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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 吳紀聖 | |
| dc.contributor.author | Tzu-Hua Wu | en |
| dc.contributor.author | 吳姿樺 | zh_TW |
| dc.date.accessioned | 2021-06-13T04:18:17Z | - |
| dc.date.available | 2007-07-25 | |
| dc.date.copyright | 2006-07-25 | |
| dc.date.issued | 2006 | |
| dc.date.submitted | 2006-07-24 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/32891 | - |
| dc.description.abstract | 為了解決二氧化碳溫室氣體和能源問題，本研究於容納216根光纖之光反應器內，以100W高壓汞燈、波長365nm、光反應器溫度348K、流動式穩定狀態氣相系統中進行二氧化碳光催化還原反應。利用改良式熱水解法製備一系列TiO2、Cu/TiO2、Ag/TiO2、Pt/TiO2覆膜液，藉由浸漬覆膜法於直徑為0.1mm之光纖表面。由SEM之觀測，光纖表面的觸媒顆粒略呈圓形，粒徑約為10-20nm，觸媒層厚約26-33nm，並具有許多奈米級孔隙。經XRD繞射圖譜分析觸媒皆為anatase晶相，且紫外-可見光吸收波長約在350nm處。由XPS表面分析結果顯示，負載於二氧化鈦的Cu、Ag及Pt等金屬，分別以Cu+、Ag0及Pt2+或Pt4+存在於二氧化鈦表面。實驗結果發現，當光強度增強時，觸媒活性也隨之增加。以GC-FID測得主要產物為甲醇，及其他微量產物甲酸、甲酸甲酯等，銅、銀、鉑等過渡金屬的添加皆有效地提高甲醇的產率。 | zh_TW |
| dc.description.abstract | In order to remedy the greenhouse gas CO2 and energy shortage, the photoreduction of CO2 is studied in a UV-illuminating steady-state gas photo-reactor with 216 optical fibers by a 100W high-pressure Hg lamp with wavelength 365nm at 348K. M(Cu, Ag, Pt)/TiO2 solutions were prepared by an improved thermal hydrolysis method. The optical fibers with the diameter of 0.1mm were coated by the dip-coating method. From the SEM micrographs, the catalyst layer had thickness about 30nm comprising fine spherical particles, which had diameter of 10-20nm and nano cavities between the crystallites. The XRD spectra showed all M(Cu, Ag, Pt)/TiO2 had anatase phase. From the UV-Vis spectra, the wavelength of absorption edge was near 350nm. The results of the XPS spectra revealed that Cu, Ag and Pt in the forms of Cu+, Ag0, Pt2+ or Pt4+ existed on TiO2 surface, respectively. The methanol yield increased with increasing UV irradiative intensity. The main product was methanol and other few products were formic acid and methyl formate. The loaded transition-metals (Cu, Ag, Pt) efficiently enhanced the methanol yield. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-13T04:18:17Z (GMT). No. of bitstreams: 1 ntu-95-R93524019-1.pdf: 1739773 bytes, checksum: a2780de4915de000512071468e6b1255 (MD5) Previous issue date: 2006 | en |
| dc.description.tableofcontents | 致謝
中文摘要 I 英文摘要 II 目錄 III 圖目錄 VI 表目錄 VIII 第一章 緒論 1 第二章 文獻回顧 3 2-1 二氧化碳的簡介 3 2-2 二氧化碳的固定 4 2-3 二氧化碳的光催化還原 7 2-4 二氧化鈦簡介 11 2-4-1 二氧化鈦結構 11 2-4-2 二氧化鈦光催化原理 15 2-4-3 二氧化鈦量子效應 17 2-4-4 二氧化鈦親水性質 18 2-5 添加金屬改質二氧化鈦 20 2-6 光纖反應器 22 2-6-1 光纖簡介 23 2-6-2 各式光纖反應器及其應用 26 2-7 增黏劑的影響 32 第三章 實驗方法 35 3-1實驗藥品與儀器設備 35 3-1-1 藥品 35 3-1-2 器材 36 3-2 觸媒覆膜液的製備 37 3-2-1 熱水解法 37 3-2-2 基材清洗 38 3-2-3 浸漬覆膜法 41 3-3 觸媒特性分析原理與方法 44 3-3-1 儀器型號與規格 44 3-3-2 紫外光-可見光光譜儀 45 3-3-3 場發射掃描式電子顯微鏡 46 3-3-4 能量散佈分析儀 48 3-3-5 X光光電子能譜儀 48 3-3-6 X光繞射儀 50 3-4 光催化活性檢測 53 3-4-1 光纖反應器改良 54 3-4-2 二氧化碳光催化還原 59 3-4-3 SISC色層分析數據處理系統 64 第四章 實驗結果 66 4-1 二氧化鈦覆膜液 66 4-2 觸媒檢測及特性分析 67 4-2-1 XRD 68 4-2-2 BET及孔徑分佈 70 4-2-3 UV-VIS 71 4-2-4 SEM 72 4-2-5 EDS 74 4-2-6 XPS 75 4-3觸媒光催化活性檢測 84 4-3-1 空白實驗 84 4-3-2 二氧化碳光催化還原 85 4-3-3 量子效率 91 第五章 結果討論 94 5-1 金屬改質效應 94 5-1-1 銅在Cu/TiO2之價態與特性 94 5-1-2 銀在Ag/TiO2之價態與特性 95 5-1-3 鉑在Pt/TiO2之價態與特性 95 5-2 影響二氧化碳光催化還原之因素 97 5-2-1 紫外光強度效應 97 5-2-2 滯留時間效應 98 5-3 活性比較 99 第六章 結論 103 第七章 參考文獻 104 附錄 111 個人小傳 124 | |
| dc.language.iso | zh-TW | |
| dc.title | M(Cu, Ag, Pt)/TiO2覆膜光纖進行二氧化碳光催化還原 | zh_TW |
| dc.title | CO2 Photo Reduction Using Optical-fiber Coated with M(Cu, Ag, Pt)/TiO2 Catalysts | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 94-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 吳乃立,顧洋 | |
| dc.subject.keyword | 光催化還原,光纖反應器,二氧化碳,二氧化鈦, | zh_TW |
| dc.subject.keyword | Photocatalytic reduction,Optical-fiber reactor,CO2,TiO2, | en |
| dc.relation.page | 123 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2006-07-25 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 化學工程學研究所 | zh_TW |
| 顯示於系所單位： | 化學工程學系 | |
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