請用此 Handle URI 來引用此文件：
http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/41742完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 王大銘(Da-Ming Wang) | |
| dc.contributor.author | Yi-Chen Kuo | en |
| dc.contributor.author | 郭怡辰 | zh_TW |
| dc.date.accessioned | 2021-06-15T00:29:38Z | - |
| dc.date.available | 2016-09-19 | |
| dc.date.copyright | 2011-09-19 | |
| dc.date.issued | 2011 | |
| dc.date.submitted | 2011-08-15 | |
| dc.identifier.citation | 1. 張閨臣 賴. 中西醫會診 齲齒. 初版 ed. 書泉, 臺北市, 1999.
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The influence of fatigue loading on the quality of the cement layer and retention strength of carbon fiber post-resin composite core restorations. Operative Dentistry. 2005; 30: 220-227. | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/41742 | - |
| dc.description.abstract | 隨著美容牙科的盛行，樹脂複合材料的快速發展，對牙體復形的要求也從不間斷，因此在牙科材料上不斷改良、推陳出新，只為求得更完美的修復。本研究團隊相繼研究開發針對在根管治療後維持牙體上所使用之材料，從中心根柱到外圍與牙齒黏著所用之黏著劑（cement）皆有不錯的效果；而先前在與牙齒之黏著系統研究中，團隊研發之樹脂黏著劑（resin cement）所搭配使用的黏合劑為市售產品OptiBond Solo Plus，因此在本實驗中使用團隊研發之樹脂黏合劑，並以先前團隊中發展之樹脂基質為基本的樹脂成分，研究在此黏著系統下之黏合劑所需因子，以提供研發增強與牙本質黏著強度之黏合劑。
實驗中利用Bis-GMA（Bisphenol-A-glycidyl dimethacrylate）與TEGDMA（triethylene glycol dimethacrylate）為黏合劑的樹脂單體，分別加入不同的單體或溶劑，探討對牙本質之黏著能力的影響；本實驗利用接觸角的量測去觀察黏合劑對酸蝕過的牙本質之潤濕能力，實驗發現，所加入的單體與溶劑皆可以提升黏合劑對牙本質的潤濕能力；另外，利用微拉伸測試法以及推離鍵結測試法來量測樹脂黏著劑搭配黏合劑的使用對牙本質的黏著強度，分別探討不同成分對黏著效果的影響，並藉由掃描式電子顯微鏡觀察測試後之牙齒破壞面的微結構；結果發現，在我們所發展的黏合系統，對酸蝕過的牙本質已具有不錯的潤濕能力，能進入牙小管以及牙本質的空隙，但與牙本質的黏著力，仍有待進一步改善。 | zh_TW |
| dc.description.abstract | Development of resin composites advances very fast because of the demand of esthetic dentistry. For better dental restoration, various kinds of new materials have been developed. Our research group studies new materials for endodontic therapy. We have developed new post and resin cement having high binding strength to the root canal dentin. However, the high binding strength relies on using the commercial product OptiBond Solo Plus as the bonding agent. The aim of this study is to explore the role of bonding agent in enhancing the binding strength to dentin, as a first step to develop new bonding agents suitable for the post and resin cement that we developed.
Bis-GMA (bisphenol-A-glycidyl dimethacrylate) and TEGDMA (triethylene glycol dimethacrylate) were used as the resin monomers of the bonding agents. Various of monomers and solvents were added in the resin monomers to enhance their binding strength to dentin. The wetting ability of the bonding agents on the etched dentin surface was evaluated by using the contact angle measurement. The results showed that all the additives elevated the wetting ability. Also, the micro-tensile bond test and the push-out bond test were used to evaluate the adhesion strength between dentin and the bonding agents, together with examining the microstructure of dentin surface, to study the influence of the additives on binding strength to dentin. The results indicated that bonding agents we developed had good wetting ability on dentin surface, but further enhancement of their binding strength is still needed. | en |
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| dc.description.tableofcontents | 誌謝 I
中文摘要 III Abstract V 總目錄 VII 表目錄 XIII 圖目錄 XV 第一章 緒論 1 第二章 文獻回顧 3 2-1 牙齒的結構 3 2-1-1 牙釉質 3 2-1-2 牙本質 4 2-1-3 牙髓 7 2-1-4 牙骨質（cementum） 7 2-2 牙體復形（Dental Restoration） 7 2-2-1 直接修復（direct restoration） 9 2-2-2 間接修復（indirect restoration） 9 2-2-3 修復材及其優缺點 9 2-2-3-1 金屬 10 2-2-3-2 金和金 10 2-2-3-3 普通金屬合金 11 2-2-3-4 牙齒汞齊填充物（dental amalgam fillings） 11 2-2-3-5 陶瓷（porcelain�ceramic） 12 2-2-3-6 金屬燒附陶瓷（porcelain fused to metal, PFM） 13 2-2-3-7 複合樹脂填充物（composite resin fillings） 13 2-2-3-8 玻璃離子聚合物黏土（glass-ionomer cement） 14 2-2-3-9 樹脂離子聚合物黏土（resin-ionomer cement） 14 2-3 牙本質黏合劑（Dentin Bonding Agent） 15 2-3-1 牙本質之黏著 15 2-3-2 牙本質黏合劑之發展 17 2-3-2-1 第一代（First Generation） 18 2-3-2-2 第二代（Second Generation） 18 2-3-2-3 第三代（Third Generation） 19 2-3-2-4 第四代（Fourth Generation） 20 2-3-2-5 第五代（Fifth Generation） 22 2-3-2-6 第六代（Sixth Generation） 22 2-3-2-7 第七代（Seventh Generation） 23 2-3-3 理想的牙本質黏合劑 24 2-3-4 牙本質黏合劑之應用 25 2-4 黏合劑之常用主要成分 26 2-4-1 樹脂單體 26 2-4-2 功能性單體 27 2-4-3 酸劑 29 2-4-4 溶劑 29 2-4-5 起始劑以及填充物 30 2-5 黏著強度之測試方法 31 2-5-1 微拉伸測試法（micro-tensile test） 32 2-5-2 推離測試法（push-out test） 34 第三章 實驗 37 3-1 實驗藥品 37 3-2 實驗儀器及裝置 41 3-3 實驗步驟與方法 42 3-3-1 黏合劑之製備 43 3-3-1-1 樹脂基材（resin matrix）之配製 43 3-3-1-2 黏合劑之配製 44 3-3-2 resin cement與黏合劑之黏著強度測試 47 3-3-3 黏合劑對牙本質之潤濕能力 48 3-3-4 牙齒試片之製備 49 3-3-4-1 微拉伸鍵結強度測試 49 3-3-4-2 推離鍵結強度測試 51 3-3-5 牙本質黏著強度之測試 55 3-3-5-1 微拉伸鍵結強度測試 55 3-3-5-2 推離鍵結強度測試 56 3-3-6 掃描式電子顯微鏡分析 58 第四章 結果與討論 59 4-1 黏合劑與IE-resin cement之黏著強度 59 4-2 黏合劑對牙本質之潤濕能力 60 4-3 IBOA與EHA在黏合劑中的角色 62 4-4 HEMA及其含量對黏合劑的影響 63 4-5 溶劑乙醇對黏合劑的影響 65 4-6 IBOA及EHA與乙醇對含有HEMA之黏合劑的影響 67 4-6-1 IBOA與EHA於黏合劑mH(30)之影響 67 4-6-2 乙醇於黏合劑mH(23)之影響 68 4-7 比較與市售黏合劑之差異 69 第五章 結論 87 第六章 未來工作 89 參考文獻 91 Appendix 105 | |
| dc.language.iso | zh-TW | |
| dc.subject | 推離鍵結測試 | zh_TW |
| dc.subject | 黏合劑 | zh_TW |
| dc.subject | 牙本質 | zh_TW |
| dc.subject | 接觸角 | zh_TW |
| dc.subject | 微拉伸測試 | zh_TW |
| dc.subject | dentin | en |
| dc.subject | push-out test | en |
| dc.subject | micro-tensile test | en |
| dc.subject | contact angle | en |
| dc.subject | bonding agent | en |
| dc.title | 以樹脂複合材研發牙本質黏合劑之研究 | zh_TW |
| dc.title | Investigation of the development of dentin bonding agent with resin composite | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 99-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.coadvisor | 李伯訓(Bor-Shiunn Lee) | |
| dc.contributor.oralexamcommittee | 戴子安(Chi-An Dai),鄭國忠(Kuo-Chung Cheng) | |
| dc.subject.keyword | 黏合劑,牙本質,接觸角,微拉伸測試,推離鍵結測試, | zh_TW |
| dc.subject.keyword | bonding agent,dentin,contact angle,micro-tensile test,push-out test, | en |
| dc.relation.page | 112 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2011-08-15 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 化學工程學研究所 | zh_TW |
| 顯示於系所單位： | 化學工程學系 | |
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