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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 王尚禮(Shan-Li Wang) | |
| dc.contributor.author | Puu-Tai Yang | en |
| dc.contributor.author | 楊圃臺 | zh_TW |
| dc.date.accessioned | 2022-11-23T08:56:51Z | - |
| dc.date.available | 2023-01-31 | |
| dc.date.available | 2022-11-23T08:56:51Z | - |
| dc.date.copyright | 2022-02-21 | |
| dc.date.issued | 2022 | |
| dc.date.submitted | 2022-01-12 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/79259 | - |
| dc.description.abstract | 鉬為動植物生長之必要微量元素，亦為新興污染物。由於過往從微量元素的角度不易探究鉬在土壤中的移動性及生物有效性，因此對此至今尚未完全了解。有鑑於土壤鉬污染對動、植物生長的潛在風險，本研究目的為探討影響鉬在土壤中吸持能力的主要土壤性質，以及對小麥和水稻的有效性。 吸持反應為影響營養元素與污染物在土壤中移動性及有效性的重要反應之一，因此本研究以十一種台灣土壤進行鉬酸根的吸附與脫附實驗，並以皮爾森相關性分析探討影響土壤鉬吸附量與釋出能力的主要土壤性質為何。結果顯示，鉬在土壤中的吸持能力受土壤酸鹼度、游離性鐵鋁氧化物含量以及可交換性鋁和鈣含量所影響。在酸性土壤中鉬酸根的吸持量較高，然而吸附於游離性鐵鋁氧化物上的鉬酸根較易被釋出；而在中鹼性土壤中，則可能形成鉬酸鈣沉澱使其釋出能力較低。雖然土壤鉬吸持能力與游離性鐵鋁氧化物含量呈正相關，而未與無定型鐵氧化物含量達顯著相關，然而隨時間增加，無定型鐵氧化物可能逐漸轉變為結晶性鐵氧化物，而可能進一步影響鉬在土壤中的移動性。故本研究進一步於25及75 ℃下進行水鐵礦老化試驗，並觀察水礦老化對鉬酸根吸持能力之影響。結果顯示，鉬酸根離子主要以四面體雙牙單核的內圈錯合型態吸持於水鐵礦上，並隨水鐵礦逐漸轉變為赤鐵礦的過程中，鉬酸根會首先以八面體雙牙單核的內圈錯合型態吸持於鐵氧化物上，再逐漸被固定到鐵氧化物的結構中，而使鉬酸根的移動性下降。 為探討上述土壤性質如何影響對植物鉬的有效性，本研究以平鎮系 (酸性黏質)、台南系 (酸性砂質)及太康系 (鹼性黏質)土壤進行盆栽試驗，並觀察鉬在小麥與水稻中的累積情形、物種組成，以及鉬在根圈土壤的空間分布。結果顯示，小麥的鉬累積量隨土壤pH上升而增加，顯示土壤酸鹼度為影響小麥鉬累積量的重要因子之一；而水稻對鉬的累積量則以台南系高於太康系，並與土壤溶液中鉬濃度隨土壤pH上升而增加的趨勢不吻合，顯示土壤溶液的鉬濃度未能反映對水稻的鉬有效性。由土壤連續萃取與根部鉬酸根物種的分析推測，造成台南系土壤水稻植體鉬累積較高的主要原因為土壤中無定型鐵氧化物比例較高，使得較高比例的鉬酸根以吸持於無定型鐵氧化物的物種存在於土壤中以及水稻根部，並在浸水還原的狀態下隨鐵氧化物還原溶解釋出，進而被水稻根部所吸收。此結果也顯示植物對鉬吸收所呈現的土壤鉬有效性，無法單純以土壤吸脫附反應以及土壤溶液的結果來評估，而需考慮土壤氧化還原狀態與植物特性等因子的影響。 為了評估土壤鉬污染在環境中的潛在風險，本研究建議後續可進一步研究：(1) 可交換陽離子對鉬由土壤膠體脫附的影響，以了解可交換性陽離子組成如何影響鉬在土壤中的移動性; (2) 鐵的氧化還原反應對鉬的物種形態的影響，以探討水田土壤中鉬的有效性；(3) 釐清控制鉬由土壤移動至根圈並進一步被植物吸收的主要反應與影響因子，以了解影響鉬在土壤中對植物有效性的主要機制。 | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-23T08:56:51Z (GMT). No. of bitstreams: 1 U0001-1001202214362300.pdf: 21052221 bytes, checksum: 6ac0ab0dc3e60ea106ed556529d1561a (MD5) Previous issue date: 2022 | en |
| dc.description.tableofcontents | "摘要 I Abstract III Table of Contents VI List of Figures XI List of Tables XVI 1. Introduction 1 2. Objectives 9 3. Literature review 11 3.1 Occurrence of molybdenum in the natural environment 11 3.1.1 Molybdenum in soils and waters 11 3.1.2 Molybdenum in plants 12 3.2 Chemical speciation of molybdenum in the natural environment 20 3.2.1 Aqueous phase 20 3.2.2 Solid phase 22 3.3 Factors affecting molybdenum mobility and availability in soils 37 3.3.1 pH 37 3.3.2 Fe and Al oxides 38 3.3.3 Organic matter 39 3.3.4 Clay minerals 40 3.3.5 Calcite 41 3.3.6 Coexisting anions 41 3.3.7 Redox and hydraulic condition 42 3.3.8 Aging 43 3.4 Determination of molybdenum speciation and binding configurations 45 3.4.1 Thermodynamic calculations 45 3.4.2 Sequential extractions 49 3.4.3 X–ray absorption spectroscopy (XAS) 54 4. Materials and methods 57 4.1 Sorption and speciation of molybdate in soils: Implications for Mo mobility and availability 57 4.1.1 Soil preparation and characterization 57 4.1.2 Mo sorption and desorption experiments 60 4.1.3 Data Analysis 62 4.1.4 X-ray absorption spectroscopy analysis 63 4.1.5 Calculation of the activity diagram 65 4.1.6 Molybdate sorption on Fe and Al oxides 65 4.2 Effects of pH and aging on the sorption of molybdate by ferrihydrite 68 4.2.1 Preparation of 2-line ferrihydrite 68 4.2.2 Sorption and aging under room temperature (25 ℃) 68 4.2.3 Adsorption and aging under high temperature (75 ℃) 70 4.2.4 Ion chromatography 71 4.2.5 X-ray absorption spectroscopy analysis 71 4.2.6 X-ray diffraction (XRD) analysis 74 4.3 Molybdenum speciation in soils and its availability to rice and wheat plants 75 4.3.1 Soil characterization 75 4.3.2 Pot experiments 76 4.3.3 Plant analysis 78 4.3.4 Sequential Extraction of Mo in soil 79 4.3.5 X-ray absorption spectroscopy analysis 80 4.3.6 Soil thin section preparation and micro X-ray fluorescence (μ-XRF) analysis 83 5. Results and Discussion 85 5.1 Sorption and speciation of molybdate in soils: Implications for Mo mobility and availability 85 5.1.1 Soil properties 85 5.1.2 Sorption of molybdate in soils 88 5.1.3 Desorption of molybdate from soils 100 5.1.4 Chemical speciation of molybdate in soils after sorption 105 5.1.5 Sorption and desorption of molybdate on Al and Fe oxides 118 5.1.6 Conclusions 125 5.2 Effects of pH and aging on the sorption of molybdate by ferrihydrite 126 5.2.1 Molybdate sorption and structural transformation of ferrihydrite at pH 4, 6, and 10 as a function of aging time at 25 ℃ 127 5.2.2 Temporal transformation of ferrihydrite and sorbed molybdate at 75 ℃ 144 5.2.3 Transformation of FSMs as a function of aging time at 75 °C 151 5.2.4 Conclusions 160 5.3 Molybdenum speciation in soils and its availability to rice and wheat plants 161 5.3.1 Soil properties 162 5.3.2 Potential Molybdate toxicity to rice and wheat seedlings 164 5.3.3 Accumulation of Mo in wheat and rice plants grown until grain harvest 175 5.3.4 The release of Mo into soil solutions under submerged condition 182 5.3.5 Speciation and fractionation of molybdenum in rice soils 187 5.3.6 Distribution and speciation of Mo and other elements near rice roots 198 5.3.7 Conclusions 209 6. Conclusions 210 7. References 212 " | |
| dc.language.iso | en | |
| dc.title | 土壤和水鐵礦對鉬酸根離子的吸持反應以及對小麥和水稻之鉬有效性的作用 | zh_TW |
| dc.title | The retention of molybdate by soils and ferrihydrite and its effects on the availability of molybdenum to wheat and rice | en |
| dc.date.schoolyear | 110-1 | |
| dc.description.degree | 博士 | |
| dc.contributor.author-orcid | 0000-0001-8656-8702 | |
| dc.contributor.oralexamcommittee | 李達源(Shih-Hong Chio),鄒裕民(Zi-Yi Chuang),許正一,莊愷瑋,劉雨庭 | |
| dc.subject.keyword | 土壤鉬有效性,X光吸收光譜,序列萃取,物種分析,吸附反應,脫附反應,無定型鐵氧化物, | zh_TW |
| dc.subject.keyword | Soil molybdenum availability,X-ray absorption spectroscopy (XAS),sequential extraction,chemical speciation,adsorption,desorption,amorphous iron oxide, | en |
| dc.relation.page | 231 | |
| dc.identifier.doi | 10.6342/NTU202200034 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2022-01-13 | |
| dc.contributor.author-college | 生物資源暨農學院 | zh_TW |
| dc.contributor.author-dept | 農業化學研究所 | zh_TW |
| 顯示於系所單位： | 農業化學系 | |
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