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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 童世煌(Shih-Huang Tung) | |
| dc.contributor.author | Dai-Hua Jiang | en |
| dc.contributor.author | 江岱樺 | zh_TW |
| dc.date.accessioned | 2022-11-23T08:57:51Z | - |
| dc.date.available | 2021-10-04 | |
| dc.date.available | 2022-11-23T08:57:51Z | - |
| dc.date.copyright | 2021-10-04 | |
| dc.date.issued | 2021 | |
| dc.date.submitted | 2021-10-01 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/79308 | - |
| dc.description.abstract | "本研究本論文主要突出三個方面:(1)新穎的彈性導電電極製備與柔性發光二極體應用◦ (2)簡易高亮度且多光色聚芴基元件之製備◦ (3)一鍋法合成聚芴基軟硬雙嵌鏈段共聚物與高量子效率之柔性按壓元件展示◦首先於第二章中，證明了銅/銀雙核殼層結構之奈米纖維膜電極具有良好彈性和導電性且可應用於柔性聚芴基發光二極體。接著於第三章中，展示了高導電與彈性聚氨酯奈米銀線電極優越穩定性，並成功展示於按壓元件上，其擁有相當高穩定性◦第四章提出聚芴基軟硬雙嵌鏈段共聚物具有展現良好拉伸性以及熒光性能的潛力，並可以簡易透過聚芴基混摻鈣鈦礦藉以螢光轉換效應達到多種光色變化。最後在第五章節中，開發出簡易的一鍋法合成，並設計出一系列的聚芴基共軛高分子，如: 聚（9,9-二-正己基-2,7-芴）-嵌段-聚(ε-癸内酯) (PFN18-b-PDLn)，利用嵌段共聚物之特性，結合軟鏈段聚(ε-癸内酯)與硬鏈段聚（9,9-二-正己基-2,7-芴）之功能性，探討其不同比例下的柔性發光二極體元件性能，其外部量子效率是聚芴高分子的六倍，且元件可以承受來回0-20%的應變300次下，性能沒有明顯的下降。綜上論述，作者成功研發出新穎導電彈性電極與聚芴嵌段共聚物的一鍋法合成，並成功的展示此軟硬嵌段共聚物擁較高的潛力應用於發光二極體，不只解決了穿戴式元件的柔性與性能之問題，更大大提升了工業量產化的可能性，在這種便捷智能合成和優越元件性能條件下，相信未來在穿戴式電子元件及光電材料等相關領域，具相當大的發展潛力。" | zh_TW |
| dc.description.provenance | Made available in DSpace on 2022-11-23T08:57:51Z (GMT). No. of bitstreams: 1 U0001-2709202110561700.pdf: 11744122 bytes, checksum: 96463f076f614ebb5d3d586862e94d99 (MD5) Previous issue date: 2021 | en |
| dc.description.tableofcontents | "Acknowledgements i Chinese Abstract ii English Abstract iii Contents iv List of Figures vi List of Tables xi List of Schemes xii Chapter 1 General Introduction 1 1.1 Fundamental Principle of Light-Emitting Diode (LED) 2 1.1.1 The basic light-emitting principle of LED 2 1.2.2 Evolution of polymer light-emitting diode (PLED) 7 1.2.3 Current issues of polymer electroluminescent materials 10 1.2 Conjugated Polymers on LED 12 1.3 Polyfluorene-Based (PF-based) Conjugated Block Copolymers (BCPs) 15 1.4 Synthesis of PF-Based Conjugated BCPs 20 1.4.1 The macroinitiator method 21 1.4.2 The coupling method 22 1.4.3 The LED applications of PF-based conjugated BCPs 23 1.5 Objective and Outline of the Dissertation 26 Chapter 2 Facile Preparation of Cu/Ag Core/Shell Nanofiber as High Flexible Transparent Conductive Electrodes for Polyfluorene Light-Emitting Diode Devices 33 2.1 Introduction 34 2.2 Experimental Section 37 2.2.1 Material 37 2.2.2 Characterization 37 2.2.3 Preparation of CuAc2/PVP-NFs 38 2.2.4 Preparation of Cu-NFs by the reduction-oxidation heating method 38 2.2.5 Preparation of Cu/Ag core/shell NFs from Ag electroless deposition 39 2.2.6 Fabrication of polyfluorene light-emitting diode devices 39 2.3 Results and Discussion 40 2.3.1 NF film morphologies and fabrications 40 2.3.2 Sheet resistance (Rs) and transmittance (T) of NFs 46 2.3.3 Performance of PF-based light-emitting diode devices 51 2.4 Conclusions 53 Chapter 3 Facile Fabrication of Stretchable Touch Responsive Light-Emitting Diodes through Using Robust Stretchable Composite Electrodes 55 3.1 Introduction 56 3.2 Experimental Section 58 3.2.1. Materials 58 3.2.2 Composite electrode fabrication (PDMS, NOA63, and PU) 58 3.2.3 Stretchable LED fabrication on PU substrate (PU/PEDOT:PSS-PEO/PVP/CsPbBr3-PEO-PVP/PU-AgNWs) 59 3.2.4 LED Measurement 59 3.3 Results and Discussion 61 3.4 Conclusion 75 Chapter 4 Light Down-Converter Based on the Blending of Polyfluorene Block Copolymers with Perovskite through Electrospinning 77 4.1 Introduction 78 4.2 Experimental Section 81 4.2.1 Material 81 4.2.2 Characterization 81 4.2.3. Synthesis of the ethynyl end-functionalized polyfluorene 83 4.2.4. Synthesis of the azido-terminated poly (n-butyl acrylate) 84 4.2.5. Synthesis of the PFN-b-PBA block copolymer 85 4.2.6. Synthesis of the CsPbX3 (X = Cl, Br, I) 86 4.2.7. Preparation of the electrospinning of CsPbBr3 QDs/polymer NFs 87 4.3 Results and Discussion 88 4.3.1 Synthesis and structure characterization of PFN-b-PBA BCPs 88 4.3.2 The physical and optical properties of the PFN-b-PBA thin films 92 4.3.3 Morphologies and stretchable performance of the PFN-b-PBA thin films 95 4.3.4 The color-tunable properties of light-emitting diodes 97 4.4 Conclusion 99 Chapter 5 Smart Synthesis of Polyfluorene-Based Block Copolymers Accelerates Design and Fabrication of Flexible Light-Emitting Diode Devices 101 5.1 Introduction 102 5.2 Experimental Section 105 5.2.1 Material 105 5.2.2 Characterization 105 5.2.3 Arrhenius formula simulation of the binding energy 108 5.2.4 The time decay curve fitting by an exponential function 108 5.2.5 Synthesis of PF-based block copolymers with ring-opening polymerization monomer through a smart one-pot procedure 108 5.2.6 Touch-responsive light-emitting diodes fabrication 110 5.3 Results and Discussion 111 5.3.1 Synthesis and structure characterization of PFN-b-PDL BCPs 111 5.3.2 The Physical and Optical Properties of the PFN-b-PDL Thin Films 126 5.3.3 The correlation between PLQY and EBE 131 5.3.4 The performance of stretchable touch-responsive light-emitting diode 134 5.4 Conclusion 143 Chapter 6 Conclusions 145 References: 151 Publication Lists: 167 " | |
| dc.language.iso | en | |
| dc.title | 聚芴基共軛高分子在拉伸發光二極體元件之應用 | zh_TW |
| dc.title | Flexible Light-Emitting Diode Application of Polyfluorene-Based Conjugated Polymers | en |
| dc.date.schoolyear | 110-1 | |
| dc.description.degree | 博士 | |
| dc.contributor.author-orcid | 0000-0002-6090-8788 | |
| dc.contributor.advisor-orcid | 童世煌(0000-0002-6787-4955) | |
| dc.contributor.coadvisor | 佐藤敏文(Toshifumi Satoh),郭霽慶(Chi-Ching Kuo) | |
| dc.contributor.coadvisor-orcid | 佐藤敏文(0000-0001-5449-9642) | |
| dc.contributor.oralexamcommittee | 鄭如忠(Hsin-Tsai Liu),闕居振(Chih-Yang Tseng),林群哲 | |
| dc.subject.keyword | 聚芴高分子,雙嵌段共聚高分子,一鍋法合成,發光二極體,柔性穿戴式元件, | zh_TW |
| dc.subject.keyword | polyfluorene,block copolymer,one-pot synthesis,light-emitting diode,flexible wearable device, | en |
| dc.relation.page | 169 | |
| dc.identifier.doi | 10.6342/NTU202103384 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2021-10-01 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 高分子科學與工程學研究所 | zh_TW |
| 顯示於系所單位： | 高分子科學與工程學研究所 | |
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