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請用此 Handle URI 來引用此文件: http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/63693
完整後設資料紀錄
DC 欄位值語言
dc.contributor.advisor廖運炫
dc.contributor.authorWei-Ru Lien
dc.contributor.author李韋儒zh_TW
dc.date.accessioned2021-06-16T17:16:34Z-
dc.date.available2016-08-20
dc.date.copyright2012-08-20
dc.date.issued2012
dc.date.submitted2012-08-17
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dc.identifier.urihttp://tdr.lib.ntu.edu.tw/jspui/handle/123456789/63693-
dc.description.abstract本研究探討正方晶形穩態氧化鋯(TZP)的表面處理方法,使用噴砂法、蝕刻法與複合式的噴砂加酸蝕法探討處理後的表面狀況。噴砂法使用人造鑽石顆粒當砂材並與氧化鋁顆粒及氧化鋯顆粒比較;蝕刻法使用到多種蝕刻液包含硝酸、氫氟酸、硫酸、鹽酸和氫氧化鉀。實驗發現採用鑽石顆粒能有效增加TZP試片表面粗糙度與表面積,人造鑽石噴砂結果的表面粗糙度參數對於壓力或顆粒粒徑有正相關性,主要原因為人造鑽石顆粒的刃邊形狀相同,採用人造鑽石顆粒對於噴砂結果的表面狀況較容易掌握,因此可以經由調整不同壓力與粒徑製造出不同類型的粗糙表面;硝酸與氫氟酸的混合水溶液,能夠在TZP試片表面上製造微小的顆粒狀結構,大幅提高表面積;複合式以大粒徑人工鑽石噴砂後加酸蝕的表面處理方法,酸蝕處理能保持噴砂後表面的粗糙水準,實驗發現能使TZP表面積Sdr數值大幅提升達1.80。元素分析結果顯示,噴砂處理後或經過適當酸蝕的TZP表面上只有微量的表面殘留物。zh_TW
dc.description.abstractThis thesis studies the tetragonal zirconia polycrystals (TZP) surface conditions after various surface treatment methods including sandblasting, etching, and the hybrid treatment of sandblasting followed by etching. The synthetic diamond particles were used in sandblasting and the results were compared with those obtained by using particles of alumina and zirconia. The aqueous solutions used in etching were nitric acid, hydrofluoric acid, sulfuric acid, hydrochloric acid and potassium hydroxide. It is found that synthetic diamond sand can effectively increase the surface roughness and the surface area ratio of TZP specimen. The variations of surface roughness parameters have positive correlation with air pressure and particle size when synthetic diamonds are used. The main reason is due to the consistent cutting edge of the particles. The mixed aqueous solution of nitric acid and hydrofluoric acid can generate the tiny granular structure on the specimen surface, and effectively increase the surface area. The rough surface after sandblasting can be maintained after acid etching treatments. The surface area ratio Sdr value increases to 1.80 by the hybrid treatment. The EDX analysis shows that there are just slight surface residues of the TZP surface after sandblasting or after appropriate etching treatments.en
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en
dc.description.tableofcontents謝誌 3
摘要 I
Abstract II
目錄 III
圖目錄 VI
表目錄 XI
第一章 相關理論 1
1.1 研究背景與動機 1
1.2 文獻回顧 2
1.2.1 牙科植體發展 2
1.2.2 鈦金屬人工牙根表面處理 5
1.2.3 鈦金屬人工牙根骨整合影響因子探討 14
1.2.4 氧化鋯陶瓷材料表面處理 16
1.3 研究目的 24
1.4 本文架構 25
第二章 相關理論 26
2.1 氧化鋯陶瓷材料 26
2.1.1 氧化鋯的種類 26
2.1.2 氧化鋯材料之機械性質 28
2.2 噴砂理論探討 31
2.3 氧化鋯酸蝕探討 34
2.4 表面粗糙度的表示法 35
2.5 鑽石 37
第三章 實驗設備與規劃 39
3.1 實驗設備與儀器 39
3.2 實驗規劃 47
3.3 噴砂實驗裝置 50
3.4 表面粗糙度參數的量測 52
第四章 實驗結果與討論 54
4.1 噴砂時間設定實驗 54
4.1.1 未經表面處理的試片 54
4.1.2 適宜的噴砂時間 57
4.2 三種砂材不同粒徑噴砂實驗 62
4.2.1 氧化鋯顆粒 62
4.2.2 白色氧化鋁顆粒 64
4.2.3 人造鑽石顆粒 67
4.2.4 噴砂製造不同TZP表面 72
4.3 氧化鋯蝕刻實驗 74
4.4 噴砂後加酸蝕表面處理實驗 78
4.5 表面元素分析結果 81
4.5.1 燒結後原始表面 81
4.5.2 氧化鋁顆粒噴砂後的表面 82
4.5.3 人造鑽石噴砂後的表面 83
4.5.4 NHF45蝕刻45分鐘後的表面 84
4.5.5 NHF45蝕刻60分鐘後的表面 85
第五章 結論與未來展望 87
5.1 結論 87
5.2 未來展望 88
參考文獻 89
dc.language.isozh-TW
dc.subject表面粗糙度zh_TW
dc.subject酸蝕表面處理zh_TW
dc.subject噴砂表面處理zh_TW
dc.subject正方晶形穩態氧化鋯zh_TW
dc.subject氧化鋯牙根zh_TW
dc.subjectsurface roughnessen
dc.subjectetching surface treatmenten
dc.subjectsandblasting surface treatmenten
dc.subjectTZPen
dc.subjectzirconia dental implanten
dc.title氧化鋯陶瓷人工牙根材料表面處理研究zh_TW
dc.titleA Study of Surface Treatments of Zirconia Dental Implanten
dc.typeThesis
dc.date.schoolyear100-2
dc.description.degree碩士
dc.contributor.oralexamcommittee羅勝益,趙崇禮
dc.subject.keyword氧化鋯牙根,正方晶形穩態氧化鋯,噴砂表面處理,酸蝕表面處理,表面粗糙度,zh_TW
dc.subject.keywordzirconia dental implant,TZP,sandblasting surface treatment,etching surface treatment,surface roughness,en
dc.relation.page97
dc.rights.note有償授權
dc.date.accepted2012-08-18
dc.contributor.author-college工學院zh_TW
dc.contributor.author-dept機械工程學研究所zh_TW
顯示於系所單位:機械工程學系

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