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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 許麗 | zh_TW |
| dc.contributor.advisor | Li Xu | en |
| dc.contributor.author | 廖育德 | zh_TW |
| dc.contributor.author | Yu-De Liao | en |
| dc.date.accessioned | 2023-08-15T17:55:45Z | - |
| dc.date.available | 2023-11-09 | - |
| dc.date.copyright | 2023-08-15 | - |
| dc.date.issued | 2023 | - |
| dc.date.submitted | 2023-08-08 | - |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/88822 | - |
| dc.description.abstract | 隨著科技的發展，人類對於能源的消耗日益上升，換言之，廢熱的總量也在日益的增加，工業上的廢熱因其熱源溫度較高，已經有許多人在探討回收的方法，一般生活上也會有廢熱的產生，但其規模、時長及溫差大多不向工業廢熱一樣容易回收利用，因此如何將讓電裝置的體積縮小、提高轉換效率甚至是對人體無害就變成是重要的議題，而熱電薄膜就是為此而誕生的里程碑。
選擇鋁摻雜氧化鋅作為此研究之材料是由於高導電性、易取得(成本低)，對環境的汙染程度較低，使其成為近年來研究發現頗具潛力的熱門熱電材料之一，本研究利用波長532 nm、脈衝波時間8 ns的雷射，利用雷射高能量密度以及極短的加熱時間，搭配2D振鏡系統，高效和低成本的方式。將摻雜鋁的氧化鋅燒結沉積在石英上。 本實驗表面質量密度固定為5.1 mg/cm^2，並將雷射掃面之線段間距固定為20 μm，藉由調整不同脈衝重疊率及雷射能量大小來找出最佳的鋁摻雜氧化鋅奈米顆粒(0.5 wt%)薄膜製成的區間參數，並以相同的雷射能量區間及相同的脈衝重疊率來對不同摻雜濃度(0.5 wt%、1 wt%、2 wt%)的鋁摻雜氧化鋅奈米顆粒的雷射燒結結果進行表面型態、電性急熱電性質的比較。 | zh_TW |
| dc.description.abstract | With increasing energy consumption, the amount of waste heat generated has become a pressing issue. Industrial waste heat, known for its high temperature, has attracted attention for potential recovery methods. However, recovering waste heat from everyday life poses challenges due to its smaller scale, shorter duration, and lower temperature differentials. To address this, researchers have focused on developing thermoelectric thin films.
Aluminum-doped zinc oxide has been chosen for this research due to its high conductivity, availability, low cost, and minimal environmental impact. It has emerged as a promising thermoelectric material. In this study, a laser with specific parameters and a 2D scanning mirror system were utilized for efficient and cost-effective fabrication. Aluminum-doped zinc oxide was sintered onto quartz substrates using laser-induced forward transfer. The experiment involved a fixed surface mass density and controlled line spacing of the scanned laser. By adjusting pulse overlap ratios and laser energy levels, the optimal parameters for fabricating thin films with aluminum-doped zinc oxide nanoparticles (0.5 wt%) were determined. Surface morphology and electrical and thermoelectric properties of the laser-sintered films were compared among different doping concentrations (0.5 wt%, 1 wt%, 2 wt%) of aluminum-doped zinc oxide nanoparticles, using the same laser energy range and pulse overlap ratio. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2023-08-15T17:55:45Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2023-08-15T17:55:45Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | 口試委員審定書 i
誌謝 ii 中文摘要 iii Abstract iv 目錄 v 圖目錄 viii 表目錄 xii 第1章 緒論 1 第2章 文獻回顧及實驗動機 2 2.1 熱電原理 2 2.1.1 席貝克效應 (Seebeck Effect) 2 2.1.2 帕爾帖效應 (Peltier Effect) 3 2.1.3 湯姆森效應 (Thomson Effect) 5 2.1.4 無因次熱電參數 6 2.2 不同摻雜材料之氧化鋅應用 9 2.2.1 砷摻雜之氧化鋅 9 2.2.2 銦摻雜之氧化鋅 11 2.2.3 鎵摻雜之氧化鋅 12 2.2.4 鋁摻雜之氧化鋅 13 2.2.5 雙摻雜之氧化鋅 14 2.2.6 不同摻雜之氧化鋅 16 2.3 鋁摻雜氧化鋅奈米顆粒 17 2.3.1 摻雜濃度對電性和熱電性質之影響 17 2.3.2 不同基材之影響 19 2.3.3 摻雜濃度對光學性質之影響 20 2.4 加法雷射燒結之應用 23 2.4.1 金屬奈米顆粒 23 2.4.2 金屬氧化物之燒結 27 2.4.3 陶瓷材料之燒結 28 2.5 研究動機與實驗目的 29 第3章 實驗方法與實驗架構 31 3.1 氧化鋅奈米顆粒之塗層製備 31 3.1.1 鋁摻雜氧化鋅奈米顆粒塗層之溶液配置 31 3.2 選擇性雷射燒結實驗 33 3.2.1 脈衝雷射光路架設 35 3.2.2 振鏡掃瞄系統 37 3.2.3 掃描狹縫光束分析儀 39 3.2.4 微型控制走台 41 3.3 薄膜表面分析 42 3.3.1 膜厚測定儀 (Surface Profiler) 42 3.3.2 X光繞射儀(X-ray diffractometer , XRD) 43 3.3.3 掃描式電子顯微鏡 (Scanning Electron Microscope , SEM) 44 3.4 薄膜之電性及熱電分析 45 3.4.1 四點探針 (Four point Probe) 45 3.4.2 霍爾量測儀 (Hall Effect Measurement System) 47 3.4.3 數位多功能電表 (Digital Multimeter , DMM) 49 3.4.4 加熱系統 (Heater) 50 第4章 結果與討論 51 4.1 鋁摻雜氧化鋅奈米顆粒塗層 51 4.2 選擇性雷射燒結之參數討論 53 4.2.1 脈衝雷射輸出功率 53 4.2.2 雷射光斑大小測量 55 4.3 雷射燒結鋁摻雜氧化鋅奈米顆粒線段 56 4.4 雷射燒結鋁摻雜氧化鋅奈米顆粒薄膜 59 4.4.1 98 %脈衝重疊率之結果 59 4.4.2 不同脈衝重疊率之薄膜型態比較 62 4.4.3 判斷燒結材料分佈及燒結現象之分析 65 4.4.4 薄膜電性分析 67 4.5 不同摻雜濃度之鋁摻雜氧化鋅奈米顆粒薄膜 69 4.5.1 不同摻雜濃度下之薄膜形態 70 4.5.2 不同摻雜濃度下薄膜電性表現 76 4.5.3 不同摻雜濃度下薄膜電性比較 78 4.6 熱電性質量測 80 4.6.1 席貝克係數及功率因子 80 4.6.2 SEM結果 82 第5章 結論及未來展望 83 5.1 結論 83 5.2 未來展望 84 參考文獻 85 | - |
| dc.language.iso | zh_TW | - |
| dc.subject | 功率因子 | zh_TW |
| dc.subject | 雷射燒結 | zh_TW |
| dc.subject | 鋁摻雜氧化鋅奈米顆粒 | zh_TW |
| dc.subject | 熱電薄膜 | zh_TW |
| dc.subject | 席貝克係數 | zh_TW |
| dc.subject | aluminum-doped zinc oxide nanoparticles | en |
| dc.subject | laser sintering | en |
| dc.subject | power factor | en |
| dc.subject | Seebeck coefficient | en |
| dc.subject | thermoelectric thin films | en |
| dc.title | 選擇性雷射燒結鋁摻雜氧化鋅奈米顆粒及其 熱電方面的應用 | zh_TW |
| dc.title | Selective Laser Sintering of Al-doped Zinc Oxide Nanoparticles for Thermoelectrical Application | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 111-2 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.oralexamcommittee | 莊嘉揚;陳奕君 | zh_TW |
| dc.contributor.oralexamcommittee | Jia-Yang Juang;I-Chun Cheng | en |
| dc.subject.keyword | 雷射燒結,鋁摻雜氧化鋅奈米顆粒,熱電薄膜,席貝克係數,功率因子, | zh_TW |
| dc.subject.keyword | laser sintering,aluminum-doped zinc oxide nanoparticles,thermoelectric thin films,Seebeck coefficient,power factor, | en |
| dc.relation.page | 89 | - |
| dc.identifier.doi | 10.6342/NTU202302914 | - |
| dc.rights.note | 同意授權(全球公開) | - |
| dc.date.accepted | 2023-08-09 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 機械工程學系 | - |
| 顯示於系所單位： | 機械工程學系 | |
文件中的檔案：
| 檔案 | 大小 | 格式 | |
|---|---|---|---|
| ntu-111-2.pdf | 8.67 MB | Adobe PDF | 檢視/開啟 |
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