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完整後設資料紀錄
DC 欄位 | 值 | 語言 |
---|---|---|
dc.contributor.advisor | 劉懷勝(Hwai-Shen Liu) | |
dc.contributor.author | Yuk-Man Tang | en |
dc.contributor.author | 鄧煜文 | zh_TW |
dc.date.accessioned | 2021-07-10T22:11:39Z | - |
dc.date.available | 2021-07-10T22:11:39Z | - |
dc.date.copyright | 2018-08-08 | |
dc.date.issued | 2018 | |
dc.date.submitted | 2018-07-25 | |
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dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/77613 | - |
dc.description.abstract | 本研究於旋轉填充床中,以氫氧化鈉與甲醇為吸收劑,進行氫氧化鈉水溶液、氫氧化鈉甲醇水溶液以及氫氧化鈉甲醇溶液化學吸收二氧化碳,以研究在化學吸收之吸收劑中添加非水溶劑的效果;文中探討氣液流量、氫氧化鈉濃度、甲醇濃度等變數對吸收百分比、表徵總括氣膜質傳係數(KGa)、吸收劑之二氧化碳負載量(loadingCO2/NaOH、loadingCO2/MeOH)之影響。
實驗結果顯示CO2吸收百分比隨轉速、液體流量以及氫氧化鈉濃度增加而上升,但隨氣體流量增加而下降;KGa隨液體流量、氣體流量、轉速以及氫氧化鈉濃度增加而上升;loadingCO2/NaOH隨轉速以及氣體流量增加而上升,但隨液體流量以及氫氧化鈉濃度增加而下降;loadingCO2/MeOH則是隨著轉速、氣體流量以及氫氧化鈉濃度增加而提升,但隨著提高液體流量以及甲醇濃度而下降;此外,本實驗之CO2吸收百分比、KGa以及loadingCO2/NaOH皆隨甲醇濃度的增加而提升,其中又以溶劑為純甲醇時效果最佳,且其吸收百分比與水溶液相比,最高差距為65%,顯示以氫氧化鈉和甲醇為吸收劑有利於二氧化碳的吸收。 本研究實驗結果以及文獻資料提出一結合化學吸收與物理氣提/吸收之經驗迴歸式如下: (K_G a)/(D_G a_t^2 )=0.6∙Re_G^0.45 Re_L^0.50 Gr_G^0.20 H_y^(-0.5) We_L^0.20 (1+〖Ha〗)^0.3 | zh_TW |
dc.description.abstract | The CO2 absorption by sodium hydroxide solutions, using water, methanol and methanol/water mixture as solvents in a rotating packed bed (RPB) were studied in this work. The gas and liquid flow rate, rotating speed, the concentration of sodium hydroxide and the weight percent of methanol were taken into consideration as operating variables to study the influence on absorption percentage, apparent overall volumetric mass transfer coefficient (KGa), loadingCO2/NaOH and loadingCO2/MeOH.
According to experiment results, as liquid flow rate, the rotating speed and the concentration of sodium hydroxide increased, absorption percentage increased. However, absorption percentage decreased as gas flow rate increased. The KGa values increased with gas and liquid flow rate, the rotating speed and the concentration of sodium hydroxide. The loadingCO2/NaOH values increased with gas flow rate and the rotating speed, but loadingCO2/NaOH values decreased as the concentration of sodium hydroxide and liquid flow rate increased. The loadingCO2/MeOH increased as gas flow rate, the rotating speed and the concentration of sodium hydroxide increased. However, loadingCO2/MeOH decreased as the weight percent of methanol increased. Moreover, using pure methanol as solvent could promote CO2 absorption efficiency and raised absorption percentage at least 65% higer than using water as solvent. In this study, the KGa values of chemical absorption and physical stripping/absorption collected in this research can be predicted well with a correlation presented as: (K_G a)/(D_G a_t^2 )=0.6∙Re_G^0.45 Re_L^0.50 Gr_G^0.20 H_y^(-0.5) We_L^0.20 (1+〖Ha〗)^0.3 | en |
dc.description.provenance | Made available in DSpace on 2021-07-10T22:11:39Z (GMT). No. of bitstreams: 1 ntu-107-R05524088-1.pdf: 11192896 bytes, checksum: 25456c8821a6097014459eab55684fad (MD5) Previous issue date: 2018 | en |
dc.description.tableofcontents | 摘要 I
Abstract II 目錄 IV 圖目錄 VIII 表目錄 XXI 第一章 緒論 1 第二章 文獻回顧 2 2-1 二氧化碳捕捉技術 2 2-1.1 物理吸收 2 2-1.2 化學吸收 3 2-1.3 物理吸附 3 2-1.4 薄膜分離 4 2-1.5 低溫冷凝 4 2-1.6 以甲醇為吸收劑吸收二氧化碳之系統 5 2-2 旋轉填充床 9 2-2.1 旋轉填充床之構造與設計 11 2-2.2 旋轉填充床的壓降 20 2-2.3 旋轉填充床之液體流態、滯留量與滯留時間 26 2-2.4 旋轉填充床之液膜質傳係數與氣膜質傳係數 30 2-2.5 旋轉填充床中化學吸收二氧化碳 35 2-2.6 旋轉填充床之應用與發展 41 第三章 實驗設備與分析方法 51 3-1 實驗裝置 51 3-2 實驗藥品、儀器與實驗流程 53 3-2.1 實驗藥品 53 3-2.2 實驗儀器 53 3-2.3 實驗流程 54 3-3 雙膜理論 (two-film theory) 56 3-4 實驗分析 61 3-4.1 吸收百分比A (absorption percentage) 61 3-4.2 表徵總括氣膜體積質傳係數(apparent overall volumetric mass transfer coefficient) 61 3-4.3 氫氧化鈉之二氧化碳負載量(loadingCO2/NaOH) 63 3-4.4 甲醇之二氧化碳負載量(loadingCO2/MeOH) 63 3-4.5 Hatta number (Ha)之分析 64 3-5 物性資料 66 3-5.1 液體表面張力 (liquid surface tension) 66 3-5.2 二氧化碳在甲醇水溶液中的物理性質 68 第四章 實驗結果與討論 69 4-1 吸收百分比A (absorption percentage) 69 4-1.1 氣、液體進口溫度對於吸收百分比的影響 69 4-1.2 氣體流量及轉速對於吸收百分比的影響 71 4-1.3 液體流量對於吸收百分比的影響 81 4-1.4 氫氧化鈉濃度對於吸收百分比的影響 87 4-1.5 甲醇濃度對於吸收百分比的影響 93 4-1.6 與其他系統吸收百分比之比較 98 4-2 表徵總括氣膜體積質傳係數 (apparent overall volumetric mass transfer coefficient, KGa) 101 4-2.1 氣、液體進口溫度對於質傳係數的影響 101 4-2.2 氣體流量以及轉速對於質傳係數的影響 103 4-2.3 液體流量對於質傳係數的影響 110 4-2.4 氫氧化鈉濃度對於質傳係數的影響 117 4-2.5 甲醇濃度對於質傳係數的影響 123 4-2.6 與其他系統之質傳係數比較 130 4-3 氫氧化鈉之二氧化碳負載量(loadingCO2/NaOH) 133 4-3.1 氣、液進口溫度對於負載量(loadingCO2/NaOH)的影響 133 4-3.2 氣體流量以及轉速對於loadingCO2/NaOH的影響 135 4-3.3 液體流量對於負載量(loadingCO2/NaOH)的影響 142 4-3.4 氫氧化鈉濃度對於負載量(loadingCO2/NaOH)的影響 148 4-3.5 甲醇濃度對loadingCO2/NaOH的影響 154 4-3.6 與其他系統之loading比較 160 4-4 甲醇之二氧化碳負載量(loadingCO2/MeOH) 162 4-4.1 氣、液體進口溫度對於loadingCO2/MeOH的影響 162 4-4.2 氣體流量及轉速對於loadingCO2/MeOH的影響 164 4-4.3 液體流量對於負載量(loadingCO2/MeOH)的影響 170 4-4.4 氫氧化鈉濃度對於負載量(loadingCO2/MeOH)的影響 175 4-4.5 甲醇濃度對於負載量(loadingCO2/MeOH)的影響 180 4-4.6 與其他系統之loadingCO2/MeOH做比較 184 4-5 總括氣膜體積質傳迴歸式 185 4-5.1 無因次的選擇與亨利常數的影響 185 4-5.2 甲醇濃度之影響 190 4-5.3 化學吸收之影響 194 4-5.4 氫氧化鈉甘油溶液與氫氧化鈉甲醇溶液之化學吸收 197 4-5.5 化學吸收與物理氣提/吸收 199 4-5.6 驗證 203 4-5.7 各參數的指數與係數之比較 206 第五章 結論 209 參考文獻 212 符號說明 227 附錄A 實驗之吸收百分比、KGa數據表 232 附錄B 在吸收二氧化碳同時,吸收劑溶劑中甲醇揮發量及甲醇之氣提百分比 273 附錄C 非球型填充物換算等體積球直徑 274 附錄D 二氧化碳濃度之校正曲線 275 附錄E 以不同填充物之特性修正物理吸收/氣提、化學吸收之迴歸 276 | |
dc.language.iso | zh-TW | |
dc.title | 旋轉填充床中氫氧化鈉甲醇溶液吸收二氧化碳 | zh_TW |
dc.title | Carbon Dioxide Absorption by Sodium Hydroxide Methanol Solution in a Rotating Packed Bed | en |
dc.type | Thesis | |
dc.date.schoolyear | 106-2 | |
dc.description.degree | 碩士 | |
dc.contributor.oralexamcommittee | 林佳璋,陳昱劭,江佳穎 | |
dc.subject.keyword | 旋轉填充床,化學吸收,吸收百分比,氣膜質傳係數,二氧化碳,甲醇, | zh_TW |
dc.subject.keyword | rotating packed bed,chemical absorption,gas-side mass transfer coefficient,absorption percentage,carbon dioxide,methanol, | en |
dc.relation.page | 278 | |
dc.identifier.doi | 10.6342/NTU201801861 | |
dc.rights.note | 未授權 | |
dc.date.accepted | 2018-07-26 | |
dc.contributor.author-college | 工學院 | zh_TW |
dc.contributor.author-dept | 化學工程學研究所 | zh_TW |
顯示於系所單位: | 化學工程學系 |
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