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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/80918完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 宋家驥(Chia-Chi Sung) | |
| dc.contributor.author | Chun-Hao Chang | en |
| dc.contributor.author | 張君豪 | zh_TW |
| dc.date.accessioned | 2022-11-24T03:21:54Z | - |
| dc.date.available | 2021-11-08 | |
| dc.date.available | 2022-11-24T03:21:54Z | - |
| dc.date.copyright | 2021-11-08 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-09-17 | |
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Gao, “Photoemission Studies on the Environmental Stability of Thermal Evaporated MAPbI3 Thin Films and MAPbBr3 Single Crystals,” Energies. 14(7): p. 2005. 2021. 106. W. Huang, J. S. Manser, P. V. Kamat, and S. Ptasinska, “Evolution of chemical composition, morphology, and photovoltaic efficiency of CH3NH3PbI3 perovskite under ambient conditions,” Chemistry of Materials. 28(1): p. 303-311. 2016. 107. S. Rondon and P. M. Sherwood, “Core level and valence band spectra of PbO by XPS,” Surface Science Spectra. 5(2): p. 97-103. 1998. | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/80918 | - |
| dc.description.abstract | 高效率鈣鈦礦太陽能電池 (PSCs) 需要使用可控制氣氛的充氮手套箱中製造。 本研究我們使用預熱 MAPbI3 前體液溫度，並在相對濕度 (60-70%) 與電池有效活性面積 ≈ 0.09 cm2 的反式混合鹵化物 CH3NH3PbI3 PSCs ，探討元件性能與鈣鈦礦薄膜之間的相關性。我們研究利用一種用於生產高質量的有機-無機鈣鈦礦薄膜和太陽能電池，並耐濕且通用的製造方法。由於採用了預熱方法，所以大大抑制了濕度的影響。使用預熱MAPbI3 前驅液可以增加對可見光波長的吸收，研究發現當結構中存在少量 H2O 時，它可以填充 MAPbI3 薄膜中的晶界； XRD分析表明改變預熱溫度可以減少中間相。使用簡單的鈣鈦礦前驅體預熱方法，在大氣環境製程 PSCs 的光電轉換效率 (PCE) 達到 7.72%。 第二部分我們將預熱鈣鈦礦前驅液90 oC，進行不同退火時間處理，來改變鈣鈦礦晶粒尺寸，有助於在環境大氣氣氛中，ITO基底上獲得均勻穩定的鈣鈦礦薄膜。最終我們得出結論，這些結果將在大氣條件下實現更好的 MAPbI3 薄膜均勻性，並提供了一種可行的方法。這一研究努力是為了理解 MAPbI3 薄膜的物理特性，並揭開在大氣環境中製備 MAPbI3 薄膜，並進行進一步的元件開發，獲得在大氣條件下製造的高效鈣鈦礦太陽能電池，而無需具有良好穩定性的有機空穴及導電材料。最終我們獲得太陽光電轉換效率為10.7%。 | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-24T03:21:54Z (GMT). No. of bitstreams: 1 U0001-1609202122073600.pdf: 8496889 bytes, checksum: 5c3e9ea7e06465810af6610165dd2a8f (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | 誌謝 i 中文摘要 ii ABSTRACT iii CONTENTS v LIST OF FIGURES viii LIST OF TABLES xii Chapter 1 Introduction 1 1.1 Motivation and Objective 4 Chapter 2 The Formats of the Thesis 5 2.1 Evolution and Principles of Solar Cells 5 2.1.1 First generation solar cells 6 2.1.2 Second generation solar cells 7 2.1.3 Third generation solar cells 9 2.1.4 Characteristics of Solar Cells 11 2.1.5 Current-Voltage measurements 13 2.2 Fundamentals of Perovskite Solar Cells 15 2.2.1 The development from Dye-Sensitized Solar Cells (DSSCs) 15 2.2.2 Organometal halide perovskites and working mechanism 20 2.3 Causes of Instability in Perovskite Solar Cells Research 21 2.3.1 The Influence of water into the perovskite precursor 22 2.3.2 The Relative humidity on the preparation of perovskite films 23 Chapter 3 Experimental procedure 25 3.1 Experiment process 26 3.1.1 Pre-treatment of ITO glass substrate 28 3.1.2 Hole transport layer 28 3.1.3 Active layer 29 3.1.4 Electron transport layer 29 3.1.5 Sputtering Pt electrode layer 29 3.2 Experimental chemicals 30 3.3 Experimental equipment and Sample characterization 31 3.3.1 Oxygen plasma treatment 31 3.3.2 Field-emission scanning electron microscope 32 3.3.3 X-Ray Diffraction 34 3.3.4 XPS photoelectron spectroscopy 36 3.3.5 UV-VIS Spectrophotometry 38 3.3.6 PL Spectrophotometry 40 3.3.7 I-V Curve Current density-voltage characteristics 42 Chapter 4 Results and Discussion 44 4.1 Different preheating precursor temperatures affects the MAPbI3 films 44 4.1.1 Effect of preheating temperature on perovskite films morphology 44 4.1.2 The influence of preheating temperature on the optical properties of perovskite films 51 4.1.3 I–V characteristics of the solar cells stored in different preheating temperatures 55 4.2 Different annealing time affects the MAPbI3 films 58 4.2.1 Effect of annealing time on perovskite films morphology 58 4.2.2 The influence of annealing time on the optical properties of perovskite films 65 4.2.3 Using XPS analysis to influence MAPbI3 films at different annealing time 67 4.2.4 I–V characteristics of the solar cells stored in different annealing time 83 Chapter 5 Conclusion and Future work 86 REFERENCE 88 | |
| dc.language.iso | en | |
| dc.subject | 大氣製程 | zh_TW |
| dc.subject | 鈣鈦礦 | zh_TW |
| dc.subject | 太陽能電池 | zh_TW |
| dc.subject | 預熱溫度 | zh_TW |
| dc.subject | 光電轉換效率 | zh_TW |
| dc.subject | 高濕度 | zh_TW |
| dc.subject | MAPbI3 | en |
| dc.subject | High Humidity | en |
| dc.subject | Preheating | en |
| dc.subject | Air preparation | en |
| dc.subject | Perovskite solar cells | en |
| dc.title | 預熱前驅液及改變退火時間在大氣下製備鈣鈦礦太陽能電池 | zh_TW |
| dc.title | "Pre-heating and annealing time for Ambient-Air-Processed, Phase-Stable MAPbI3 in Perovskite Solar Cells" | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 博士 | |
| dc.contributor.oralexamcommittee | 李岳聯(Hsin-Tsai Liu),張合(Chih-Yang Tseng),蔡孟霖,許春耀 | |
| dc.subject.keyword | 鈣鈦礦,太陽能電池,預熱溫度,光電轉換效率,高濕度,大氣製程, | zh_TW |
| dc.subject.keyword | Air preparation,Perovskite solar cells,MAPbI3,Preheating,High Humidity, | en |
| dc.relation.page | 95 | |
| dc.identifier.doi | 10.6342/NTU202103222 | |
| dc.rights.note | 同意授權(限校園內公開) | |
| dc.date.accepted | 2021-09-22 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 工程科學及海洋工程學研究所 | zh_TW |
| 顯示於系所單位： | 工程科學及海洋工程學系 | |
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