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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/87627完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 黃心豪 | zh_TW |
| dc.contributor.advisor | Hsin-Haou Huang | en |
| dc.contributor.author | 胡哲愷 | zh_TW |
| dc.contributor.author | Zhe-Kai Hu | en |
| dc.date.accessioned | 2023-06-20T16:26:43Z | - |
| dc.date.available | 2023-11-09 | - |
| dc.date.copyright | 2023-06-20 | - |
| dc.date.issued | 2023 | - |
| dc.date.submitted | 2023-02-14 | - |
| dc.identifier.citation | [1] J. Zhang, V. S. Chevali, H. Wang, and C.-H. Wang, "Current status of carbon fibre and carbon fibre composites recycling," Composites Part B: Engineering, vol. 193, p. 108053, 2020.
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/87627 | - |
| dc.description.abstract | 在這項研究中介紹了一種碳纖維回收方式，能夠將其製造成儲能設備以獲得更高的再利用價值。本研究利用濃硫酸進行碳纖維複合材料的回收作業並成功從中取得回收碳纖維，並且回收碳纖維的機械性能與初始碳纖維表現相似 (拉伸強度分別為322.4 MPa 和 321.2 MPa)；在電化學儲能機制的部分，回收碳纖維電極並不會因為本研究中所使用的回收方式產生影響。在比電容值的表現中，經過回收處理後的碳纖維表現有微幅上升(30.8 mF/g提升至42.7 mF/g)。
本研究將所取得之回收碳纖維結合改良的自動化局部高溫活化儀器(D70，600℃-70分鐘)及實驗室先前所研發的膠體電解質(Gel polymer)製作成超級電容，透過真空袋(PE)及環氧樹脂(Epoxy)進行多功能儲能複合材料的封裝。量測其最終成品的比電容值在5 mA/g的電流密度下，擁有最大比電容值3281 mF/g。 為了更符合實際應用層面，本研究亦針對了內部串疊進行研究。在將兩個單一元件進行內部串疊之後，其工作電位成功擴充至2 V並且將能量密度從1275.5 J/Kg提升至2500 J/Kg，達成提升儲能表現及工作電位的目的。最後將針對此多功能儲能複合材料進行機械性質測驗，透過施加不同大小的循環負載，測量其剛性的保留率，最後發現其在800 N的循環負載下，其材料剛性仍舊維持良好的表現。 | zh_TW |
| dc.description.abstract | In this study, we report a way to recycle carbon fibers and fabricate them into energy storage devices to create a new reuse method. First, by soaking the carbon fiber composite materials in sulfuric acid and it can obtain a recycled carbon fibers. The products based on recycled carbon fibers(RCF) showed similar mechanical performance to virgin carbon fibers-based products (tensile strengths are 322.4 MPa and 321.2 MPa , respectively); At energy storage mechanism, the recycled carbon fiber electrodes will not be affected by this recycled process. Moreover, the specific capacitance value of RCF was slightly increased from 30.8 mF/g to 42.7 mF/g.
Then, the activation of recycled carbon fiber was carried out by improved activation instrument (D70, 600°C-70 minutes). The gel electrolyte fabrication method which was developed by the our lab. Finally, packaged with the PE bag and epoxy resin for multifunctional energy storage composite. The specific capacitance value of the final product was 3281 mF/g at 5 mA/g of current density . In order to be more practical to the application, this research also studies the tandem stack method. After connecting two single circuit, the working potential was successfully expanded to 2 V and the energy density increased from 1275.5 J/Kg to 2500 J/Kg. It successfully increase the energy storage ability and working potential. Finally, the mechanical properties of this product will be measured by observed the stiffness retention ratio. Furthermore, the stiffness retention have great performance after 800 N cyclic loading test. | en |
| dc.description.provenance | Submitted by admin ntu (admin@lib.ntu.edu.tw) on 2023-06-20T16:26:43Z No. of bitstreams: 0 | en |
| dc.description.provenance | Made available in DSpace on 2023-06-20T16:26:43Z (GMT). No. of bitstreams: 0 | en |
| dc.description.tableofcontents | 論文口試委員會審定書 i
誌謝 ii 摘要 iii Abstract iv 目錄 v 圖目錄 viii 表目錄 xiii 第一章 簡介 1 1.1 動機 1 1.2 研究背景 2 1.3 研究目的 2 1.4 重要性與貢獻 3 1.5 名詞對照與符號說明 4 1.5.1 英文專有名詞與中文翻譯對照 4 1.5.2 符號說明表 8 第二章 文獻探討 10 2.1 碳纖維複合材料之回收及再利用 10 2.1.1 機械回收 10 2.1.2 熱回收 12 2.1.3 化學回收 14 2.2 超級電容、電容、電池比較 15 2.3 碳纖維活化方式 18 2.4 靜電紡絲分隔層和膠體電解質製備探討 20 2.5 超級電容內部串疊 22 2.6 碳纖維超級電容複合材料 24 第三章 研究方法 29 3.1 研究流程 29 3.2 實驗方法 30 3.2.1 電化學分析方法 30 3.2.2 材料分析方法 41 3.2.3 碳纖維複合材料回收方式 43 3.2.4 回收碳纖維電極複合材料力性測試 43 3.2.5 碳纖維電極活化方法 44 3.2.6 膠體電解質製備方法 46 3.2.7 碳纖維超級電容封裝 47 3.2.8 壽命檢測 47 3.2.9 碳纖維超級電容內部串疊實驗 47 3.2.10 多功能儲能複合材料機械性質分析 48 3.3 實驗儀器及設備 49 3.4 實驗藥品 50 第四章 研究結果 53 4.1 碳纖維複合材料回收實驗 53 4.1.1 回收碳纖維形貌 53 4.1.2 回收碳纖維複合材料的樹脂分解率 54 4.1.3 回收碳纖維SEM結果 55 4.1.4 回收碳纖維XRD結果 56 4.1.5 回收碳纖維FTIR結果 56 4.1.6 回收碳纖維複合材料機械性質測試結果 57 4.1.7 回收碳纖維複合材料電化學性質測試結果 60 4.2 自動化碳纖維電極活化機改良實驗 62 4.2.1 碳纖維活化參數改良設置 62 4.2.2 單束碳纖維活化碳纖維比電容值 63 4.2.3 碳纖維電極和膠體電解質適配性實驗 65 4.3 整合式多功能儲能複合材料 66 4.3.1 多功能儲能材料封裝製程 66 4.3.2 多功能儲能複合材料電化學特性 67 4.3.3 壽命檢測 73 4.3.4 內部串疊多功能儲能複合材料實驗 75 4.3.5 與前人之性能比較分析 79 4.3.6 多功能儲能複合材料機械性質檢測 80 第五章 討論 82 5.1 回收碳纖維實驗討論 82 5.1.1 回收機制探討 82 5.1.2 回收碳纖維清洗方式探討 83 5.2 VARTM封裝製程討論 85 5.3 內部串疊多功能儲能複合材料討論 86 5.3.1 內部串疊超級電容的工作電位窗探討 86 5.3.2 內部串疊超級電容比電容值下降討論 87 第六章 結論與未來展望 88 6.1 結論 88 6.2 未來展望 89 第七章 參考文獻 90 | - |
| dc.language.iso | zh_TW | - |
| dc.title | 以回收碳纖維電極實現多功能儲能複合材料之可行性研究 | zh_TW |
| dc.title | On realization of multifunctional energy storage composite materials based on recycled carbon fiber electrodes | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 111-1 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.coadvisor | 陳洵毅 | zh_TW |
| dc.contributor.coadvisor | Hsun-Yi Chen | en |
| dc.contributor.oralexamcommittee | 張豐丞;宋家驥;黃勝翊 | zh_TW |
| dc.contributor.oralexamcommittee | Feng-Cheng Chang;Chia-Chi Sung;hseng-ji Huang | en |
| dc.subject.keyword | 碳纖維複合材料回收,碳纖維活化,多功能儲能複合材料,內部串疊,超級電容, | zh_TW |
| dc.subject.keyword | CFRP recycled,activated carbon fiber,multifunctional energy storage composite,tandem stack,supercapacitors, | en |
| dc.relation.page | 99 | - |
| dc.identifier.doi | 10.6342/NTU202300413 | - |
| dc.rights.note | 未授權 | - |
| dc.date.accepted | 2023-02-15 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 工程科學及海洋工程學系 | - |
| 顯示於系所單位： | 工程科學及海洋工程學系 | |
文件中的檔案：
| 檔案 | 大小 | 格式 | |
|---|---|---|---|
| ntu-111-1.pdf 目前未授權公開取用 | 6.82 MB | Adobe PDF |
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