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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 許正一(Zeng-Yei Hseu) | |
| dc.contributor.author | Cho-Yin Wu | en |
| dc.contributor.author | 吳卓穎 | zh_TW |
| dc.date.accessioned | 2021-05-19T17:40:49Z | - |
| dc.date.available | 2024-08-07 | |
| dc.date.available | 2021-05-19T17:40:49Z | - |
| dc.date.copyright | 2019-08-07 | |
| dc.date.issued | 2019 | |
| dc.date.submitted | 2019-07-31 | |
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Statistical analyses of geochemical variables in soils of Ireland. Geoderma, 146, 378–390. | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/7270 | - |
| dc.description.abstract | 2001到2017年間，全球工業中釩的需求量增加超過一倍，如此迅速成長的釩需求也成為環境品質以及人類健康的潛在威脅。然而，關於釩的地質化學方面的知識仍十分薄弱。因此，本研究欲利用17個採集自臺灣不同母質 (板岩、砂頁岩互層、安山岩、玄武岩以及蛇紋岩) 之土壤剖面進行釩全面性的探討，包含其來源、潛在移動性、剖面中的分佈以及生物有效性。結果顯示，由ICP-AES測定氫氟酸消化後之供試土樣中總釩濃度為35.4-475 mg/kg其平均值為182 mg/kg，其中，玄武岩母質的土樣中總釩濃度遠高於其餘土樣。此外，風化程度並未對總釩濃度有顯著影響。攜帶式X射線螢光光譜儀之測定結果顯示其在土樣中釩的快速檢測具有高度實用性。BCR序列萃取結果指出，供試土樣中的釩主要固定於礦物晶格中，然而鐵錳氧化物結合態的釩也佔有可觀的比例。利用DCB萃取法以及電子探針顯微分析儀，本研究更進一步證實釩在母質以及風化後的土壤中皆具有高度親鐵性。釩的X射線吸收近邊緣結構圖譜顯示在供試土樣中釩的主要化學物種V(IV) (VO2+) 和V(V) (H2VO4-)，此兩者皆可有效地被NaHCO3所萃取。以小白菜 (Brassica rapa var. chinensis) 進行之盆栽試驗顯示NaHCO3土壤釩萃取量和植物地上部之釩吸收量呈顯著正相關，此結果同時證明，釩潛在的生物有效性可由包含土壤總釩濃度以及土壤酸鹼值之多變因回歸等式計算而出。 | zh_TW |
| dc.description.abstract | The global vanadium (V) demand in industry increased over 100% from 2001 to 2017, thus the burgeoning V demand leads to potential risks to environment quality and human health. However, there is still a knowledge gap in pedogeochemical aspect of V. This study attempted to explore the sources, fractionation, profile distribution, and bioavailability of V from 17 soil pedons with 94 horizon samples in Taiwan. These pedons were derived from different parent materials including slate, sandstone interstratified with shale, andesite, basalt, and serpentine. The total V content was measured by using ICP-AES followed with HF-digestion and portable x-ray fluorescence (pXRF). The total V content by ICP-AES in the soils ranged from 35.4 to 475 mg/kg with an average level of 182 mg/kg. Moreover, the total V content in the basalt-derived soils was much higher than those of other parent materials. Nevertheless, the weathering degree of soil did not clearly affect the V level among soils. Furthermore, the pXRF showed high practicality in rapid V determination. The Commission of the European Communities Bureau of Reference (BCR) selective sequential extraction (SSE) method indicated V was primarily fixed in the mineral lattices. However, the Fe/Mn-oxide-bound fraction was remarkably observed. The siderophilic affinity of V in parent materials and derived soils was further confirmed by the dithionite-citrate-bicarbonate (DCB)-extractable Fe and element mapping conducted with electron probe X-ray microanalyzer (EPMA). V(IV) (VO2+) and V(V) (H2VO4-) were the dominant species of V in the soils demonstrated by the V K-edge X-ray absorption near edge structure (XANES) spectra, while both can be efficiently extracted by NaHCO3 extraction to predict a better bioavailability of V than CaCl2, HCl, and EDTA. The plant assay conducted with Chinese cabbage (Brassica rapa var. chinensis) revealed the soil NaHCO3 extractable V positively and significantly correlated with the plant shoot uptake of V, supporting the potentially bioavailable V can be computed by using multivariate regression equation considering the soil total V and pH. | en |
| dc.description.provenance | Made available in DSpace on 2021-05-19T17:40:49Z (GMT). No. of bitstreams: 1 ntu-108-R05623038-1.pdf: 2355713 bytes, checksum: 1c70b8f70e00a0ff12ce24da481d4e0f (MD5) Previous issue date: 2019 | en |
| dc.description.tableofcontents | 摘要............. i
Abstract ii Contents iv List of Tables vii List of Figures viii Chapter 1 Background 1 Chapter 2 Introduction 3 2.1. Chemical characteristics of vanadium 3 2.2. Application of vanadium in industry 3 2.3. Biological toxicity of vanadium 4 2.4. Vanadium in soils 6 2.4.1. Natural background 6 2.4.2. Anthropogenic sources 9 2.4.3. Geochemical fractions of V in soils 10 2.4.4. Sorption of vanadium 11 2.4.5. Vanadium speciation in soils 12 2.4.6. Bioavailability of soil vanadium 14 2.5. Aims of this study 17 Chapter 3 Materials and methods 18 3.1. Sample source 18 3.2. Soil sampling 21 3.3. Physical and chemical analysis 21 3.3.1. Water content 21 3.3.2. Particle size analysis 21 3.3.3. Soil pH 23 3.3.4. Organic C (OC) 23 3.3.5. Total element content 24 3.4. Geochemical fractions 25 3.5. Dithionite–citrate–bicarbonate (DCB) extraction of Fe, Al, Mn and V 26 3.6. Spatial distribution of soil vanadium 26 3.7. Valence of soil vanadium 27 3.8. Bioavailability of soil vanadium 28 3.8.1. Single extraction 28 3.8.2. Pot experiment 29 3.8.3. Vanadium content in plant shoot 30 3.10. Quality assurance and quality control 30 3.11. Statistical analysis 31 Chapter 4 Results and discussions 32 4.1. Soil physicochemical characteristics 32 4.2. Total vanadium contents 38 4.3. Geochemical fractions of vanadium 44 4.4. Spatial distribution of soil vanadium 51 4.5. Valence of soil vanadium 53 4.6. Bioavailability of soil vanadium 55 4.7. Multivariate regression of independent parameters 63 Chapter 5 Conclusions 64 Chapter 6 References 65 Appendix 1 80 Appendix 2 81 | |
| dc.language.iso | zh-TW | |
| dc.subject | X射線吸收近邊緣結構圖譜 | zh_TW |
| dc.subject | 土壤母質 | zh_TW |
| dc.subject | 電子探針顯微分析儀 | zh_TW |
| dc.subject | 生物有效性 | zh_TW |
| dc.subject | 序列萃取 | zh_TW |
| dc.subject | XANES | en |
| dc.subject | sequential extraction | en |
| dc.subject | parent material | en |
| dc.subject | EPMA | en |
| dc.subject | bioavailability | en |
| dc.title | 釩在臺灣不同類型土壤的分佈與有效性評估 | zh_TW |
| dc.title | Assessment of vanadium distribution and availability in different types of soil in Taiwan | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 107-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 陳尊賢(Zueng-Sang Chen),田村憲司(Kenji Tamura),山路?子(Keiko Yamaji),山下祐司(Yuji Yamashita) | |
| dc.subject.keyword | 生物有效性,電子探針顯微分析儀,土壤母質,序列萃取,X射線吸收近邊緣結構圖譜, | zh_TW |
| dc.subject.keyword | bioavailability,EPMA,parent material,sequential extraction,XANES, | en |
| dc.relation.page | 81 | |
| dc.identifier.doi | 10.6342/NTU201902117 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2019-07-31 | |
| dc.contributor.author-college | 生物資源暨農學院 | zh_TW |
| dc.contributor.author-dept | 農業化學研究所 | zh_TW |
| dc.date.embargo-lift | 2024-08-07 | - |
| 顯示於系所單位： | 農業化學系 | |
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