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DC 欄位 | 值 | 語言 |
---|---|---|
dc.contributor.advisor | 陳建彰 | zh_TW |
dc.contributor.advisor | Jian-Zhang Chen | en |
dc.contributor.author | 藍佩伶 | zh_TW |
dc.contributor.author | Pei-Ling Lan | en |
dc.date.accessioned | 2024-07-23T16:29:29Z | - |
dc.date.available | 2024-07-24 | - |
dc.date.copyright | 2024-07-23 | - |
dc.date.issued | 2024 | - |
dc.date.submitted | 2024-07-17 | - |
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dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/93247 | - |
dc.description.abstract | 本研究使用網印技術在碳布基材上沉積還原氧化石墨烯(rGO)-鋰錳氧化物(LiMnOx)奈米複合前驅物,接著利用氮氣常壓噴射式電漿(Atmospheric-Pressure Plasma Jet, APPJ)進行了超快速(<300秒)的焙燒處理,並使用硫酸(H2SO4)、氯化鋰(LiCl)和硫酸鋰(Li2SO4)三種凝膠態電解質製備具有還原氧化石墨烯(rGO)-鋰錳氧化物(LiMnOx)奈米複合電極的混合型超級電容器。通過分析表面特徵及電化學測量結果來比較不同電漿處理時間的影響,並探討了三種凝膠態電解質對電極性能的影響。
以面積電容、能量密度和循環穩定性等電化學分析結果及電解質的性能特點來評估混合型超級電容器中電極材料與電解質的相容性。研究顯示,電漿處理後大幅改善混合型超級電容器之性能。在所製備之混合型超級電容器中,使用硫酸鋰凝膠態電解質表現出最佳的面積電容值和能量密度。此情形源於其具有高擬電容效應(PC)和鋰離子遷移速率,增強了電極-電解質界面反應和有效表面積。此外,嵌入的鋰離子與電雙層電容(EDLC)的耦合進一步促進了整體電容的顯著增強。使用硫酸凝膠態電解質的混合型超級電容器則表現出更好的循環穩定性。研究結果闡明了凝膠電解質和電極材料之間的相互作用,為高性能混合型超級電容器的設計和優化提供了見解[1]。 | zh_TW |
dc.description.abstract | This study utilized screen printing technology to deposit a nanocomposite precursor of reduced graphene oxide (rGO) and lithium manganese oxide (LiMnOx) on a carbon cloth substrate. Subsequently, a rapid (<300 seconds) annealing process was carried out using nitrogen atmospheric-pressure plasma jet (APPJ). Three gel electrolytes, H2SO4/PVA, LiCl/PVA, and Li2SO4/PVA, were then employed to prepare hybrid supercapacitors (HSCs) featuring the rGO-LiMnOx nanocomposite electrode. The impact of different plasma treatment times was compared by surface analyses and electrochemical measurements, and the influence of the three gel electrolytes on electrode performance was investigated.
The compatibility between electrode materials and electrolytes in hybrid supercapacitors was assessed based on electrochemical analyses, including areal capacitance, energy density, and cyclic stability, along with the electrolyte's performance characteristics. The study revealed that plasma treatment significantly improved the performance of the HSC. Among the prepared HSCs, the use of Li2SO4 gel electrolyte exhibited the best areal capacitance and energy density values. This situation arises from its high pseudocapacitance (PC) effect and lithium-ion migration rate, enhancing the electrode-electrolyte interface reactions and effective surface area. Furthermore, the coupling of embedded lithium ions with the electric double-layer capacitance (EDLC) further promotes a significant enhancement of overall capacitance. The HSC employing H2SO4 gel electrolyte also demonstrated improved cyclic stability. The research findings elucidate the interactions between gel electrolytes and electrode materials, providing insights for the design and optimization of high-performance HSCs[1]. | en |
dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2024-07-23T16:29:29Z No. of bitstreams: 0 | en |
dc.description.provenance | Made available in DSpace on 2024-07-23T16:29:29Z (GMT). No. of bitstreams: 0 | en |
dc.description.tableofcontents | 致謝 i
摘要 ii Abstract iii 目次 iv 圖次 vii 表次 xii 第一章 緒論 1 1.1 前言 1 1.2 研究動機 2 1.3 論文大綱 3 第二章 文獻回顧與理論介紹 4 2.1 超級電容器 4 2.1.1 超級電容器及儲能元件之演進 4 2.1.2 超級電容器之能量儲存機制 6 2.1.3 超級電容器之電極與活性材料 11 2.1.4 超級電容器之電解質 20 2.2 實驗之電極材料 23 2.2.1 還原氧化石墨烯 23 2.2.2 鋰錳氧化物 25 2.3 實驗之凝膠態電解質 26 2.4 常壓電漿 27 2.4.1 電漿原理介紹 27 2.4.2 電漿的碰撞反應 30 2.4.3 常壓電漿之種類及應用 33 2.5 電化學分析 36 2.5.1 循環伏安法 36 2.5.2 恆電流充放電 38 2.5.3 電化學阻抗圖譜 39 第三章 實驗流程與儀器介紹 40 3.1 實驗材料與儀器清單 40 3.1.1 實驗材料清單 40 3.1.2 實驗儀器清單 42 3.2 製程儀器 44 3.2.1 迴旋濃縮機 44 3.2.2 氣壓式網版印刷機 45 3.3 實驗流程 46 3.3.1 製備還原氧化石墨烯-鋰錳氧化物前驅漿料 46 3.3.2 還原氧化石墨烯-鋰錳氧化物電極製備 47 3.3.3 凝膠態電解質製備 48 3.3.4 可撓性超級電容器製備 49 3.4 分析儀器 51 3.4.1 水接觸角量測儀 51 3.4.2 場發射鎗掃描式電子顯微鏡 52 3.4.3 X射線繞射儀 53 3.4.4 X射線光電子能譜儀 54 3.4.5 電化學工作站 56 第四章 結果與討論 57 4.1 還原氧化石墨烯-鋰錳氧化物電極之電漿參數選用 57 4.1.1 氮氣常壓噴射式電漿之氣體流量 57 4.1.2 氮氣常壓噴射式電漿之電漿處理時間 57 4.2 還原氧化石墨烯-鋰錳氧化物電極之微結構觀察 61 4.3 還原氧化石墨烯-鋰錳氧化物電極之親水性分析 65 4.4 還原氧化石墨烯-鋰錳氧化物電極之晶體結構分析 67 4.5 還原氧化石墨烯-鋰錳氧化物電極之表面化學型態分析 68 4.6 還原氧化石墨烯-鋰錳氧化物超級電容器之電化學分析 76 4.6.1 循環伏安法分析 76 4.6.2 Trasatti分析 80 4.6.3 恆電流充放電分析 85 4.6.4 Ragone plot 88 4.6.5 電化學阻抗圖譜分析 90 4.6.6 穩定性測試 92 第五章 結論 95 第六章 附錄 96 6.1 還原氧化石墨烯-鋰錳氧化物超級電容器之能量色散X射線譜分析 96 6.2 還原氧化石墨烯-鋰錳氧化物超級電容器之恆電流穩定性測試 97 參考文獻 99 個人期刊發表 112 | - |
dc.language.iso | zh_TW | - |
dc.title | 常壓噴射電漿超快速製備硫酸、氯化鋰、硫酸鋰凝膠態電解質還原氧化石墨烯-鋰錳氧化物超級電容器 | zh_TW |
dc.title | Rapid atmospheric-pressure plasma jet processed reduced graphene oxide (rGO)-LiMnOx supercapacitors with H2SO4, LiCl, and Li2SO4 gel electrolytes | en |
dc.type | Thesis | - |
dc.date.schoolyear | 112-2 | - |
dc.description.degree | 碩士 | - |
dc.contributor.oralexamcommittee | 陳奕君;羅世強;王孟菊 | zh_TW |
dc.contributor.oralexamcommittee | I-Chun Cheng;Shyh-Chyang Luo;Meng-Jiy Wang | en |
dc.subject.keyword | 混合型超級電容器,常壓噴射電漿,可撓性電極,還原氧化石墨烯, | zh_TW |
dc.subject.keyword | Hybrid supercapacitor (HSC),atmospheric-pressure plasma (APPJ),flexible electronics,reduced graphene oxide (rGO), | en |
dc.relation.page | 112 | - |
dc.identifier.doi | 10.6342/NTU202401834 | - |
dc.rights.note | 同意授權(限校園內公開) | - |
dc.date.accepted | 2024-07-18 | - |
dc.contributor.author-college | 工學院 | - |
dc.contributor.author-dept | 應用力學研究所 | - |
顯示於系所單位: | 應用力學研究所 |
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