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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 駱尚廉(Shang-Lien Lo) | |
| dc.contributor.author | Ho-Hsi Yang | en |
| dc.contributor.author | 楊和熙 | zh_TW |
| dc.date.accessioned | 2022-11-23T09:11:32Z | - |
| dc.date.available | 2021-08-13 | |
| dc.date.available | 2022-11-23T09:11:32Z | - |
| dc.date.copyright | 2021-08-13 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-08-11 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/79792 | - |
| dc.description.abstract | " 過氧化氫 (Hydrogen peroxide, H₂O₂) 與異丙醇 (Isopropanol, IPA) 大量用於半導體製程中，且為了不額外產生污泥與擴大處理設備，提出在原有的設備中加裝超聲波，本研究為在連續流反應器中以超聲波搭配臭氧 (US/O₃) 去除過氧化氫與異丙醇，作為未來放大規模之前導實驗的參考。 本研究使用頻率20 kHz與功率500 W的超聲波，以批次實驗研究降解過氧化氫與異丙醇之反應動力學與自由基反應，探討在US/O₃連續流系統中進流量、氨氮、pH值、過氧化氫及異丙醇的初始濃度對去除率之影響，並觀察系統中氨氮變化與異丙醇之副產物，最終將US/O₃連續流系統應用在實場廢水中。 根據聲化學中空蝕現象 (Acoustic cavitation)，本系統降解過氧化氫與異丙醇的主要反應機制，過氧化氫為空蝕氣泡中熱裂解，異丙醇為氣泡的液氣界面處被氫氧自由基氧化。結果發現在鹼性環境中氨氮透過鹽析作用 (Salting out) 使過氧化氫有利於進入空蝕氣泡中熱裂解，產生更多氫氧自由基，在pH值為10中247 ppm的氨氮比0 ppm的氨氮，其過氧化氫與異丙醇去除率提升41.81%與36.74%，結果相比過去的研究，能更有效去除水中過氧化氫。將本系統應用在半導體廠廢水，在水力停留時間為33分鐘時，廢水中過氧化氫與異丙醇之去除率為80%及70%，證明本研究成功建立US/O₃連續流系統處理實廠廢水。" | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-23T09:11:32Z (GMT). No. of bitstreams: 1 U0001-0908202123560300.pdf: 8882201 bytes, checksum: 5f8a4ff891681261afcb2a03340d791d (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | 摘要 i Abstract ii 目錄 iii 圖目錄 viii 表目錄 x 第一章 緒論 1 1.1 研究緣起 1 1.2 研究目的 2 1.3 研究內容 2 第二章 文獻回顧 3 2.1 異丙醇 3 2.1.1 異丙醇之性質與應用 3 2.1.2 異丙醇之毒性 4 2.2過氧化氫 5 2.2.1過氧化氫之性質與應用 5 2.2.2過氧化氫之毒性 6 2.3異丙醇及過氧化氫之處理技術 7 2.3.1異丙醇之處理方法 8 2.3.2過氧化氫之處理 11 2.4 超聲波處理 13 2.4.1 聲音空蝕原理及反應機制 13 2.4.2 超聲波的應用 16 2.4.3 超聲波結合過氧化氫與臭氧系統 19 2.4.4 超聲波的操作參數 22 2.4.5 超聲波連續流系統 27 2.5 自由基鑑定方法 29 第三章 實驗步驟與方法 31 3.1 實驗內容與架構 31 3.2 實驗材料及設備 33 3.2.1 實驗藥品 33 3.2.2 實驗設備 35 3.3 儀器分析方法 37 3.3.1 氣相層析儀 37 3.3.2 分光光度計 39 3.3.3 離子層析儀 41 3.3.4 高效液相層析儀 42 3.4 實驗步驟及方法 42 3.4.1 去除水中過氧化氫與異丙醇實驗 42 3.4.2 批次實驗反應動力學 44 3.4.3 連續流實驗反應動力學 45 3.4.4 評估連續流中超聲波的結合效率 46 3.4.5 自由基鑑定實驗 46 3.4.6 實驗品質管制 47 第四章 結果與討論 48 4.1 批次超聲波系統實驗 48 4.1.1 一階反應動力學 48 4.1.2 自由基鑑定 50 4.2 連續流系統背景實驗 52 4.2.1 水中臭氧濃度 52 4.2.2 單獨攪拌實驗 53 4.2.3 曝氣實驗 54 4.2.4 不同氨氮來源 55 4.2.5 可行性試驗 57 4.3 超聲波結合臭氧 (US/O₃) 連續流系統 60 4.3.1 進流量對過氧化氫及異丙醇之去除率影響 60 4.3.2 氨氮濃度對過氧化氫及異丙醇之去除率影響 62 4.3.3 初始pH值對過氧化氫及異丙醇之去除率影響 65 4.3.4 鹽析作用對過氧化氫及異丙醇之去除率影響 67 4.3.5 初始過氧化氫濃度對過氧化氫及異丙醇之去除率影響 69 4.3.6 初始異丙醇濃度對過氧化氫及異丙醇之去除率影響 71 4.3.7 在US/O₃連續流系統中氨氮的變化 73 4.3.8 在US/O₃連續流系統中異丙醇之副產物分析 75 4.3.9 在US/O₃連續流系統中過氧化氫及異丙醇之降解反應機制 77 4.4 實廠廢水分析結果 79 4.4.1 在US/O₃連續流系統應用在實廠廢水 79 4.4.2 以不同流量去除實廠廢水中過氧化氫與異丙醇 80 4.4.3 在US/O₃連續流系統之實廠廢水中氨氮的變化 81 4.4.4 在US/O₃連續流系統之實廠廢水中異丙醇副產物分析 82 第五章 結論與建議 83 5.1 結論 83 5.2 建議 85 參考文獻 86 附錄 103 | |
| dc.language.iso | zh-TW | |
| dc.subject | 氫氧自由基 | zh_TW |
| dc.subject | 連續流 | zh_TW |
| dc.subject | 過氧化氫 | zh_TW |
| dc.subject | 異丙醇 | zh_TW |
| dc.subject | 超聲波 | zh_TW |
| dc.subject | 氨氮 | zh_TW |
| dc.subject | 鹽析 | zh_TW |
| dc.subject | 熱裂解 | zh_TW |
| dc.subject | ultrasound | en |
| dc.subject | salting out | en |
| dc.subject | continuous flow reactor | en |
| dc.subject | hydrogen peroxide | en |
| dc.subject | isopropanol | en |
| dc.subject | ammonia nitrogen | en |
| dc.subject | hydroxyl radicals | en |
| dc.subject | pyrolysis | en |
| dc.title | 以超聲波連續流裝置同時去除水中異丙醇與過氧化氫之研究 | zh_TW |
| dc.title | Simultaneously Removal of Isopropanol and H₂O₂ from Wastewater by Ultrasound in Continuous Reactor | en |
| dc.date.schoolyear | 109-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 劉雅瑄(Hsin-Tsai Liu),胡景堯(Chih-Yang Tseng),劉于榕 | |
| dc.subject.keyword | 連續流,過氧化氫,異丙醇,超聲波,氨氮,鹽析,熱裂解,氫氧自由基, | zh_TW |
| dc.subject.keyword | continuous flow reactor,hydrogen peroxide,isopropanol,ultrasound,ammonia nitrogen,salting out,pyrolysis,hydroxyl radicals, | en |
| dc.relation.page | 127 | |
| dc.identifier.doi | 10.6342/NTU202102233 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2021-08-12 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 環境工程學研究所 | zh_TW |
| 顯示於系所單位： | 環境工程學研究所 | |
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