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完整後設資料紀錄
DC 欄位 | 值 | 語言 |
---|---|---|
dc.contributor.advisor | 梁文傑 | |
dc.contributor.author | Chiou-Ling Chang | en |
dc.contributor.author | 張秋玲 | zh_TW |
dc.date.accessioned | 2021-06-15T07:04:31Z | - |
dc.date.available | 2016-01-17 | |
dc.date.copyright | 2011-01-17 | |
dc.date.issued | 2010 | |
dc.date.submitted | 2010-12-25 | |
dc.identifier.citation | (1) Shirota, Y.; Kageyama, H. Chemical Reviews 2007, 107, 953.
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dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/48610 | - |
dc.description.abstract | Due to triphenylamine (TPA) with good hole transport, and electron-rich properties, we try to introduce this moiety onto the fullerene to investigate the electrochemical properties and the performance of photovoltaic devices. Besides, TPA with electroactive properties, we also functionalize single walled carbon nanotubes (SWCNTs) with TPA derivative to explore the behavior of electropolymerization. Moreover, we functionalize SWCNTs with thiol groups to study the self assembly behavior.
In chapter 2, we synthesize fullerene derivatives H-C60 mono 5a and H-C60 di 6a with TPA moiety. We discuss the electrochemical behavior of fullerene derivatives and the electrochemical properties of the polymeric films. We find that the polymeric films have the electrochemical memory in DMF. In chapter 3, we synthesize fullerene derivatives with TPA moiety containing para methyl substitution, Me-C60 mono 5b and Me-C60 di 6b. We study the performance of photovoltaic devices based on P3HT : fullerene derivatives with various blend ratios and casting solvents. The device of P3HT : Me-C60 mono 5b with the blend ratio 1 : 0.7 in a mixed solvent of ODCB and TCB showed high open circuit voltage (Voc) of 0.69 V under the illumination of AM 1.5G, 100 mW/cm2 with high power conversion efficiency (PCE) of 3.16 %. The device of P3HT : Me-C60 di 6b (1 : 1) shows even higher Voc of 0.87 V with the PCE of 1.83 %. In chapter 4, we combine the good merits of PCBM with higher Jsc and Me-C60 di 6b with higher Voc. This is the first time to tune Voc by adding Me-C60 di 6b as a dopant. We find the correlation between Voc and the blend ratios of PCBM to Me-C60 di 6b. In chapter 5, we investigate ternary mixing consisting of poly(3-hexythiophene) (P3HT), PCBM and Me-C60 mono 5b. From the changes of optical micrography, TEM images, UV-Vis absorption, and photoluminescence , we find that thermal stability of polymer solar cells with the addition 10 % of Me-C60 mono 5b are remarkly enhanced by supressing the destructive phase segregation between the polymer and fullerene. For ternary films, there are no significant degradation in morphology or performance even after 15 hr annealing at 160 oC, where the performance of devices based on PCBM or based on Me-C60 mono 5b degraded dramatically against long-time annealing. In chapter 6, we synthesize a series of soluble single walled carbon nanotube derivatives by amidation. We investigate the self assembly behavior between Au substrate and gold nanoperticles and thiol- functionalized nanotubes (2-4). The gold nanoparticles are sticking not only at the terminal, but also on the side-wall of SWCNT. Further, we can purify and separate from higher molecular weight by GPC. Besides, we synthesize SWCNT with TPA moiety (2-6) can proceed the electropolymerization while applying potential. | en |
dc.description.provenance | Made available in DSpace on 2021-06-15T07:04:31Z (GMT). No. of bitstreams: 1 ntu-99-D93223016-1.pdf: 16570709 bytes, checksum: b5080b6e5a4fcfaafa70692f12068ea4 (MD5) Previous issue date: 2010 | en |
dc.description.tableofcontents | Table of Contents
Page Table of Contents I List of Figures . X List of Tables . XXXII List of Schemes . XXXVII Abstract . XXXIX Chapter 1 Introduction 1 1.1. Thesis introduction 1 1.1.1. Review the Studies of Triphenylamine Based Materials in lab. 4 1.2. Basic Properties of Triphenylamine Based Materials 8 1.2.1. Hole Transport Property of Triphenylamine Based Materials 9 1.2.2. Electro Chemical Property of Triphenylamine Based Materials 10 1.2.2.1. Property of Electropolymerization of Triphenylamine Based Materials 11 1.3. Application of Triphenylamine Derivatives in OPVs 14 1.3.1. Based on Triphenylamine Small Molecules 14 1.3.2. Based on Triphenylamine Polymer Molecules 18 1.4. Improvement of the Performance by the Addition of Dopants 20 1.4.1. Doping with Small Molecules 21 1.4.2. Doping with Triplet Excitons or Spin 1/2 Radicals 22 1.4.3. Doping with Improved Spectral Coverage 25 1.4.4. Doping with Single Walled Carbon NanoTubes or Multiwalled Carbon Nanotubes 27 1.5. Thesis theme 32 Chapter 2 Properties of the Electrochemistry of Fullerene with Tripheylamine Addends: Formation of a Redox- Active Polymeric Films 33 2.1. Introduction 33 2.2. Results and Disscussion 42 2.2.1. Synthesis 42 2.2.2. UV-Vis absorption of H-C60 mono 5a and H-C60 di 6a 44 2.2.3. Analysis of Electrochemical Behavior of H-C60 mono 5a and H-C60 di 6a by Cyclic Voltammetry 45 2.2.4. Analysis the Electrochemical Behavior of Polymeric films of 7 and 8 by Cyclic Voltammetry 51 2.2.5. Study of UV-Vis absorption, EQCM, Thickness Analysis and SEM images of Electropolymeric films 8 55 2.2.5.1. Study of UV-Vis absorption of Electropolymeric films 8 55 2.2.5.2. EQCM study of Electropolymeric films 8 57 2.2.5.3. Film thickness study of Electropolymeric films 8 58 2.2.5.4. SEM study of Electropolymerics films 8 59 2.2.6. Electrochemical Memory Effects Study of Polymer 8 62 Chapter 3 Triphenylamine Derivatives- Substituted Methanofullerene Derivatives for Enhanced Open-Circuit Voltages and Efficiencies in Polymer Solar Cells 66 3.1. Introduction 66 3.1.1. History and several approaches of solar cells 66 3.1.2. Basic Acquaintance of Solar cells 67 3.1.3. Organic Photovoltaic Device Architectures 73 3.1.3.1. Bilayer Devices (Tang type cell) 73 3.1.3.2. Bulk Heterojunction Devices (BHJ) 75 3.1.3.3. Stacked bulk heterojunction Devices (A multilayer Structure) 76 3.1.4. Preparation Techiques: 79 3.2. Result and discussion 81 3.2.1. Molecules syntheses: 81 3.2.2. Electrochemistry Ananlysis 86 3.2.3. Photophysical Properties of Me-C60 mono 5b and Me-C60 di 6b 88 3.2.4. Photophysical Properties of Me-C60 mono 5b and Me-C60 di 6b, PCBM and BisPCBM in P3HT 89 3.2.4.1. UV-Vis Absorption of Me-C60 mono 5b and Me-C60 di 6b, PCBM and BisPCBM in P3HT 89 3.2.4.2. Photoluminescence of Me-C60 mono 5b and Me-C60 di 6b, PCBM and BisPCBM in P3HT 90 3.2.5. Photovoltaic Properties 91 3.2.5.1. Photovoltaic properties of P3HT : Me-C60 mono 5b 92 3.2.5.2. Photovoltaic Properties of P3HT : Me-C60 di 6b 100 3.2.6. Morphology Study 104 Chapter 4 Tuning the Open Circuit Voltage of The Solar Cells Based on Blending P3HT with PCBM and Triphenylamine- Substituted Methanofullerene Derivative as a Dopant 109 4.1. Introduction 109 4.2. Results and discussion 113 4.2.1. Effects of molecular weight and annealing temperature on Performance of Solar Cells 114 4.2.2. Study of Performance of solar cells based on P3HT : PCBM while Me-C60 di 6b as dopant and TEM analysis 118 Chapter 5 Enhanced the Thermal Stability of Active Layers of Polymer Solar Cells by The Addition of Amorphous Fullerene Derivatives with Tripheylamine Addend 124 5.1. Introduction 124 5.2. Results and Discussion 130 5.2.1. Study of Performance of Solar Cells based on Ternary Mixing 131 5.2.2. Morphological Change of P3HT : PCBM : Me-C60 mono 5b During the Thermal Annealing 144 5.2.3. Effect of Temperature on Optical Spectroscopy of Ternary Mixing 151 5.2.3.1. Effect of Temperature on UV-Vis Absorption of P3HT : PCBM : Me-C60 mono 5b 151 5.2.3.2. Effect of Temperature on Photoluminescence of P3HT : PCBM : Me-C60 mono 5b 153 Chapter 6 Preparation of Soluble Carbon Nanotube Derivatives and Observation The Properties of Self Assembly and Electropolymerization 157 6.1. Introduction 157 6.2. Results and Discussion 163 6.2.1. Synthesis 163 6.2.2. Characterization by IR, NMR 169 6.2.3. Self-Assembly Behavior with Gold Substrate and Gold Nanoparticle Detected by AFM, UV-Vis, TEM, and ESCA. 173 6.2.3.1. Observation the Self Assembly Behavior with Gold Nanoparticle in Solution 173 6.2.3.2. Study the Self Assembly behavior by AFM, UV-Vis and TEM 176 6.2.3.3. Purify Functionalized SWCNT 2-4 by GPC 180 6.2.3.4. Study the Self Assembly Behavior by AFM and ESCA after Purication 183 6.2.4. Electropolymeric Behavior of 2-6 Detected by Cyclic Voltammetry 187 Chapter 7 Conclusion 190 Chapter 8 References 193 Chapter 9 Experimental Section 218 9.1. Experimental Instruments and Chemicals 218 9.1.1. Instruments: 218 9.1.1.1. Nuclear magnetic resonance spectrum 218 9.1.1.2. Other instruments 219 9.1.2. Chemicals: Solvents and reagents 219 9.2. Synthetic Procedures: 221 9.3. NMR data 246 9.4. Mass Spectrascopy 293 9.5. Electrochemical Measurement of Fullerene Derivatives 300 9.5.1. Cyclic Voltammetry Study 300 9.5.2. EQCM Experiment: 328 9.6. UV-Vis spectroscopy 331 9.7. FL Spectascopy 346 9.8. Fabrication and characterization of photovoltaic cells Properties of P3HT : Me-C60 mono 5b and P3HT : Me-C60 di 6b 357 9.8.1. Device Fabrication 357 9.8.2. Device Measurements 358 9.9. Optical Microscopy 371 9.10. TEM images 376 9.11. IR Sepectrum 378 | |
dc.language.iso | en | |
dc.title | 富勒烯及單壁奈米碳管具三苯胺衍生物之合成、性質探討與應用 | zh_TW |
dc.title | Synthesis and Characterization of Fullerene and Single Walled Carbon NanoTubes Derivatives with Triphenylamine Moiety,
and Their Applications | en |
dc.type | Thesis | |
dc.date.schoolyear | 99-1 | |
dc.description.degree | 博士 | |
dc.contributor.oralexamcommittee | 王立義,何國川,汪若蕙,戴子安 | |
dc.subject.keyword | 電聚合,高分子太陽能電池,碳六十衍生物,3-己烷基聚噻,吩,熱穩定性,官能基化奈米碳管,自組裝, | zh_TW |
dc.subject.keyword | Electropolymerization,Polymer solar cells,Fullerene derivatives,Poly (3-hexylthiophene) (P3HT),Thermal stability,Functionalization of single walled carbon nanotubes (SWCNTs),Self-assembly, | en |
dc.relation.page | 381 | |
dc.rights.note | 有償授權 | |
dc.date.accepted | 2010-12-25 | |
dc.contributor.author-college | 理學院 | zh_TW |
dc.contributor.author-dept | 化學研究所 | zh_TW |
顯示於系所單位: | 化學系 |
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