesis MIL-101 membranes 57 3.3 Characterization of MIL-101 and MIL-101 membrane 60 3.3.1 Field-emission scanning electron microscope (FESEM) 60 3.3.2. X-ray diffracatometer for particles (XRD) 60 3.3.3. X-ray diffracatometer for thin film(XRD) 61 3.3.4 Specific surface area analyzer 61 3.3.5 UV/VIS Spectrophotometer 61 3.4 Nanofiltration performance 62 Chapter 4 - Results and conclusions 64 4.1. Characterization of MIL-101 nanoparticles 64 4.2. Characterization of MIL-101 membranes 68 4.2.1 Effect of additives 68 4.2.2 Effect of concentration of reactants on in situ method 71 4.2.3 Effect of amount of acetic acid 74 4.2.4 Effect of concentration of reactants in defect healing procedure 77 4.2.5 Compare to other methods 79 4.3 OSN performance 81 Chapter 5 Conclusion 88 Chapter 6 Reference 90 | |
| dc.language.iso | en | |
| dc.title | MIL-101陶瓷膜之製備及其於有機溶劑奈米過濾之應用 | zh_TW |
| dc.title | Synthesis of MIL-101 supported on ceramic membrane for organic solvent nanofiltration | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 104-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 黃國楨,莊清榮,林俊德 | |
| dc.subject.keyword | 有機溶劑奈米過濾,MIL-101,陶瓷膜, | zh_TW |
| dc.subject.keyword | organic solvent nanofiltration,MIL-101,ceramic membrane,in-situ method, | en |
| dc.relation.page | 101 | |
| dc.identifier.doi | 10.6342/NTU201600805 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2016-07-18 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 化學工程學研究所 | zh_TW |
| 顯示於系所單位： | 化學工程學系 | |
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