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| ???org.dspace.app.webui.jsptag.ItemTag.dcfield??? | Value | Language |
|---|---|---|
| dc.contributor.advisor | 韋文誠 | |
| dc.contributor.author | Po-Wei Wang | en |
| dc.contributor.author | 王柏崴 | zh_TW |
| dc.date.accessioned | 2021-07-11T14:42:44Z | - |
| dc.date.available | 2021-10-14 | |
| dc.date.copyright | 2016-10-14 | |
| dc.date.issued | 2016 | |
| dc.date.submitted | 2016-08-16 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/78116 | - |
| dc.description.abstract | 本研究選用TiO2-Na2O-SiO2-B2O3 (TN-SB)氧化物玻璃,進行熔融擠出與熱電偶鍍膜兩種應用測試。經由調整TN-SB玻璃配方之B2O3/SiO2比例，以固相粉體混合，再以高溫1250 ˚C, 0.5 h熔融製備氧化物玻璃。透過數種熱分析量測不同配比的氧化物玻璃之玻璃轉換溫度、軟化點、熱膨脹係數及黏度。另外，利用碳化矽加熱棒與鐵鉻鋁加熱絲組合一加熱體，並以薄層陶瓷耐火綿、高氧化鋁澆注材製成之袖套，及高氧化鋁熱絕緣層形成之三層斷熱結構，組合為一可用於高溫熔融擠出之組件。在提供最高187 W輸出之電源供應下，此組件可於10分鐘內達1300 ˚C。另外，設計合適之加熱基板及送料裝置，利用此高溫噴頭，示範氧化物玻璃進行高溫熔融擠出之可行性，達到持續200 s之擠出時間與平均25 mm.s-1之擠出速度。研究工作並完成三種銅基熱電偶之玻璃鍍膜製備工作，並校正熱電偶之短時間與長時間(≤30 hr)之熱電位輸出，文中並討論高溫持溫產生之電位誤差之可能原因。 | zh_TW |
| dc.description.abstract | This study selected TiO2-Na2O-SiO2-B2O3 (TN-SB) glasses for the applications of melt extrusion and electrical insulation layer on Cu-based alloy thermocouple. First, the oxide glasses adjusting SiO2/B2O3 ratio were prepared by melt-quenched at 1250 ˚C for 30 min. Thermal properties of the glasses were investigated, including glass transition temperature (Tg), softening temperature (Ts), thermal expansion coefficient (CTE) and viscosity. Moreover, a melt extrusion module with an electromagnetic heating plate and a feeding system were assembled with a heating module, which combined a SiC heating element and Fe-Cr-Al heating wire for heating, and covering with thin ceramic fiber, castable outer sleeve, and a refractory support made by high Al2O3 ceramic board as thermal insulation layers. After providing 187 W power at most, the nozzle could reach 1300 ˚C in 10 min. Also, the formability of the oxide glass by extrusion was tried and capable of continuous extrusion over 200 s at an average speed of 25 mm.s-1. This work also completed a glass coating on various Cu-based thermocouples, calibrated the potential output in short and long ( 30 hr) terms. The possible causes of the deviation of the potential of the thermocouples were discussed. | en |
| dc.description.provenance | Made available in DSpace on 2021-07-11T14:42:44Z (GMT). No. of bitstreams: 1 ntu-105-R03527059-1.pdf: 6368256 bytes, checksum: f05108d3b5607bd2be3778590087aaa6 (MD5) Previous issue date: 2016 | en |
| dc.description.tableofcontents | 摘要 I
ABSTRACT II 圖目錄 VI 表目錄 XI 第一章 緒論 1 第二章 文獻回顧 4 2.1 玻璃特性簡介 4 2.1.1 玻璃的形成 4 2.1.2 玻璃成分與功能簡介 5 2.1.3 玻璃黏流變特性 7 2.2 積層製造 8 2.2.1 積層製造種類 8 2.3 熱電偶 10 2.3.1 熱電動勢原理 10 2.3.2 熱電偶種類與製造方法 12 2.3.3 熱電偶之封裝方法 13 第三章 實驗步驟 26 3.4 實驗材料 26 3.5 玻璃性質分析 26 3.5.1 玻璃合成 27 3.5.2 微差掃描熱分析 27 3.5.3 熱機械分析 27 3.5.4 玻璃結晶性分析 28 3.5.5 導電率量測 28 3.5.6 微結構分析 29 3.5.7 密度量測 29 3.6 熔融擠出噴頭(melt extrusion nozzle) 30 3.6.1 加熱體組裝 30 3.6.2 澆注材製備 31 3.7 玻璃高溫黏度 31 3.7.1 玻璃纖維潛變黏度測試 31 3.7.2 旋轉黏度儀 32 3.8 溫度分布量測 32 3.9 熱電偶製作 33 3.10 管路流體行為實驗 33 第四章 結果與討論 43 4.1 TiO2-Na2O-SiO2-B2O3玻璃系統特性 43 4.1.1 B2O3/SiO2的影響 43 4.1.2 玻璃之熱膨脹行為 44 4.1.3 TN-SB玻璃之結晶性 44 4.1.4 玻璃之電絕緣性質 45 4.1.5 玻璃黏度特性 45 4.2 高溫熱擠出頭的組裝 63 4.2.1 加熱體選用 63 4.2.2 熱擠出噴頭之組裝 64 4.2.3 熱擠出頭之熱模擬分析 65 4.2.4 熱擠出噴頭之性能表現 65 4.3 加熱基板組件設計 75 4.3.1 電阻式加熱基板組件 75 4.3.2 電磁感應加熱基板 77 4.4 玻璃之熔融擠出 89 4.4.1 進料裝置 89 4.4.2 管內流體之應力分析 90 4.4.3 玻璃熔融擠出 92 4.5 熱電偶材料測試 110 4.5.1 熱電動勢與席貝克係數 110 4.5.2 熱電偶之長時間裂化 111 4.5.3 氧化物玻璃塗層之影響 111 第五章 結論 121 | |
| dc.language.iso | zh-TW | |
| dc.subject | 熱電偶 | zh_TW |
| dc.subject | 銅基合金 | zh_TW |
| dc.subject | 熔融擠出 | zh_TW |
| dc.subject | 噴頭 | zh_TW |
| dc.subject | 玻璃 | zh_TW |
| dc.subject | extrusion nozzle | en |
| dc.subject | glass | en |
| dc.subject | melt extrusion | en |
| dc.subject | Cu-based alloy | en |
| dc.subject | thermocouple | en |
| dc.title | 高熱膨脹氧化物玻璃用於熱熔擠出及電絕緣特性之應用研究 | zh_TW |
| dc.title | Applications of High Thermal-Expansion-Coefficient Oxide Glass for Melt Extrusion and Electrical Insulation | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 104-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 王安邦,劉浩志 | |
| dc.subject.keyword | 玻璃,噴頭,熔融擠出,銅基合金,熱電偶, | zh_TW |
| dc.subject.keyword | glass,extrusion nozzle,melt extrusion,Cu-based alloy,thermocouple, | en |
| dc.relation.page | 130 | |
| dc.identifier.doi | 10.6342/NTU201602485 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2016-08-16 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 材料科學與工程學研究所 | zh_TW |
| Appears in Collections: | 材料科學與工程學系 | |
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