請用此 Handle URI 來引用此文件：
http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/85390完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 羅世強 | zh_TW |
| dc.contributor.advisor | Shyh-Chyang Luo | en |
| dc.contributor.author | 胡采甯 | zh_TW |
| dc.contributor.author | Tsai-Ning Hu | en |
| dc.date.accessioned | 2023-03-19T23:16:03Z | - |
| dc.date.available | 2023-12-26 | - |
| dc.date.copyright | 2022-08-02 | - |
| dc.date.issued | 2022 | - |
| dc.date.submitted | 2002-01-01 | - |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/85390 | - |
| dc.description.abstract | 隨著工業的發展和現代科技的進步，世界面臨著水污染和水資源匱乏的問題。近年來，太陽能蒸汽生成、太陽能純化水因其不會額外耗能的優點而備受關注。不同於傳統的淨水方式，其利用太陽能轉化為熱能，通過蒸發後獲得純水，在這個過程中，所有的鹽和雜質都會從蒸汽中分離，蒸汽被冷凝成純水並收集。水純化過程中不會產生污染物、脫鹽膜可以重複使用等優勢，提供了環境友善的水純化方法。純化薄膜或脫鹽膜必須滿足兩項主要性質：1.可吸收太陽光並轉化成熱能，提供水蒸發的吸收熱。2.多孔隙、具有連續的微孔結構，提供水分子藉由毛細現象向上傳輸的途徑。另外，熱能須集中在表面，避免熱傳導分散到膜內及底下的水，以達到最高的水蒸發、純化水效率。在此研究中，我們利用三氧化二鈦(Ti2O3)及羥基官能化聚(3,4-亞乙基二氧噻吩) (PEDOT-OH)作為光熱轉換材料，並在親水的官能化聚四氟乙烯(polytetrafluoroethylene, PTFE)過濾薄膜上合成原位生長(in-situ)的金屬有機骨架(metal-organic framework, MOF) CAU-10-H，藉由PTFE基材的孔洞吸收下方的鹽水，再經由MOF中的結構孔洞及晶隙傳輸至吸光層，吸收熱能並蒸發。研究中，探討了PEDOT-OH和不同比例的PEDOT-OH包覆Ti2O3奈米複合材料的光吸收量及光熱轉換效果，而重量比例1:1的PEDOT-OH包覆Ti2O3複合材料能良好塗佈在MOF薄膜上又具有最高的吸光量、光熱轉換量。同時，我們合成不同晶體厚度的in-situ CAU-10-H，晶體厚度不但影響水傳輸路徑長短，也會造成絕熱效果的改變。研究結果以厚度13 μm的CAU-10-H達到兩種機制的平衡，其塗佈薄膜具有最高的水蒸發速率，達2.17 kg.m-2.h-1，而光熱轉換要率達98%。有別於其他太陽能純化水的發表，緻密in-situ CAU-10-H 的低熱傳導率有利於熱能集中在表面，而此裝置中的脫鹽膜也無須額外的隔熱層以避免熱能分散至水體。結果證明，PEDOT-OH包覆Ti2O3奈米複合材料塗佈CAU-10-H薄膜在太陽能蒸氣生成及海水淡化等永續能源領域具有巨大的優勢。 | zh_TW |
| dc.description.abstract | With the advancement of modern technology, the world is facing the issues of water pollution and scarcity of water resources. Solar steam generation and desalination have attracted much attention due to their intrinsic advantages. In the purification process, salts and impurities are separated from the steam, which is condensed into pure water and collected. Moreover, no pollutants are produced during the water purification process. Desalination membranes are also repeatable, providing an environmentally friendly water purification method. In this research, we successfully fabricated titanium trioxide coated with poly(hydroxymethyl EDOT) (Ti2O3@PEDOT-OH) nanocomposites as a photothermal conversion material, and well synthesized in-situ metal-organic framework (MOF), CAU-10-H based membranes. Ti2O3@PEDOT-OH coating 13 μm CAU-10-H self-floating on the water achieves the highest water evaporation rate of 2.17 kg.m-2.h-1 with an efficient thermal insulating ability and an evaporation efficiency of 98%. Also, the ion concentrations of collected water tremendously decrease and are much lower than drinkable water standards by WHO. The results have shown that Ti2O3@PEDOT-OH nanocomposites on CAU-10-H films possess excellent potential in the fields of sustainable energy such as solar steam generation and seawater desalination. | en |
| dc.description.provenance | Made available in DSpace on 2023-03-19T23:16:03Z (GMT). No. of bitstreams: 1 U0001-2107202216001100.pdf: 4481969 bytes, checksum: fa8be3df84ef32ab8fc25bf6f5b9b12b (MD5) Previous issue date: 2022 | en |
| dc.description.tableofcontents | 誌謝 i 中文摘要 ii ABSTRACT iii CONTENTS iv LIST OF FIGURES vii LIST OF TABLES xi Chapter 1 Introduction 1 1.1 Desalination Materials 3 1.2 Metal-organic Framework for Solar Desalination 5 1.3 Conducting Polymer Composite as Solar Absorber 6 1.4 Research Goal 7 Chapter 2 Materials and Methods 9 2.1 Materials and Instruments 9 2.1.1 Materials and Chemicals 9 2.1.2 Instruments and Measurements 10 2.2 Nanoparticles and Nanocomposites Fabrication 10 2.2.1 Ball-milling Process of Ti2O3 Nanoparticles 10 2.2.2 Synthesis of PEDOT-OH and Ti2O3@PEDOT-OH 11 2.3 Synthesis of CAU-10-H 12 2.3.1 Synthesis of CAU-10-H in Powder Form 12 2.3.2 Synthesis of in-situ CAU-10-H Membranes 12 2.4 Coating Composites on CAU-10-H Membranes 13 2.5 Characterization 14 2.5.1 Scanning Electron Microscope (SEM) 14 2.5.2 UV-VIS Spectrophotometer 14 2.5.3 Contact Angle Measurements 14 2.5.4 X-ray Powder Diffraction (XRD) 14 2.5.5 X-ray Diffraction (XRD) 15 2.5.6 Inductively Coupled Plasma Mass Spectrometry (ICP-MS) 15 2.6 Evaporation and Purification Tests 15 2.6.1 Device Setup of Evaporation Tests 15 2.6.2 Device to Collect Condensed Water 16 Chapter 3 Result and Discussion 18 3.1 Photothermal Composites 18 3.1.1 Comparison between PEDOT-OH and Ti2O3@PEDOT-OH 18 3.1.2 Comparison between As-received Ti2O3 and Ti2O3 Nanoparticles 20 3.1.3 Ti2O3@PEDOT-OH Nanocomposites with Different Ratios 22 3.1.4 The Dispersity of Nanocomposites 27 3.2 CAU-10-H Membranes 29 3.2.1 Surface Morphology and Thickness 29 3.2.2 Crystal Analysis 34 3.3 Surface Analysis of Coating Membranes 35 3.3.1 Contact Angle 35 3.3.2 Surface and Cross-Section Morphology 37 3.3.3 Device Setup 38 3.4 Solar Desalination Tests 40 3.4.1 Photothermal Capacity 40 3.4.2 Evaporation Tests 43 3.4.3 Evaporation Efficiency 47 3.4.4 Practical Application and Purification Analysis 48 Chapter 4 Conclusion 50 Chapter 5 Future Work 51 REFERENCE 52 | - |
| dc.language.iso | en | - |
| dc.subject | 太陽純化水 | zh_TW |
| dc.subject | 金屬有機骨架 | zh_TW |
| dc.subject | 太陽純化水 | zh_TW |
| dc.subject | 導電高分子 | zh_TW |
| dc.subject | 金屬有機骨架 | zh_TW |
| dc.subject | 導電高分子 | zh_TW |
| dc.subject | Conducting polymer | en |
| dc.subject | PEDOT | en |
| dc.subject | metal-organic framework | en |
| dc.subject | solar steam generation | en |
| dc.subject | solar desalination | en |
| dc.subject | metal-organic framework | en |
| dc.subject | PEDOT | en |
| dc.subject | Conducting polymer | en |
| dc.subject | solar steam generation | en |
| dc.subject | solar desalination | en |
| dc.title | 導電高分子奈米複合材料塗佈金屬有機骨架薄膜用於太陽能水純化 | zh_TW |
| dc.title | Metal-Organic Framework (MOF) Based Membranes Coated with Conducting Polymer Nanocomposites for Solar Steam Generation | en |
| dc.type | Thesis | - |
| dc.date.schoolyear | 110-2 | - |
| dc.description.degree | 碩士 | - |
| dc.contributor.oralexamcommittee | 康敦彥;陳建甫 | zh_TW |
| dc.contributor.oralexamcommittee | Dun-Yen Kang;Chien-Fu Chen | en |
| dc.subject.keyword | 導電高分子,太陽純化水,金屬有機骨架, | zh_TW |
| dc.subject.keyword | Conducting polymer,PEDOT,metal-organic framework,solar steam generation,solar desalination, | en |
| dc.relation.page | 58 | - |
| dc.identifier.doi | 10.6342/NTU202201614 | - |
| dc.rights.note | 同意授權(全球公開) | - |
| dc.date.accepted | 2022-07-25 | - |
| dc.contributor.author-college | 工學院 | - |
| dc.contributor.author-dept | 材料科學與工程學系 | - |
| dc.date.embargo-lift | 2024-07-30 | - |
| 顯示於系所單位： | 材料科學與工程學系 | |
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