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| ???org.dspace.app.webui.jsptag.ItemTag.dcfield??? | Value | Language |
|---|---|---|
| dc.contributor.advisor | 廖英志 | zh_TW |
| dc.contributor.advisor | Ying-Chih Liao | en |
| dc.contributor.author | 葉佾叡 | zh_TW |
| dc.contributor.author | Yi-Jui Yeh | en |
| dc.date.accessioned | 2025-04-02T16:19:11Z | - |
| dc.date.available | 2025-04-03 | - |
| dc.date.copyright | 2025-04-02 | - |
| dc.date.issued | 2025 | - |
| dc.date.submitted | 2025-02-21 | - |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/97290 | - |
| dc.description.abstract | 石墨烯量子點（Graphene Quantum Dots, GQDs）以其奈米尺度的尺寸、可調控的表面化學性質以及量子侷限效應，在多尺度分子分離的膜技術中帶來進步。雖然共價有機框架（COFs）、金屬有機框架（MOFs）和碳奈米管（CNTs）等材料在分離應用中顯示出潛力，但其實際應用面臨許多限制，例如合成過程複雜、生產成本高、機械結構脆弱以及易受污染影響。相比之下，基於石墨烯量子點的材料提供了一個可持續且多功能的替代方案，利用其簡單的電漿合成方法、科學的結構特性探討，以及在各種尺度上精細調控分子交互的能力。
在這項研究中，我們開發了結合氮摻雜石墨烯量子點（GQDs）的電漿工程膜，將其作為多功能的奈米填料。這些GQDs是通過綠色、大氣壓電漿技術合成，能夠精準控制孔結構、表面功能性以及分子間的交互作用。在奈米濾膜應用中，GQD膜表現達到了超高的水通量（289 L·m⁻²·h⁻¹·bar⁻¹）以及99.96%的染料阻絕率，這歸因於其優異的表面親水性和互聯的奈米通道。同時，GQD-無機複合材料在次奈米尺度的應用中展現出色的性能，對分子量相差200 Da的分子分離因子達到92.68。在氣體分離方面，GQD-Pebax混合基質膜實現了卓越的CO₂滲透率（415 Barrer）和CO₂/N₂選擇性（125），這得益於其形成了有利於CO₂擴散的埃米尺度通道。 透過解決多尺度分子分離的挑戰，薄膜技術為水純化、碳捕集和工業廢棄物處理等多樣化應用提供了量身定制的解決方案。小尺度分離（如氣體淨化和藥品精煉）依賴於分子專一性和精確的孔控設計，而大尺度分離（如大分子過濾和污染物去除）則受益於增強的機械穩定性和表面化學交互作用。這種多尺度框架不僅提高了分離效率，還擴展了膜的功能多樣性，為清潔能源、環境保護以及生物醫學技術之應用。 | zh_TW |
| dc.description.abstract | Graphene Quantum Dots (GQDs), with their nanoscale dimensions, tunable surface chemistry, and exceptional quantum effects, represent a transformative advancement in membrane technologies for multi-scale molecular separation. While existing materials, such as covalent organic frameworks (COFs), metal-organic frameworks (MOFs), and carbon nanotubes (CNTs), have demonstrated potential in separation applications, their practical implementation is hindered by several limitations, including complex synthesis procedures, high production costs, mechanical fragility, and susceptibility to fouling. In contrast, GQD-based matrices present a sustainable and versatile alternative, capitalizing on their facile plasma-based synthesis, robust structural attributes, and capacity to fine-tune molecular interactions across various scales.
In this study, we developed plasma-engineered membranes incorporating nitrogen-doped GQDs as multifunctional nanofillers. Synthesized using a green, atmospheric-pressure microplasma process, GQDs offer precise control over pore architectures, surface functionality, and molecular interactions. At the nanofiltration scale, GQD membranes demonstrated exceptional performance, achieving ultrahigh water permeability (289 L·m⁻²·h⁻¹·bar⁻¹) and superior dye rejection (99.96%), attributed to enhanced hydrophilicity and interconnected nanochannels. Meanwhile, GQD-inorganic nanocomposites exhibited a remarkable separation factor of 92.68 for molecules differing by 200 Da in molecular weight, operating effectively at the sub-nanometer scale. For gas separation, GQD-Pebax mixed matrix membranes achieved exceptional CO₂ permeability (415 Barrer) and CO₂/N₂ selectivity (125), enabled by the creation of angstrom-level pathways favoring CO₂ diffusion. By addressing molecular separations across multiple scales, these membranes offer tailored solutions for diverse challenges in water purification, carbon capture, and industrial waste treatment. Small-scale separations, essential for applications such as gas purification and pharmaceutical refinement, rely on molecular specificity and precise pore control. Conversely, larger-scale separations, such as macromolecule filtration and pollutant removal, benefit from enhanced mechanical stability and surface chemical interactions. This multi-scale framework not only improves separation efficiency but also extends the functional versatility of membranes, paving the way for transformative applications in clean energy, environmental protection, and biomedical technologies. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2025-04-02T16:19:11Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2025-04-02T16:19:11Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | 致謝 I
中文摘要 II ABSTRACT III BIOGRAPHY V CONTENTS IX LIST OF FIG.S XIII LIST OF TABLES XXII OUTLINE XXIII CHAPTER 1 INTRODUCTION 1 1.1. WATER PURIFICATION VIA THIN FILM NANOCOMPOSITE (TFN) MEMBRANE 1 1.1.1 Membrane separation technology 1 1.1.2 Types of membranes 3 1.1.3.1 Thin film nanocomposite (TFN) membrane 5 1.1.3.2 Interfacial Polymerization (IP) 9 1.1.4 Review of graphene quantum dot (GQD) 13 1.1.5 Molecular simulation 17 1.2.1 Carbon dioxide capture technologies 22 1.2.2 Gas separation mechanism 23 1.2.3 Membrane materials 25 1.2.4. Adopted material 27 1.2.4.1 Graphene quantum dot 27 1.2.4.2 Polyether Block Amide (Pebax) 29 CHAPTER 2 EXPERIMENTAL MATERIALS AND EQUIPMENT 31 2.1 MATERIALS AND CHEMICALS 31 2.2 INSTRUMENTATIONS 32 2.2.1 Ultraviolet-Visible Spectroscopy (UV-Vis) 32 2.2.2 Photoluminescence (PL) Spectroscopy 32 2.2.3 Raman Spectroscopy 32 2.2.4 X-ray Photoelectron Spectroscopy (XPS) 33 2.2.5 Transmission Electron Microscopy (TEM) 33 2.2.6 Scanning Electron Microscopy (SEM) 34 2.2.7 Differential Scanning Calorimetry (DSC) 34 2.2.8 Zeta Potential Measurements 34 2.2.9 Fourier-Transform Infrared Spectroscopy (FT-IR) 35 2.2.10 Contact Angle Meter 35 2.2.11 Nanofiltration System in Flat Membrane 36 2.2.12 Nanofiltration System in Hollow Fiber Membrane 37 CHAPTER 3 PLASMA-ENABLED GRAPHENE QUANTUM DOT-BASED NANOFILTRATION MEMBRANES FOR WATER PURIFICATION AND DYE MONITORING 38 3.1 INTRODUCTION 38 3.2. EXPERIMENTAL SECTION 41 3.2.1 Preparation of GQD-based membranes 41 3.2.2 Materials characterization 42 3.2.3 Membrane performance evaluation 42 3.2.4 Theoretical calculation 43 3.3. RESULTS AND DISCUSSION 44 3.3.1 GQD NF membrane fabrication and characterization 44 3.3.2 Nanofiltration of GQD membranes 52 3.3.3 Theoretical calculation study of GQD membranes 57 3.3.4 PL-based dye monitoring study of GQD membranes 61 3.4 CONCLUSION 63 CHAPTER 4 ENGINEERING LOCAL ENVIRONMENT OF GQD-INORGANIC NANOCOMPOSITES FOR HIGH MOLECULAR SEPARATIONS 64 4.1 INTRODUCTION 64 4.2 EXPERIMENTAL SECTION 69 4.2.1 Synthesis of GQD-inorganic membranes 69 4.2.2 Characterization 70 4.2.3 NF separation measurement 71 4.3 RESULTS AND DISCUSSIONS 74 4.3.1 Synthesis and characterization of AHF substrate 74 4.3.3 Separation performance study of GQD membranes 83 4.4 CONCLUSIONS 91 CHAPTER 5 PLASMA-ENGINEERED GRAPHENE QUANTUM DOT-BASED NANOCOMPOSITES AS SMART CO2-PHILIC MEMBRANES WITH EXTREMELY HIGH SEPARATION PERFORMANCE 92 5.1 INTRODUCTION 92 5.2. EXPERIMENTAL SECTION 95 5.2.1 GQD@Pebax membrane fabrication. 95 5.2.2 Carbon capture measurement. 95 5.2.3 Theoretical calculation. 96 5.3 RESULTS AND DISCUSSION 97 5.3.1 GQD@Pebax membrane fabrication and characterization 97 5.3.2 Gas separation study of GQD@Pebax membranes 103 5.3.3 Theoretical calculation study of GQD@Pebax nanocomposite membranes 109 5.3.4 In situ PL spectroscopy study of GQD@Pebax membranes 113 5.4 CONCLUSION 115 CHAPTER 6 SUMMARY AND PERSPECTIVES 116 6.1 SUMMARY 116 6.2 PERSPECTIVES 118 REFERENCE 120 | - |
| dc.language.iso | en | - |
| dc.subject | 碳捕集 | zh_TW |
| dc.subject | 分子分離 | zh_TW |
| dc.subject | 石墨烯量子點 | zh_TW |
| dc.subject | 電漿奈米工程 | zh_TW |
| dc.subject | 奈米濾膜 | zh_TW |
| dc.subject | molecular separation | en |
| dc.subject | carbon capture | en |
| dc.subject | nanofiltration membranes | en |
| dc.subject | plasma nanotechnology | en |
| dc.subject | graphene quantum dots | en |
| dc.title | 石墨烯量子點混合基質薄膜進行多尺度分子分離 | zh_TW |
| dc.title | Graphene Quantum Dot-based Matrix Membrane for Multi-Scale Molecular Separation | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 113-2 | - |
| dc.description.degree | 博士 | - |
| dc.contributor.coadvisor | 童國倫;江偉宏 | zh_TW |
| dc.contributor.coadvisor | Kuo-Lun Tung;Wei-Hung Chiang | en |
| dc.contributor.oralexamcommittee | 吳紀聖;張鑑祥;杜育銘;曹恆光;葉禮賢 | zh_TW |
| dc.contributor.oralexamcommittee | Chi-Sheng Wu;Chien-Hsiang Chang;Yu-Ming Tu;Heng-Kwong Tsao;Li-Hsien Yeh | en |
| dc.subject.keyword | 分子分離,石墨烯量子點,碳捕集,奈米濾膜,電漿奈米工程, | zh_TW |
| dc.subject.keyword | molecular separation,graphene quantum dots,carbon capture,nanofiltration membranes,plasma nanotechnology, | en |
| dc.relation.page | 144 | - |
| dc.identifier.doi | 10.6342/NTU202500737 | - |
| dc.rights.note | 未授權 | - |
| dc.date.accepted | 2025-02-21 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 化學工程學系 | - |
| dc.date.embargo-lift | N/A | - |
| Appears in Collections: | 化學工程學系 | |
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