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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳建彰 | zh_TW |
| dc.contributor.advisor | Jian-Zhang Chen | en |
| dc.contributor.author | 鄭亦辰 | zh_TW |
| dc.contributor.author | Yi-Chen Cheng | en |
| dc.date.accessioned | 2021-07-11T15:15:19Z | - |
| dc.date.available | 2024-07-31 | - |
| dc.date.copyright | 2019-07-31 | - |
| dc.date.issued | 2019 | - |
| dc.date.submitted | 2002-01-01 | - |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78731 | - |
| dc.description.abstract | 本研究主要是使用氮氣電弧式常壓噴射電漿，及氬氣介電質放電噴射電漿對碳纖維布進行改質，並將還原氧化石墨烯-聚苯胺-殼聚醣奈米複合材料，網印在處理過之碳纖維布上，作為軟性超級電容電極。氮氣電弧式常壓電漿處理時的基板溫度峰值在約500°C，而氬氣介電質放電噴射電漿處理時基板溫度約在40°C。在碳纖維布經電漿改質前後方面，由電子顯微鏡 (SEM) 與原子力顯微鏡 (AFM) 的觀察，發現處理過後之碳纖維布表面皆變粗糙，由水接觸角 (WCA) 發現改質後的碳纖維布皆呈現親水性，但兩者電漿處理後的碳纖維布在空氣中貯存則有相當不同的反應。氮氣電弧式常壓電漿所處理之碳布親水性可以維持20週以上，但氬氣介電質放電噴射電漿處理之碳布親水性在12小時後開始往疏水轉變。由X-射線繞射儀 (XRD) 與拉曼光譜儀 (Raman spectrometer) 發現處理後之碳纖維布皆無結構上之明顯改變，由電子微探儀 (EPMA) 與X-射線光電子能譜儀 (XPS)，發現處理過後之碳纖維布皆有氧摻雜的作用，而氮氣電弧式電漿則有強烈之氮摻雜反應。在超級電容應用方面，發現兩種常壓電漿皆有效地提升超級電容之電容值，並以電化學阻抗頻譜分析 (EIS) 結果可得知，改質後的碳纖維布皆具有較小之電荷轉移電阻，且具有較高之電雙層電容與法拉第電容。從此研究證實了電漿之高反應性粒子具有碳纖維布表面改質功能，增加親水官能基於碳纖維，增加碳布的親水性，進而提升超級電容的性能。溫度則具有協同的碳布改質效果，因此電弧式常壓噴射電漿 (氣體溫度較高) 所處理之碳布在空氣中儲存能維持較長時間之親水性。 | zh_TW |
| dc.description.abstract | This study investigates the carbon cloth modified by nitrogen arc atmospheric pressure plasma jet (APPJ) and Ar dielectric barrier discharge jet (DBD jet). The carbon cloth is then used as the collecting electrode for reduced graphene oxide (rGO)-polyaniline (PANI)-chitosan (CS) nanocomposite flexible supercapacitor. The peak temperature of substrate under nitrogen arc APPJ processing is ~500°C whereas that under Ar DBD jet is ~40°C. The roughness of carbon fibers increases upon plasma treatment, as evidenced by scanning electron microscopy (SEM) and atomic force microscopy (AFM).
Water contact angle measurements indicate the improvement in the hydrophilicity of carbon cloth after nitrogen arc APPJ and Ar DBD jet treatments. However, the hydrophilicity to hydrophobicity recovering rate is very different with these two types of plasma treatment. Upon storage in normal environment, carbon cloth treated by nitrogen arc APPJ can maintain the hydrophilicity for more than 20 weeks, however, that treated by Ar DBD jet starts to recover to hydrophobicity after 12 h. X-ray diffraction (XRD) and the Raman spectrometry analyses show no significant structural alternation upon plasma treatment. X-ray photoelectron spectroscopy (XPS) and electron probe microanalyzer (EPMA) indicates the introduction of oxygen- functional groups to the carbon fibers of the carbon cloth by both nitrogen arc APPJ and Ar DBD jet treatments. Moreover, nitrogen arc APPJ treatment also introduce nitrogen doping on carbon fibers. Both nitrogen arc APPJ and Ar DBD jet treatments on carbon cloth can improve the capacitance value of the supercapacitor. Electrochemical impedance spectroscopy (EIS) show lower charge transfer resistance upon both plasma treatments. Our results suggest that reactive plasma species can modify the surface properties of carbon cloth by introduction oxygen-containing functional groups and increase the surface roughness. Temperature has additional effect on surface modification of carbon fibers such that carbon cloth treated by nitrogen arc APPJ can maintain the hydrophilicity for a much longer period. | en |
| dc.description.provenance | Made available in DSpace on 2021-07-11T15:15:19Z (GMT). No. of bitstreams: 1 ntu-108-R06543006-1.pdf: 15325683 bytes, checksum: 6eaf187b03f1cc11f7c1dad1fdd2678a (MD5) Previous issue date: 2019 | en |
| dc.description.tableofcontents | 致謝 I
中文摘要 II ABSTRACT III 總目錄 V 圖目錄 X 表目錄 XVII 第一章 緒論 1 1.1前言 1 1.2研究動機 3 1.3論文架構 4 第二章 實驗理論及文獻回顧 5 2.1常壓電漿 (Atmospheric pressure plasma, APP) 5 2.1.1電漿簡介 [29, 30] 5 2.1.2常壓電漿工作原理與種類 11 2.1.3常壓電漿種類與應用 [42] 13 2.2石墨烯 (Graphene)之特性 17 2.2.1石墨烯之材料性質與結構簡介 [63] 17 2.2.2石墨烯之製備方式 18 2.3聚苯胺 (Polyaniline)之特性 22 2.3.1聚苯胺之材料性質與結構簡介 22 2.3.2聚苯胺之製備方式 24 2.4超級電容 (Supercapacitor)之簡介 25 2.4.1超級電容之特性 [74] 25 2.4.2超級電容之儲能機制 [11, 95] 33 2.4.3商業超級電容 39 第三章 實驗方法及流程 40 3.1實驗藥品及儀器 40 3.2實驗規劃 44 3.3實驗流程 45 3.3.1玻璃樣本瓶與無鹼玻璃之清洗 45 3.3.2殼聚醣膠體溶液製備 46 3.3.3還原氧化石墨烯-聚苯胺-殼聚醣漿料製備 47 3.3.4還原氧化石墨烯-聚苯胺-殼聚醣電極之製備 47 3.3.5凝膠態電解液製備 50 3.3.6液態電解液及凝膠態電解液超級電容之製備 50 3.3.7電性量測試片之製作 51 3.4製程儀器與原理 52 3.4.1網版印刷機 (Screen print machine) 52 3.4.2常壓噴射電漿 (Atmospheric pressure plasma jet) 53 3.4.3電子束蒸鍍機 (E-beam evaporation) 56 3.5量測儀器與原理 57 3.5.1原子力顯微鏡 (Atomic force microscopy) [128, 129] 57 3.5.2掃描式電子顯微鏡 (Scanning electron microscopy) [133, 134] 60 3.5.3光放射光譜儀 (Optical emission spectroscopy) [138, 139] 62 3.5.4接觸角儀 (Contact angle instrument) [140] 64 3.5.5 X光繞射儀 (X-ray diffraction) [142, 143] 66 3.5.6拉曼光譜儀 (Raman spectrometer) [147] 68 3.5.7 X射線光電子能譜儀 (X-ray photoelectron spectroscopy) [150] 69 3.5.8電子微探針試驗儀 (Electron probe microanalyzer，EPMA) [152, 153] 71 3.5.9熱重分析儀 (Thermogavimetric analysis) [155] 73 3.5.10紫外光-可見光光譜儀 (UV-Visible spectrometer) [156] 73 3.5.11電性量測 (Electrical measurement) 75 3.5.12電化學量測 (Electrochemical measurement) [158] 75 3.6 實驗流程示意圖 80 第四章 實驗結果與討論 81 4.1常壓噴射電漿掃描處理碳纖維布之溫度變化圖 81 4.1.1 氮氣電弧式常壓噴射電漿掃描製程之溫度變化圖 81 4.1.2 氬氣介電質放電常壓噴射電漿掃描製程之溫度變化圖 82 4.2常壓噴射電漿掃描處理碳纖維布之光發射光譜圖 84 4.2.1 氮氣電弧式常壓噴射電漿之光發射光譜圖 84 4.2.2 氬氣介電質放電噴射電漿之光發射光譜圖 90 4.3常壓噴射電漿掃描掃描處理碳纖維布之溫度模擬 95 4.4常壓噴射電漿掃描處理碳纖維布之表面型態 99 4.5常壓噴射電漿掃描處理碳纖維布之表面親疏水特性分析 104 4.6常壓噴射電漿掃描處理碳纖維布之晶體結構分析 106 4.7常壓噴射電漿掃描處理碳纖維布之拉曼光譜分析 108 4.8常壓噴射電漿掃描處理碳纖維布之表面化學型態分析 109 4.8.1 氮氣電弧式常壓噴射電漿之表面化學型態分析 109 4.8.2 氬氣介電質放電常壓噴射電漿之表面化學型態分析 112 4.9常壓噴射電漿掃描處理碳纖維布之成分分析 115 4.10常壓噴射電漿掃描處理碳纖維布之電化學分析 116 4.10.1常壓噴射電漿掃描處理碳纖維布之循環伏安法量測 116 4.10.2常壓噴射電漿掃描處理碳纖維布之電化學阻抗分析 118 4.11還原氧化石墨烯-聚苯胺-殼聚醣之表面型態與親疏水特性分析 119 4.12還原氧化石墨烯-聚苯胺-殼聚醣之熱重、光學穿透與電性分析 123 4.13凝膠態電解液軟性超級電容之電化學分析 127 4.13.1還原氧化石墨烯-聚苯胺-殼聚醣電極之循環伏安法量測 127 4.13.2還原氧化石墨烯-聚苯胺-殼聚醣凝膠態電解液超級電容之恆電流充放電量測 130 4.14液態電解質超級電容之電化學分析 132 4.14.1還原氧化石墨烯-聚苯胺-殼聚醣電極之循環伏安法量測 132 4.14.2還原氧化石墨烯-聚苯胺-殼聚醣電極液態電解液超級電容之恆電流充放電量測 134 4.14.3還原氧化石墨烯-聚苯胺-殼聚醣電極之電化學阻抗分析 137 4.15凝膠態電解液超級電容LED實用性測試 139 第五章 結論與未來展望 140 附錄 實驗A 表面擴散式介電質放電常壓電漿處理還原氧化石墨烯-聚苯胺超級電容之應用 142 A.1前言 142 A.2實驗方法 143 A.2.1實驗儀器架設 143 A.2.2實驗步驟 144 A.3實驗結果與討論 145 A.3.1表面擴散式介電質放電電漿溫度變化圖 145 A.3.2表面擴散式介電質放電電漿處理電極之水接觸角變化 146 A.3.3凝膠態電解質超級電容之電化學分析 147 附錄 實驗B 氮氣電弧式常壓噴射電漿處理發泡鎳基板之材料分析 149 B.1前言 149 B.2實驗方法 150 B.3實驗結果與討論 150 B.3.1發泡鎳之水接觸角變化 150 B.3.2發泡鎳之SEM影像圖 151 B.3.3發泡鎳之XPS量測分析 152 B.3.4發泡鎳之EPMA量測結果 155 B.3.5發泡鎳之XRD量測結果 156 附錄 實驗C 氦氣介電質放電常壓噴射電漿之溫度與光譜分析 157 C.1實驗結果與討論 157 C.1.1氦氣介電質放電常壓噴射電漿溫度變化圖 157 C.1.2氦氣介電質放電常壓噴射電漿之光發射光譜圖 158 C.1.3氦氣介電質放電常壓噴射電漿溫度模擬 159 參考文獻 160 | - |
| dc.language.iso | zh_TW | - |
| dc.title | 介電質放電及電弧式常壓噴射電漿掃描製成於氧化還原石墨烯-聚苯胺-殼聚醣超級電容之應用 | zh_TW |
| dc.title | Application of scan-mode dielectric barrier discharge and arc atmospheric pressure plasma jet (APPJ) processes to reduce graphene oxide (rGO)-polyaniline (PANI)-chitosan (CS) supercapacitors | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 107-2 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.oralexamcommittee | 陳奕君;徐振哲;王孟菊 | zh_TW |
| dc.contributor.oralexamcommittee | I-Chun Cheng;Cheng-Che Hsu;Meng-Jiy Wang | en |
| dc.subject.keyword | 常壓噴射電漿,介電質放電,介電質放電噴射電漿,大氣電漿,碳纖維布,還原氧化石墨烯,聚苯胺,殼聚醣,奈米複合材料,表面改質,軟性超級電容, | zh_TW |
| dc.subject.keyword | atmospheric pressure plasma jet,dielectric barrier discharge,dielectric barrier discharge jet,atmospheric pressure plasma,carbon cloth,reduced graphene oxide,polyaniline,chitosan,nanocomposite,surface modification,flexible supercapacitor, | en |
| dc.relation.page | 178 | - |
| dc.identifier.doi | 10.6342/NTU201901917 | - |
| dc.rights.note | 未授權 | - |
| dc.date.accepted | 2019-07-26 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 應用力學研究所 | - |
| dc.date.embargo-lift | 2024-07-31 | - |
| 顯示於系所單位： | 應用力學研究所 | |
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