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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78365完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳建彰(Jian-Zhang Chen) | |
| dc.contributor.author | Pei-Yu Cheng | en |
| dc.contributor.author | 鄭珮妤 | zh_TW |
| dc.date.accessioned | 2021-07-11T14:53:15Z | - |
| dc.date.available | 2024-07-22 | |
| dc.date.copyright | 2020-07-31 | |
| dc.date.issued | 2020 | |
| dc.date.submitted | 2020-07-27 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78365 | - |
| dc.description.abstract | 本研究分為兩部分。第一部分為使用氮氣直流脈衝常壓噴射電漿(DC-pulse atmospheric-pressure plasma jet)與十八烷基三氯矽烷自組裝分子(octadecyltrichlorosilane self-assembling monolayers, OTS SAM)對於鐵鈷鎳鉻中熵合金(FeCoNiCr medium-entropy alloy, FeCoNiCr MEA)進行表面改質，並進一步探討其對於抗腐蝕性質的影響。根據水接觸角實驗，常壓噴射電漿、十八烷基三氯矽烷自組裝分子或兩者都使用可以提升鐵鈷鎳鉻中熵合金的疏水性。透過極化曲線與電化學組抗分析，(Electrochemical Impedance Spectroscopy, EIS)，經過大氣電漿處理的鐵鈷鎳鉻中熵合金有最佳的抗腐蝕性。而在X-射線光電子光譜儀(X-ray photoelectron spectroscopy, XPS)的實驗結果中，常壓噴射電漿氧化了所有鐵鈷鎳鉻中熵合金中的金屬元素。然而，第二部分為使用大氣介電質放電噴射電漿(atmospheric-pressure dielectric-barrier-discharge jet, DBDjet)與十八烷基三氯矽烷自組裝分子以紙為基板製作紙基微流道，並使用水接觸角、X-射線光電子光譜儀(XPS)和表面輪廓儀等實驗探討其機制。在這個部分中，成功的蝕刻出一毫米寬的微流道。且兩種不同的液體可以在微流道中被傳輸或混合。 | zh_TW |
| dc.description.abstract | This study demonstrates two applications of atmospheric-pressure plasma jet. The first one is surface modification of FeCoNiCr medium-entropy alloy (MEA) using Octadecyltrichlorosilane (OTS) and DC-pulse atmospheric-pressure plasma jet (APPJ). Corrosion properties was investigated. According to contact angle measurements, engaging OTS-coating treatment, APPJ treatment, or the combination of both treatments (OTS-coated APPJ-treated) can improve the hydrophobicity of the FeCoNiCr MEA. The APPJ-treated FeCoNiCr MEA exhibits the best anti-corrosion properties, evidenced by potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) tests. APPJ treatment oxidizes all alloying elements of MEA, as revealed by X-ray photoelectron spectroscopy (XPS). The second part is the hydrophilic patterning of octadecyltrichlorosilane (OTS)-coated paper via atmospheric-pressure dielectric-barrier-discharge jet (DBDjet).Water contact angle measurement, X-ray photoelectron spectroscopy (XPS), and surface profilerwere used to characterize the DBDjet patterned OTS-coated paper. 1-mm-wide hydrophilic microstripes are patterned successfully, and liquids are successfully demonstrated to be transported and mixed in the hydrophilic microstripes. | en |
| dc.description.provenance | Made available in DSpace on 2021-07-11T14:53:15Z (GMT). No. of bitstreams: 1 U0001-2207202015113600.pdf: 7967904 bytes, checksum: 1fcacf87c5b8e5e128f0045af31c61e3 (MD5) Previous issue date: 2020 | en |
| dc.description.tableofcontents | 致謝 I 中文摘要 II ABSTRACT III 總目錄 IV 圖目錄 VII 表目錄 XII 第一章 緒論 1 1.1 前言 1 1.2 研究動機 1 1.3 論文大綱 2 第二章 基本原理與文獻回顧 3 2.1 中熵合金 3 2.1.1. 簡介與定義 3 2.1.2. 性質 4 2.2 紙基微流體裝置製程技術 6 2.2.1 光蝕刻法(Photolithography) 6 2.2.2 塗蠟法(Wax Patterning) 7 2.2.3 噴墨列印法(Inkjet Printing or Etching) 7 2.2.4 柔版印刷法(Flexographic Printing) 7 2.2.5 切割成型法(Paper Cutting and Shaping) 8 2.2.6 化學改質法(Chemical Modification of Paper) 8 2.2.7 其他製程方法 9 2.3 大氣常壓電漿 9 2.3.1 工作原理 10 2.3.2 優勢與應用 13 第三章 實驗方法與流程 14 3.1 實驗材料與測量儀器 14 3.2 實驗規劃 16 3.3 實驗流程 17 3.3.1 中熵合金製程 17 3.3.2 微流道製程 20 3.4 測量儀器與原理 22 3.4.1 光放射光譜儀(Optical emission spectroscopy, OES) 22 3.4.2 高解析場發射鎗掃描式電子顯微鏡 (Scanning electron microscope, SEM) 23 3.4.3 X-射線光電子光譜儀(X-ray photoelectron spectroscopy, XPS) 24 3.4.4 X射線繞射儀(X-ray Diffractometer, XRD) 25 3.4.5 電化學分析 26 第四章 實驗結果與討論 30 4.1 氮氣直流脈衝常壓噴射電漿與十八烷基三氯矽烷自組裝分子對於中熵合金的抗腐蝕性質影響 30 4.1.1 水接觸角 30 4.1.2 極化曲線 31 4.1.3 EIS 33 4.1.4 XPS 36 4.1.5 SEM EDS 41 4.1.6 XRD 54 4.2 大氣介電質放電噴射電漿與十八烷基三氯矽烷自組裝分子以紙為基板製作紙基微流體裝置 55 4.2.1 DBDjet對於OTS-treated paper圖案化之成果 55 4.2.2 水接觸角 56 4.2.3 表面粗糙度分析 58 4.2.4 OES 60 4.2.5 XPS 62 4.2.6 SEM 70 第五章 結論與未來展望 73 附錄I：MEA的極化曲線量測四次的詳細圖 74 I.I 極化曲線實驗參數 74 I.II 極化曲線實驗結果 74 附錄II：MEA的EIS量測之詳細圖表 76 II.I EIS實驗參數 76 II.II EIS實驗結果 76 附錄III：MEA的OES量測結果 81 附錄IV：MEA的XPS之縱深量測結果 83 附錄V：DBDJET處理紙張的XPS AU4F之量測結果 85 附錄VI：表面粗糙度分析的MATLAB程式碼 87 參考文獻 89 | |
| dc.language.iso | zh-TW | |
| dc.title | 使用十八烷基三氯矽烷自組裝分子與大氣常壓噴射電漿進行FeCoNiCr中熵合金與纖維素紙的表面改質 | zh_TW |
| dc.title | Surface modification of FeCoNiCr medium-entropy alloy and chromatography paper using octadecyltrichlorosilane self-assembling monolayers (SAM) and atmospheric-pressure plasma jet | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 108-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.author-orcid | 0000-0003-3647-9212 | |
| dc.contributor.advisor-orcid | 陳建彰(0000-0002-1071-2234) | |
| dc.contributor.oralexamcommittee | 陳奕君(I-Chun Cheng),李岳聯(Yueh-Lien Lee),徐振哲(Cheng-Che Hsu) | |
| dc.contributor.oralexamcommittee-orcid | 陳奕君(0000-0003-2209-3298),李岳聯(0000-0001-6620-2586),徐振哲(0000-0002-8366-3592) | |
| dc.subject.keyword | 大氣常壓噴射電漿,表面處理,疏水性,中熵合金,氧化,十八烷基三氯矽烷自組裝分子,介電質放電,微流體裝置,紙基生物晶片, | zh_TW |
| dc.subject.keyword | Atmospheric-pressure plasma jet,dielectric barrier discharge,Octadecyltrichlorosilane,Surface treatment,Hydrophobicity,Medium entropy alloy,Oxidation,microfluidic device,paper-based biochip, | en |
| dc.relation.page | 98 | |
| dc.identifier.doi | 10.6342/NTU202001738 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2020-07-27 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 應用力學研究所 | zh_TW |
| dc.date.embargo-lift | 2024-07-22 | - |
| 顯示於系所單位： | 應用力學研究所 | |
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