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完整後設資料紀錄
DC 欄位 | 值 | 語言 |
---|---|---|
dc.contributor.advisor | 陳奕君(I-Chun Cheng) | |
dc.contributor.author | Yu Cheng | en |
dc.contributor.author | 鄭宇 | zh_TW |
dc.date.accessioned | 2021-07-11T15:33:05Z | - |
dc.date.available | 2021-08-21 | |
dc.date.copyright | 2018-08-21 | |
dc.date.issued | 2018 | |
dc.date.submitted | 2018-08-15 | |
dc.identifier.citation | [1] 沈輝 and 曾祖勤, 太陽能光電技術. 五南圖書, 2008.
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dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78969 | - |
dc.description.abstract | 本研究以溶液式製程製備之奈米銀線薄膜取代真空蒸鍍銀薄膜作為對電極,成功開發出全溶液式製程之平面正規結構鈣鈦礦太陽能電池,並以短時間紫外光臭氧處理奈米銀線對電極面,改善界面特性,使此全溶液製程製備之元件特性與真空蒸鍍銀對電極之元件相當,極具應用潛力。研究中奈米銀線對電極分別以旋轉塗佈及以氮氣或空氣為載流氣體之噴閥式塗佈等溶液式製程製備。由掃描式電子顯微鏡分析可知,噴閥式塗佈之膜均勻性明顯優於旋轉塗佈。由電性分析發現,以空氣為載流氣體之噴閥式塗佈表現最佳,並且可藉由多次噴塗增加奈米銀線厚度,使鈣鈦礦太陽能電池的表現提升。接著,針對此鈣鈦礦太陽能電池之奈米銀線對電極面進行紫外光臭氧處理30、60、120與240 s。由掃描式電子顯微鏡分析可知,經短時間紫外光臭氧處理之奈米銀線/spiro-OMeTAD界面變得較為緊密;X光子能譜分析顯示,紫外光臭氧處理有助於spiro-OMeTAD表面的p型摻雜效應,使奈米銀線/spiro-OMeTAD之界面更為匹配;分流電阻分析說明短時間紫外光臭氧處理能大幅降低漏電流;以及電化學阻抗分析顯示,短時間紫外光臭氧處理有助於降低奈米銀線/spiro-OMeTAD界面傳輸阻抗。最後經電性分析發現最佳處理時間為60 s,元件的能量轉換效率達12.92 %,開路電壓為1.057 V,短路電流密度為18.35 mA/cm2,填充因子為66.6 %;相較於未經紫外光臭氧處理之能量轉換效率10.58 %,開路電壓1.054 V,短路電流密度19.23 mA/cm2與填充因子52.2 %,效率顯著提升22 %。 | zh_TW |
dc.description.abstract | In this study, we demonstrated all-solution-processed n-i-p type planar perovskite solar cells by replacing vacuum-deposited silver (Ag) with solution-processed silver nanowires (AgNWs) as top electrodes. Furthermore, an ultraviolet ozone (UVO) treatment was applied on the AgNWs counter electrode to improve the cell performance. The deposition of AgNWs was carried out by spin coating and spray coating with nitrogen or air as carrier gas. The scanning electron microscopic (SEM) images show that the uniformity of spray-coated AgNWs films is obviously superior to that of spin-coated ones. Cells with AgNWs counter electrode deposited by spray coating with air as carrier gas exhibit best performance. Next, an UVO treatment was performed on the AgNWs top electrode of the cell for 30, 60, 120 and 240 s. The SEM images show that the contact between spiro-OMeTAD and AgNWs becomes better after UVO treatment for a short duration. The X-ray photoelectron spectroscopy (XPS) analysis reveals that the UVO treatment contributes to p-type doping on the surface of spiro-OMeTAD, leading to a better energy level alignment between spiro-OMeTAD and AgNWs. Moreover, the shunt resistance analysis and electrochemical impedance spectroscopy (EIS) analysis indicate that UVO treatment for a short duration can reduce the cell’s leakage current and the charge transfer resistance at the spiro-OMeTAD/AgNWs interface, respectively. With an optimal UVO treatment duration of 60 s, the cell exhibits a photoelectric conversion efficiency (PCE) of 12.92 %, open circuit voltage (Voc) of 1.057 V, short circuit current density (Jsc) of 18.35 mA/cm2, and fill factor (F.F.) of 66.6 %. Compared with the counterpart without UVO treatment (PCE of 10.58 %, Voc of 1.054 V, Jsc of 19.23 mA/cm2 and F.F. of 52.2 %), the PCE is greatly improved 22 %. | en |
dc.description.provenance | Made available in DSpace on 2021-07-11T15:33:05Z (GMT). No. of bitstreams: 1 ntu-107-R05941064-1.pdf: 9619744 bytes, checksum: 6e8ccb0c99a84589434e5ed6e34c54ab (MD5) Previous issue date: 2018 | en |
dc.description.tableofcontents | 致謝 ii
中文摘要 iii Abstract iv 目錄 v 圖目錄 viii 表目錄 xii 第1章 緒論 1 1.1 前言 1 1.2 太陽能電池發展 1 1.3 研究動機 3 1.4 論文架構 4 第2章 文獻回顧 5 2.1 太陽能電池 5 2.1.1 太陽能電池原理 5 2.1.2 太陽能電池特性參數 7 2.2 鈣鈦礦太陽能電池 9 2.2.1 鈣鈦礦材料 9 2.2.2 鈣鈦礦太陽能電池發展 10 2.2.3 全溶液製程之各層探討 11 2.2.4 奈米銀線對電極於反結構鈣鈦礦太陽能電池之應用 12 2.2.5 奈米銀線對電極於正結構鈣鈦礦太陽能電池之應用 15 2.2.6 以奈米銀線為對電極之鈣鈦礦太陽能電池文獻統整 20 2.3 奈米銀線後處理 21 2.3.1 熱、壓處理 21 2.3.2 光吸收處理 23 第3章 研究方法 25 3.1 製程儀器 25 3.1.1 氮氣手套箱 25 3.1.2 旋轉塗佈系統 25 3.1.3 噴閥式塗佈系統 26 3.1.4 紫外光臭氧系統 28 3.2 鈣鈦礦太陽能電池製作流程 29 3.2.1 基材蝕刻、切割與清洗 31 3.2.2 電子傳輸層調配、塗佈與燒結 32 3.2.3 鈣鈦礦調配、塗佈與燒結 33 3.2.4 電洞傳輸層調配與塗佈 34 3.2.5 奈米銀線電極沉積與後處理 35 3.3 量測分析 36 3.3.1 掃描式電子顯微鏡 36 3.3.2 四點探針 37 3.3.3 紫外光-可見光光譜儀 38 3.3.4 X光子能譜儀 40 3.4 太陽能電池元件之特性分析 41 3.4.1 太陽光模擬系統 41 3.4.2 分流電阻分析 42 3.4.3 電化學阻抗分析 43 第4章 實驗結果與討論 46 4.1 奈米銀線全溶液製程之探討 46 4.1.1 旋轉塗佈 46 4.1.2 噴閥式塗佈(氮氣) 51 4.1.3 噴閥式塗佈(空氣) 54 4.1.4 噴塗各次數(空氣)之元件橫截面 57 4.1.5 噴塗各次數(空氣)之穿透與反射頻譜 58 4.2 紫外光臭氧處理之薄膜分析 60 4.2.1 掃描式電子顯微鏡分析 60 4.2.2 奈米銀線片電阻值分析 63 4.2.3 奈米銀線紫外光-可見光頻譜分析 65 4.2.4 奈米銀線/spiro-OMeTAD之X光子能譜分析 67 4.3 紫外光臭氧處理之太陽能電池特性 73 4.3.1 電性分析 73 4.3.2 前處理spiro-OMeTAD之效應 77 4.3.3 分流電阻分析 78 4.3.4 電化學阻抗分析 79 第5章 結論與未來展望 82 附錄A 高真空蒸鍍製程之銀對電極 84 附錄B 背板覆蓋法 85 附錄C 其他後處理之應用探討 87 參考文獻 93 | |
dc.language.iso | zh-TW | |
dc.title | 奈米銀線對電極於全溶液式製程鈣鈦礦太陽能電池之應用 | zh_TW |
dc.title | All Solution Processed Perovskite Solar Cells with Silver Nanowire Top Electrodes | en |
dc.type | Thesis | |
dc.date.schoolyear | 106-2 | |
dc.description.degree | 碩士 | |
dc.contributor.oralexamcommittee | 陳建彰(Jian-Zhang Chen),吳肇欣(Chao-Hsin Wu),廖英志(Ying-Chih Liao) | |
dc.subject.keyword | 鈣鈦礦太陽能電池,奈米銀線,噴閥式塗佈,紫外光臭氧處理, | zh_TW |
dc.subject.keyword | Perovskite solar cells,silver nanowires,spray coating,ultraviolet ozone, | en |
dc.relation.page | 100 | |
dc.identifier.doi | 10.6342/NTU201803680 | |
dc.rights.note | 有償授權 | |
dc.date.accepted | 2018-08-16 | |
dc.contributor.author-college | 電機資訊學院 | zh_TW |
dc.contributor.author-dept | 光電工程學研究所 | zh_TW |
顯示於系所單位: | 光電工程學研究所 |
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