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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 張尊國(Tsun-Kuo Chang) | |
| dc.contributor.author | Ying-Fang Chang | en |
| dc.contributor.author | 張映昉 | zh_TW |
| dc.date.accessioned | 2021-06-16T16:44:07Z | - |
| dc.date.available | 2013-08-22 | |
| dc.date.copyright | 2012-08-22 | |
| dc.date.issued | 2012 | |
| dc.date.submitted | 2012-08-21 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/63473 | - |
| dc.description.abstract | 油品含鉛一直被視為人體鉛暴露之主要途徑之一，雖然無鉛汽油之使用後已大幅降低此風險，但依然未能完全排除。本研究建立油品之穩定性鉛同位素分析技術，分析臺灣地區不同廠牌之市售油品穩定性鉛同位素特徵值，並將之與環境介質鉛同位素特徵加以比對研析。採集樣品包含中油公司和台塑公司所販售之92無鉛汽油、95無鉛汽油、98無鉛汽油及超級柴油，以多頻道感應耦合電漿質譜儀（MC-ICP-MS）進行高精度之油品鉛同位素分析，測定208Pb/207Pb、208Pb/206Pb、207Pb/206Pb、206Pb/ 204Pb等4種比值；油品鉛含量另以磁場式感應耦合電漿質譜儀（ICP-SF-MS）進行測定。
研究結果發現，臺灣油品之鉛濃度為5 ng g-1至50 ng g-1之間。各鉛同位素比值利用T檢定（T-test）分析數據得知，同一廠牌不同加油站之油品鉛同位素比值特徵與兩種廠牌市售各油品類別間之鉛同位素比值特徵皆無顯著差異。另以T檢定檢視中油公司及台塑公司之油品鉛同位素比值，結果顯示在不考慮油品類別之情況下，兩廠牌的鉛同位素特徵具鑑別度。以銷售比例及加油站數比例加權，估算整體油品各鉛同位素比值，其中（208Pb/207Pb、207Pb/206Pb）分別為2.4269、0.8710，與臺北地區氣膠之鉛同位素比值特徵2.4270、0.8720極為相似，顯示臺北地區氣膠中鉛來源受地域性之油品影響。 | zh_TW |
| dc.description.abstract | Leaded gasoline has been regarded as one of the major source of human lead exposure. Nowadays, people reduce this risk by using unleaded gasoline, but we can’t eliminate them all. This study established a lead isotope analyze technique of gasoline. We analyzed and compared the characteristics of stable lead isotopes between gasoline of different brands and environmental media. Set 92 unleaded gasoline, 95 unleaded gasoline, 98 unleaded gasoline, and diesel fuel samples are collected from the Chinese Petroleum Corporation （CPC）and Formosa Plastics Corporation（FPCC）. High-precision lead isotope ratios of gasoline samples were obtained by using Multi Collector-Inductively Coupled plasma Mass Spectrometry （MC-ICP-MS）. Four lead isotope ratios： 208Pb/207Pb, 208Pb/206Pb, 207Pb/206Pb, and 206Pb/204Pb, were determined. Meanwhile, lead concentrations in gasoline were measured by using Inductively Coupled Plasma Sector Field Mass Spectrometer （ICP-SF-MS）.
Results reveal the lead concentrations in gasoline ranged from 5 ng g-1 to 50 ng g-1. The lead isotope ratio data analysis via T-test shows that the ratio characteristics have non-significant difference between different sites of gas station under the same brand. Furthermore, there is significant difference between two brands of gas products on its lead isotopic ratios. To estimate the lead isotope ratios of overall vehicle exhaust based on sales ratio and gas stations number, the lead isotope ratios （208Pb/207Pb and 207Pb/206Pb） are 2.4269 and 0.8710, it’s very similar to Taipei area aerosols lead isotope ratios of 2.4270 and 0.8720, respectively. Represent that the lead in Taipei area aerosols mainly from local gasoline combustion. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-16T16:44:07Z (GMT). No. of bitstreams: 1 ntu-101-R99622017-1.pdf: 5922481 bytes, checksum: 31c1d1942b74f50d46100900ec97e43f (MD5) Previous issue date: 2012 | en |
| dc.description.tableofcontents | 口試委員會審定書...............................................................................................I
誌謝.......................................................................................................................II 中文摘要..............................................................................................................IV 英文摘要...............................................................................................................V 目錄......................................................................................................................VI 圖目錄..................................................................................................................IX 表目錄..................................................................................................................XI 公式目錄...........................................................................................................XIII 第一章 前言........................................................................................................1 1.1研究動機.................................................................................................1 1.2研究目的.................................................................................................2 1.3研究架構.................................................................................................2 第二章 文獻回顧..................................................................................................4 2.1鉛之基本介紹.........................................................................................4 2.2人為鉛量之排放.....................................................................................6 2.3臺灣及國際油品資訊概述.....................................................................7 2.4油品污染現況及來源鑑識方式.............................................................8 2.5鉛同位素鑑識應用................................................................................10 2.5.1鉛同位素之環境鑑識應用起源與案例.......................................10 2.5.2氣膠中鉛來源之鉛同位素示蹤...................................................11 2.6油品鉛同位素鑑識技術........................................................................14 第三章 研究材料與方法..................................................................................16 3.1實驗材料................................................................................................16 3.2研究規劃................................................................................................19 3.3實驗試劑與器皿....................................................................................23 3.3.1實驗試劑......................................................................................23 3.3.2實驗器皿......................................................................................24 3.4採樣作業方法........................................................................................25 3.5樣本前處理............................................................................................28 3.5.1樣本乾燥......................................................................................28 3.5.2樣本消化......................................................................................29 3.6油品鉛同位素分離程序........................................................................31 3.7鉛濃度檢測............................................................................................32 3.7.1檢量線配製...................................................................................32 3.7.2儀器介紹與參數設定...................................................................34 3.8 鉛同位素檢測.......................................................................................35 3.8.1儀器介紹.......................................................................................35 3.8.2參數設定.......................................................................................38 3.9品保品管程序........................................................................................39 3.9.1數據品保目標...............................................................................39 3.9.2樣本管制.......................................................................................39 3.10統計分析..............................................................................................41 第四章 結果與討論..........................................................................................43 4.1油品盛裝容器材質與保存天數對鉛同位素比值之影響....................43 4.2油品鉛濃度測定....................................................................................47 4.2.1油品鉛濃度測定品保品管程序...................................................47 4.2.2臺灣市售油品之鉛濃度...............................................................48 4.3油品鉛同位素比值測定........................................................................49 4.3.1油品鉛同位素比值測定品保品管程序.......................................49 4.3.2油品鉛同位素比值測定...............................................................51 4.4油品鉛濃度與鉛同位素比值特徵之關聯性比較................................58 4.5同一廠牌不同場址加油站之油品鉛同位素比值特徵比較...............59 4.6中油公司及台塑公司油品之鉛同位素比值特徵比較........................62 4.7市售油品間相互之鉛同位素比值特徵比較........................................66 4.8臺灣油品與國際油品之鉛同位素比值特徵比較................................70 4.9油品鉛同位素比值加權結果................................................................72 4.10油品與氣膠之鉛同位素比值特徵比較探討......................................74 4.10.1油品與臺北地區氣膠之鉛同位素比值特徵比較....................74 4.10.2油品與彭佳嶼及中國氣膠之鉛同位素比值特徵比較............76 第五章 結論與建議..........................................................................................78 參考文獻..............................................................................................................79 | |
| dc.language.iso | zh-TW | |
| dc.subject | 油品 | zh_TW |
| dc.subject | 穩定性鉛同位素 | zh_TW |
| dc.subject | 環境鑑識 | zh_TW |
| dc.subject | 感應耦合電漿質譜儀 | zh_TW |
| dc.subject | Gasoline | en |
| dc.subject | Stable lead isotopes | en |
| dc.subject | Environmental forensics | en |
| dc.subject | Inductively coupled plasma mass spectrometer | en |
| dc.title | 臺灣油品之鉛同位素特徵及其環境鑑識應用 | zh_TW |
| dc.title | The Characteristics of Lead Isotopes of Taiwan Gasoline and Its Application to Environmental Forensics | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 100-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 張文亮,沈川洲,徐貴新 | |
| dc.subject.keyword | 油品,穩定性鉛同位素,環境鑑識,感應耦合電漿質譜儀, | zh_TW |
| dc.subject.keyword | Gasoline,Stable lead isotopes,Environmental forensics,Inductively coupled plasma mass spectrometer, | en |
| dc.relation.page | 88 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2012-08-21 | |
| dc.contributor.author-college | 生物資源暨農學院 | zh_TW |
| dc.contributor.author-dept | 生物環境系統工程學研究所 | zh_TW |
| 顯示於系所單位： | 生物環境系統工程學系 | |
文件中的檔案：
| 檔案 | 大小 | 格式 | |
|---|---|---|---|
| ntu-101-1.pdf 未授權公開取用 | 5.78 MB | Adobe PDF |
系統中的文件，除了特別指名其著作權條款之外，均受到著作權保護，並且保留所有的權利。