請用此 Handle URI 來引用此文件：
http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78730完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳建彰(Jian-Zhang Chen) | |
| dc.contributor.author | TE-EN LI | en |
| dc.contributor.author | 力得恩 | zh_TW |
| dc.date.accessioned | 2021-07-11T15:15:15Z | - |
| dc.date.available | 2022-07-31 | |
| dc.date.copyright | 2019-07-31 | |
| dc.date.issued | 2019 | |
| dc.date.submitted | 2019-07-26 | |
| dc.identifier.citation | [1] W. Hicks, 'Claims for solar cell efficiency put to test at NREL,' ed: Phys. org, 2016.
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78730 | - |
| dc.description.abstract | 本研究中使用表面擴散式介電質放電電漿(SDDBD)以及氬氣介電質放電噴射電漿(Argon DBD jet)對導電高分子聚合物PEDOT:PSS進行表面處理，並進行材料分析，SDDBD所處理之PEDOT:PSS並用於反結構(Inverted structure)鈣鈦礦太陽能電池的電洞傳輸層。
實驗一的部分是透過表面擴散式介電質放電電漿(SDDBD)進行PEDOT:PSS的處理。電漿在介電質及鐵網之間產生後，擴散至PEDOT:PSS表面，和PEDOT:PSS反應。處理後之PEDOT:PSS並應用於反結構鈣鈦礦太陽能電池的電洞傳輸層(Hole transport layer)。由於其SDDBD可攜式的特性，SDDBD電漿系統是置入充滿氮氣的手套箱內操作。隨著SDDBD處理時間的增加，PEDOT：PSS的電阻率隨時間先降低然後增加。X射線光電子能譜（XPS）之S2p結合能峰面積比的變化顯示SDDBD處理可以移除表面過量的PSS並改變PEDOT與PSS的比例，從而改變PEDOT：PSS的電阻率，而其功函數也可能隨之改變。當此電漿處理的PEDOT:PSS作為反結構鈣鈦礦太陽能電池(Perovskite solar cell, PSC)之電洞傳輸層，可能影響到介面電荷傳輸和電荷蒐集，從而使PSC性能轉換效率得到改善以及減低遲滯效應。使用30秒SDDBD處理可以實現PSC的最佳效率。 實驗二的部分是透過氬氣介電質放電噴射電漿在大氣壓的環境下對PEDOT:PSS薄膜做表面改質，並於經由噴射電漿處理後的PEDOT:PSS做薄膜的材料分析，因電漿噴流的口徑較小，只約1 mm左右，故往復掃描的次數方式作為改變參數，分別以水接觸角、SEM俯瞰圖、薄膜導電率量測其表面性質的改變，從結果中得到電漿與表面薄膜反應性比實驗一所述的SDDBD還要高，其在掃瞄5次、7次、9次後表面有很大的變化，進一步以XPS之S2p能譜分析得到此電漿密度較高的Ar DBD jet系統能夠與表面快速反應且移除材料，由SEM剖面圖觀察到厚度隨著電漿處理次數變化，可能可做為材料的微蝕刻或應用在需要高反應性的材料改質上。因此電漿和PEDOT:PSS的反應劇烈，處理過後之PEDOT:PSS做成之鈣鈦礦太陽能電池的效能極差或沒有太陽能電池特徵曲線，因此本部分沒有做鈣鈦礦太陽能電池的探討。 | zh_TW |
| dc.description.abstract | This study investigates the PEDOT:PSS films treated by surface-diffusion dielectric barrier discharge (SDDBD) and Ar DBDjet. SDDBD-treted PEDOT:PSS is then used as the hole transport layer (HTL) of perovskite solar cells (PSCs).
In the first part of the experiment, SDDBD-treated PEDOT:PSS is characterized. The plasma is generated between the dielectric layer and the stainless steel mesh and and diffuses to the materials being treated. The whole SDDBD device is used inside a nitrogen-filled glove box. As the SDDBD treatment time increases, the resistivity decreases and the increases. XPS analyses indicate the removal of the excess PSS on the surface, revealing the PEDOT phase. This change the ratio of PEDOT/PSS, which thereby varies the resistivity and the work function. This could influence the charge transport across the interface and the charge collection, which thereby improve the performance of PSCs and reduce the hysteresis. 30-s SDDBD treatment leads to the best efficiency of PSCs. Second part of the experiment applies Ar dielectric barrier discharge jet (DBDjet) to treat PEDOT:PSS. Because the jet size is ~1 mm, number of scanning times is the parameter. The reaction of Ar DBDjet plasma and PEDOT:PSS is vigorous. XPS S2p results indicate Ar DBDjet effectively removal the whole PEDOT:PSS. DBDjet-treated PEDOT:PSS is not functioning to act as the HTL of PSCs. Therefore, in this part of experiment, no PSC results are presented. | en |
| dc.description.provenance | Made available in DSpace on 2021-07-11T15:15:15Z (GMT). No. of bitstreams: 1 ntu-108-R06543086-1.pdf: 5774453 bytes, checksum: 6459ed235fd08e2d9678592899ef91d8 (MD5) Previous issue date: 2019 | en |
| dc.description.tableofcontents | 目錄
誌謝 II 中文摘要 III Abstract V 圖目錄 IX 表目錄 XII 第1章 13 1.1 前言 13 1.2 研究動機 15 1.3 論文大綱 17 第2章 18 2.1 太陽能電池 18 2.1.1 太陽能電池發展 18 2.1.2 太陽能電池特性參數 21 2.2 鈣鈦礦太陽能電池 24 2.2.1 鈣鈦礦太陽能電池之介紹 24 2.2.2 中孔性結構(mesoporous structure) 25 2.2.3 正規結構(n-i-p structure) 26 2.2.4 倒置結構(p-i-n structure) 27 2.3 反結構鈣鈦礦太陽能電池各層材料 28 2.3.1 透明導電玻璃基板 28 2.3.2 電子傳輸層 28 2.3.3 電洞傳輸層 29 2.4 電漿 31 2.4.1 電漿簡介 31 2.4.2 電漿工作原理 31 2.4.3 電漿操作電壓與溫度 34 2.4.4 常壓電漿 36 第3章 38 3.1 實驗材料與儀器 38 3.2 實驗架構 40 3.3 製程儀器 41 3.3.1 表面擴散式常壓介電質放電電漿系統 41 3.3.2 噴射式常壓介電質放電電漿系統 43 3.3.3 氮氣手套箱 44 3.3.4 旋轉塗佈機 45 3.3.5 電子束蒸鍍機 46 3.4 量測儀器 47 3.4.1 掃描式電子顯微鏡 47 3.4.2 X光子能譜儀 48 3.4.3 太陽光模擬器 49 3.4.4 電化學阻抗分析儀 50 3.4.5 光譜分析儀 51 3.5 實驗流程 53 3.5 實驗一 53 3.5 實驗二 58 第4章 60 4.1 實驗一 60 4.1.1 表面擴散式常壓介電質放電電漿之溫度變化 60 4.1.2 表面擴散式常壓介電質放電電漿之光放射光譜 61 4.1.3 PEDOT:PSS導電性 62 4.1.4 PEDOT:PSS之表面型貌 64 4.1.5 PEDOT:PSS之水接觸角 66 4.1.6 PEDOT:PSS之XPS化學組成 67 4.1.7反結構鈣鈦礦太陽能電池之電性表現 70 4.1.8 PSC元件之電化學阻抗分析 76 4.2 實驗二 79 4.2.1噴射式常壓介電質放電電漿之溫度變化 79 4.2.2噴射式常壓介電質放電電漿之光放射光譜 80 4.2.3 PEDOT:PSS導電性 81 4.2.4 PEDOT:PSS之水接觸角 82 4.2.5 PEDOT:PSS之表面型貌 83 4.2.6 PEDOT:PSS之XPS化學組成 85 第5章 89 附錄A：SDDBD改質之元件效率統計 90 附錄B：常壓噴射電漿(APPJ)處理NiO 92 附錄C：Helium介電質放電噴射電漿(He DBD jet)處理PEDOT:PSS之分析 95 參考文獻 97 | |
| dc.language.iso | zh-TW | |
| dc.title | 表面擴散式及噴射式介電質放電電漿處理聚二氧乙基噻吩-聚苯乙烯磺酸 | zh_TW |
| dc.title | Surface-diffusion and jet-type dielectric barrier discharge plasma treatments on PEDOT:PSS | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 107-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 陳奕君(I-Chun Cheng),徐振哲(Cheng-Che Hsu),王孟菊(Meng-Jiy Wang) | |
| dc.subject.keyword | PEDOT:PSS,表面改質,常壓介電質放電電漿,鈣鈦礦太陽能電池, | zh_TW |
| dc.subject.keyword | PEDOT: PSS,surface modification,atmospheric dielectric barrier discharge plasma,perovskite solar cell, | en |
| dc.relation.page | 108 | |
| dc.identifier.doi | 10.6342/NTU201901916 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2019-07-26 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 應用力學研究所 | zh_TW |
| 顯示於系所單位： | 應用力學研究所 | |
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