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完整後設資料紀錄
DC 欄位 | 值 | 語言 |
---|---|---|
dc.contributor.advisor | 陳建彰 | zh_TW |
dc.contributor.advisor | Jian-Zhang Chen | en |
dc.contributor.author | 曾家筠 | zh_TW |
dc.contributor.author | Chia-Yun Tseng | en |
dc.date.accessioned | 2023-08-09T16:32:05Z | - |
dc.date.available | 2023-11-09 | - |
dc.date.copyright | 2023-08-09 | - |
dc.date.issued | 2023 | - |
dc.date.submitted | 2023-07-12 | - |
dc.identifier.citation | [1] Zhang T, Wu J, Chen J, Pan Q, Wang X, Zhong H, et al. Activating titanium metal with H2 plasma for the hydrogen evolution reaction. ACS Applied Materials & Interfaces. 2021;13:24682-91.
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dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/88321 | - |
dc.description.abstract | 本研究將鎳鐵雙金屬有機框架(Metal Organic Frameworks, MOF)以水熱合成法(hydrothermal synthesis)原位生長在在鎳泡沫上,接著使用低壓電漿清潔機(plasma cleaner),以Ar、Ar/H2(95:5)和Ar/O2(95:5)作為工作氣體進行電漿後處理,探索不同電漿氣體對鎳鐵雙金屬有機框架進行表面改質在析氧反應(oxygen evolution reaction, OER)各方面性能表現的影響。由此開發的電催化劑在鹼性溶液(1 M KOH)中進行測試。結果表明,以Ar/H2(95:5)還原性氣體電漿處理明顯提高了RuCo/ANF的電催化活性,實現在電流密度10 mA/cm2下149 mV的過電位,這可能是由於氫自由基的摻入使得表面的氧化物被還原。接著利用電化學阻抗圖譜(EIS)和循環伏安法(CV)分析進行電化學量測,顯示出電荷轉移阻抗顯著降低以及電雙層電容明顯提升,分別證明電荷轉移加速和電化學表面積擴大。最後經由12小時的連續循環測試以評估所製備的電催化劑之耐久性,觀察到循環後經由摻氫電漿處理的電極過電位僅增加29 mV。此現象乃歸因於反應產生的氣泡會衝擊電極,導致電極材料本身劣化,但仍保持令人滿意的過電位可能是由於基材和MOF之間穩定的機械粘附,使活性位點得到充分利用。 | zh_TW |
dc.description.abstract | In this study, nickel-iron bimetallic organic frameworks were grown in-situ on nickel foam by the hydrothermal method. Then, Ar, Ar/H2(95:5) and Ar/O2(95:5) were used as working gases for plasma post-treatment to explore the effects of different plasma gases on the surface modification of nickel-iron bimetallic organic frameworks in all aspects of OER performance. The developed electrocatalysts perform oxygen evolution reaction in alkaline solution (1 M KOH) showing that plasma treatment with Ar/H2(95:5) gas significantly improved the electrocatalytic activity of NiFe-MOFs/NF, achieving an overpotential of 149 mV at a current density of 10 mA/cm2, attributing to the reduction of surface oxides due to the incorporation of hydrogen radicals. Electrochemical impedance spectroscopy (EIS) and cyclic voltammetry (CV) analysis showed that a great reduction in charge transfer impedance and a significant increase in electric double layer capacitance, proving the acceleration of charge transfer and the expansion of electrochemical surface area, respectively. Finally, the durability of the prepared electrocatalyst was evaluated by 12 h continuous cycle test. The overpotential of the electrode treated with hydrogen-containing plasma only increased by 29 mV after cycling. This phenomenon is attributed to bubbles generated by the reaction impacting the electrode, causing the electrode material to deteriorate itself. The satisfactory overpotential may be due to the stable mechanical adhesion between the substrate and the MOF, making the active sites be fully utilized. | en |
dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2023-08-09T16:32:05Z No. of bitstreams: 0 | en |
dc.description.provenance | Made available in DSpace on 2023-08-09T16:32:05Z (GMT). No. of bitstreams: 0 | en |
dc.description.tableofcontents | 致謝 i
摘要 ii Abstract iii 目錄 iv 圖目錄 vii 表目錄 xi 第一章 緒論 1 1.1 前言 1 1.2 研究動機 2 1.3 論文大綱 3 第二章 理論與文獻回顧 4 2.1 電催化水分解反應 4 2.1.1 析氫反應機制 6 2.1.2 析氧反應機制 7 2.1.3 起始電位與過電位 9 2.1.4 塔弗斜率 11 2.1.5 電化學活性表面積 13 2.2 電催化劑 14 2.2.1 活性位點 14 2.2.2 鎳基材料 14 2.2.3 鐵基材料 15 2.2.4 釕基材料 15 2.3 電漿 16 2.3.1 電漿基本概念 16 2.3.2 電漿原理 17 2.3.3 電漿中的碰撞 18 2.3.4 局部與非局部熱平衡電漿 21 2.3.5 低壓電漿與大氣電漿 22 2.3.6 電漿源 23 第三章 實驗方法與儀器介紹 27 3.1 實驗材料與儀器 27 3.2 實驗流程 30 3.2.1 基板的選擇 30 3.2.2 NF基板的預處理 30 3.2.3 製作鎳鐵雙金屬有機框架催化劑於鎳泡沫基材上 30 3.2.4 表面改質 31 3.3 分析與製程儀器設備 32 3.3.1 X射線光電子能譜儀(X-ray photoelectron spectroscopy, XPS) 32 3.3.2 X射線繞射分析儀(X-ray diffractometer, XRD) 34 3.3.3 掃描電子顯微鏡(Scanning Electron Microscopy, SEM) 36 3.3.4 接觸角測量儀(Contact Angle Meter) 38 3.3.5 電漿清潔機(Plasma Cleaner) 39 3.3.6 電化學工作站量測 42 第四章 結果與討論 46 4.1 水接觸角分析 46 4.2 表面型態與化學成分映射 48 4.3 表面化學元素組成分析 51 4.4 晶相分析 55 4.5 線性掃描伏安法及相應的塔弗斜率分析 56 4.6 電化學阻抗圖譜分析 58 4.7 循環伏安法與電雙層電容 60 4.8 耐久性量測 64 第五章 結論 65 第六章 附錄:低壓電漿改質鈷釕雙金屬析氫反應之電催化劑 66 6.1 摘要 66 6.2 實驗流程 66 6.3 結果與討論 68 6.3.1 表面型態與元素分布 68 6.3.2 水接觸角分析 71 6.3.3 表面化學型態 72 6.3.4 晶體結構分析 73 6.3.5 線性掃描伏安法與塔弗斜率 74 6.3.6 電化學阻抗圖譜分析 75 6.3.7 循環伏安法與電雙層電容值 77 6.3.8 耐久性量測 78 6.4 結論 80 參考文獻 81 個人期刊發表 93 | - |
dc.language.iso | zh_TW | - |
dc.title | 低壓電漿改質鎳鐵雙金屬析氧反應之電催化劑 | zh_TW |
dc.title | Low-pressure plasma modified nickel-iron bimetallic electrocatalysts for oxygen evolution reaction | en |
dc.type | Thesis | - |
dc.date.schoolyear | 111-2 | - |
dc.description.degree | 碩士 | - |
dc.contributor.oralexamcommittee | 陳奕君;羅世強;陳建甫 | zh_TW |
dc.contributor.oralexamcommittee | I-Chun Cheng;Shyh-Chyang Luo;Chien-Fu Chen | en |
dc.subject.keyword | 鎳鐵合金,金屬有機框架,低壓電漿,析氧反應,水熱合成法, | zh_TW |
dc.subject.keyword | nickel-iron alloys,metal organic framework,plasma,OER,hydrothermal synthesis, | en |
dc.relation.page | 93 | - |
dc.identifier.doi | 10.6342/NTU202301362 | - |
dc.rights.note | 同意授權(限校園內公開) | - |
dc.date.accepted | 2023-07-13 | - |
dc.contributor.author-college | 工學院 | - |
dc.contributor.author-dept | 應用力學研究所 | - |
顯示於系所單位: | 應用力學研究所 |
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