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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳建彰 | zh_TW |
| dc.contributor.advisor | Jian-Zhang Chen | en |
| dc.contributor.author | 卓韋瀚 | zh_TW |
| dc.contributor.author | Wei-Hang Cho | en |
| dc.date.accessioned | 2023-08-09T16:32:40Z | - |
| dc.date.available | 2023-11-09 | - |
| dc.date.copyright | 2023-08-09 | - |
| dc.date.issued | 2023 | - |
| dc.date.submitted | 2023-07-11 | - |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/88323 | - |
| dc.description.abstract | 本研究使用氮氣常壓噴射式電漿（Atmospheri Pressure Plasma Jet, APPJ）對碳布進行表面改質作為電極基材，接著網印上還原氧化石墨烯（rGO）-聚苯胺（PANI）漿料作為活性材料並烤乾製成還原氧化石墨烯-聚苯胺（rGO-PANI）超級電容電極，以銀/氯化銀電極（Ag/AgCl）作為參考電極和使用白金作為對電極，並分別使用了氯化鋰（LiCl）溶液、硫酸鋰（Li2SO4）溶液和硫酸（H2SO4）作為電解液對rGO-PANI電極進行三電極系統電化學分析。
為了評估rGO-PANI超級電容器的性能，運用了電化學阻抗譜（EIS）、循環伏安法（CV）和恆電流充放電法（GCD）等多種方法進行性能量測。電化學實驗结果表明，使用含鋰離子溶液作為電解液的rGO-PANI超級電容器表現出顯著的擬電容（PC）效應，而使用H2SO4電解液的超級電容器則表現出較大的電雙層電容（EDLC）效應。使用H2SO4電解液的超級電容器有最大的面積比電容，在三電極系統量測下為48.83 mF/cm2。在進行了10,000次循環伏安法的穩定性測試後，使用Li2SO4溶液電解液的rGO-PANI超級電容器表現出比使用LiCl溶液和H2SO4作為電解液的超級電容器更好的循環穩定性。 | zh_TW |
| dc.description.abstract | In this study, atmospheric pressure plasma jet (APPJ) was utilized to modify the surface of carbon cloth as an electrode substrate. Then, the reduced graphene oxide (rGO) and polyaniline (PANI) slurry was screen-printed and dried to form a rGO-PANI supercapacitor electrode. Three-electrode system electrochemical analysis of the rGO-PANI electrode was tested with Ag/AgCl electrode as reference electrode and platinum as counter electrode in LiCl solution, Li2SO4 solution, and H2SO4 electrolytes.
The results of the electrochemical experiments showed that the rGO-PANI supercapacitors with lithium salt solution electrolytes exhibited a significant pseudocapacitance (PC) effect, whereas the supercapacitor with H2SO4 electrolytes had a large electrical double-layer capacitance (EDLC) effect. The supercapacitor using H2SO4 electrolyte exhibited the highest areal capacitance, measuring at 48.83 mF/cm2 in three-electrode system measurements. Furthermore, after conducting a 10,000-cycle CV stability test, the rGO-PANI supercapacitor using Li2SO4 solution electrolyte showed better cycling stability than those with LiCl solution and H2SO4 electrolytes. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2023-08-09T16:32:40Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2023-08-09T16:32:40Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | 致謝 i
摘要 ii Abstract iii 目錄 iv 圖目錄 vii 表目錄 xi 1 第一章 緒論 1 1.1 前言 1 1.2 研究動機 2 1.3 論文大綱 4 2 第二章 理論與文獻回顧 5 2.1 超級電容器 5 2.1.1 超級電容器及儲能元件之發展 5 2.1.2 超級電容器之儲能原理與機制 7 2.1.3 超級電容器之電極與活性材料 11 2.1.4 超級電容器之電解液 16 2.2 石墨烯與聚苯胺 19 2.2.1 石墨烯 19 2.2.2 聚苯胺 21 2.3 常壓電漿 23 2.3.1 電漿原理及介紹 23 2.3.2 常壓電漿之種類及應用 27 3 第三章 實驗流程與各項儀器 30 3.1 實驗藥品與儀器 30 3.2 製程儀器 32 3.2.1 氣壓式網版印刷機 32 3.2.2 迴旋濃縮儀 33 3.3 實驗流程 34 3.3.1 調配還原氧化石墨稀-聚苯胺-殼聚醣漿料 34 3.3.2 還原氧化石墨稀-聚苯胺電極製備 35 3.4 分析儀器 36 3.4.1 場發射鎗掃描式電子顯微鏡及能量色散X射線譜 36 3.4.2 水接觸角量測儀 38 3.4.3 X射線繞射儀 39 3.4.4 X射線光電子能譜儀 41 3.4.5 電化學工作站 43 4 第四章 結果與討論 49 4.1 還原氧化石墨稀-聚苯胺電極之親水性分析 49 4.2 還原氧化石墨稀-聚苯胺電極之表面型態 50 4.3 還原氧化石墨稀-聚苯胺電極之結晶性分析 51 4.4 還原氧化石墨稀-聚苯胺電極之表面化學型態量測 52 4.5 還原氧化石墨稀-聚苯胺電極之電化學分析 55 4.5.1 循環伏安法分析 55 4.5.2 恆電流充放電分析 59 4.5.3 電化學阻抗譜分析 61 4.6 還原氧化石墨稀-聚苯胺電極之穩定性量測 63 4.6.1 循環伏安法穩定性量測 63 4.6.2 表面型態 64 4.6.3 晶體結構分析 65 5 第五章 結論 66 6 第六章 附錄：還原氧化石墨稀-聚苯胺超級電容 67 6.1 摘要 67 6.2 實驗流程 68 6.2.1 配製凝膠態電解質 68 6.2.2 組裝可撓性超級電容器 68 6.3 結果與討論 70 6.3.1 還原氧化石墨稀-聚苯胺超級電容器之循環伏安法分析 70 6.3.2 還原氧化石墨稀-聚苯胺超級電容器之恆電流充放電分析 72 6.3.3 還原氧化石墨稀-聚苯胺超級電容器之電化學阻抗譜分析 74 6.3.4 還原氧化石墨稀-聚苯胺超級電容器之可撓性測試 75 6.3.5 還原氧化石墨稀-聚苯胺超級電容器之穩定性量測 76 6.4 結論 78 7 參考文獻 79 8 個人期刊發表 93 | - |
| dc.language.iso | zh_TW | - |
| dc.subject | 聚苯胺 | zh_TW |
| dc.subject | 還原氧化石墨烯 | zh_TW |
| dc.subject | 可撓性電極 | zh_TW |
| dc.subject | 超級電容器 | zh_TW |
| dc.subject | Supercapacitor | en |
| dc.subject | Flexible electrode | en |
| dc.subject | Reduced graphene oxide | en |
| dc.subject | Polyaniline | en |
| dc.title | 還原氧化石墨烯-聚苯胺超級電容於含鋰電解液之性能比較 | zh_TW |
| dc.title | Performance comparison of reduced graphene oxide (rGO)-polyaniline (PANI) supercapacitors with lithium ion containing electrolytes | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 111-2 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.oralexamcommittee | 陳奕君;徐振哲 | zh_TW |
| dc.contributor.oralexamcommittee | I-Chun Cheng;Cheng-Che Hsu | en |
| dc.subject.keyword | 可撓性電極,超級電容器,還原氧化石墨烯,聚苯胺, | zh_TW |
| dc.subject.keyword | Flexible electrode,Supercapacitor,Reduced graphene oxide,Polyaniline, | en |
| dc.relation.page | 93 | - |
| dc.identifier.doi | 10.6342/NTU202301309 | - |
| dc.rights.note | 同意授權(全球公開) | - |
| dc.date.accepted | 2023-07-12 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 應用力學研究所 | - |
| 顯示於系所單位： | 應用力學研究所 | |
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