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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 蘇忠楨 | |
| dc.contributor.author | Yu-Chun Chou | en |
| dc.contributor.author | 周佑峻 | zh_TW |
| dc.date.accessioned | 2021-06-17T02:01:34Z | - |
| dc.date.available | 2019-08-01 | |
| dc.date.copyright | 2017-08-01 | |
| dc.date.issued | 2017 | |
| dc.date.submitted | 2017-07-18 | |
| dc.identifier.citation | 郭猛德、林晉卿、郭春芳。2000。豬糞尿污泥之處理與利用。畜產研究 33:4，頁397-408。
郭猛德、蕭庭訓、王政騰。2008。養豬三段式廢水與污泥處理技術。畜牧半月刊 81:5，頁 29-38。 黃雅祺、劉華美。2012。美國生質能推動政策與法制之研究。經濟部能源局，能源論文，26。 謝政哲。2015。畜牧業廢棄污泥產製生質柴油之技術研究。國立臺灣大學生物資源暨農學院動物科學技術系碩士論文。 經濟部能源局。2016。2016年能源產業技術白皮書。Retrieved March 3, 2017 Ağdağ, O., and Sponza, D. (2007). Co-digestion of mixed industrial sludge with municipal solid wastes in anaerobic simulated landfilling bioreactors. J Hazard Mater 140, 75–85. Amon, T., Amon, Kryvoruchko, Bodiroza, Pötsch, and Zollitsch (2006). Optimising methane yield from anaerobic digestion of manure: Effects of dairy systems and of glycerine supplementation. Int. Congr. Ser. 1293, 217-220. Andrew, D. E., Lenore, S. C., Arnold, E. G. (1995) Standard Methods for the Examination of Water and Wastewater Atabani, A.E., Silitonga, A.S., Badruddin, I., Mahlia, T.M.I., Masjuki, H.H., and Mekhilef (2012). A comprehensive review on biodiesel as an alternative energy resource and its characteristics. Renew Sustain Energy Rev 16, 2070–2093. Ayoub, M., and Abdullah, A. (2012). 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Bioresource Technol 100, 1122–1129. | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/67974 | - |
| dc.description.abstract | 現今的人類活動促使大量對石化燃料的需求及廢水需要處理。污泥為廢水處理過程中會產生的廢棄物，其處理成本約佔總廢水處理成本的50~60%。本研究的目的為評估以屠宰場污泥餅轉酯化產製生質柴油及利用其副產物粗甘油進行厭氧共消化生產沼氣之可行性。在轉酯化試驗中，屠宰場污泥餅在55℃下與甲醇及濃硫酸或鹽酸進行轉酯化，試驗分為三種催化劑濃度 (2、4及8%) 與四個反應時間 (4、8、16及24小時)。在4%濃硫酸及鹽酸下反應24小時分別可得到最高2.78±0.19及2.67±0.08%的FAME產率。此外，以污泥餅產製的FAME主要皆由C16:0、C16:1、C18:0及C18:1之脂肪酸甲酯組成。在粗甘油厭氧共消化試驗中，利用以濃硫酸催化所得的粗甘油以三種不同添加量 (2、4及8%) 與養牛廢水進行共消化試驗，試驗在35℃下反應14天。雖然8%組有最高的甲烷產氣量，其過多的揮發性脂肪酸造成pH值過低進而使其化學需氧量、生化需氧量及懸浮固形物的去除率皆下降。添加2與4%粗甘油組相較於控制組分別提高了177與226%的甲烷產氣量，且無減低化學需氧量、生化需氧量及懸浮固形物的去除率。然而，研究結果顯示不論額外添加多少濃度的粗甘油，皆會降低槽體總固形物及揮發性固形物的去除率。總結而言，透過本研究所建立的轉酯化及厭氧共消化反應的整合平台，屠宰場污泥餅可以作為生產生質能源的原料。 | zh_TW |
| dc.description.abstract | The human activities nowadays had given rise to a huge demand on petroleum-based fuels and also contributed to numerous wastewaters to process. Sludge is a waste formed during wastewater treatment process and its treating cost 50−60% of total wastewater treatment. The aim of this study is to evaluate the feasibility of producing biodiesel and biogas by transesterification of slaughterhouse sludge cake and anaerobic co-digestion of its processing by-product, crude glycerol, respectively. For biodiesel producing experiments, sludge cake was transesterified with methanol and sulfuric acid or hydrochloric acid at 55℃. Three catalyst concentrations (2, 4, and 8%, v/v) under four reaction periods (4, 8, 16, and 24 hrs) were applied. The highest FAME yield of 2.78±0.19 and 2.67±0.08% can be achieved when 4% (v/v) of sulfuric acid and hydrochloric acid added for 24-h reaction, respectively. Methyl esters of palmitic acid (C16:0), palmitoleic acid (C16:1), stearic acid (C18:0), and oleic acid (C18:1) were found to be the major components of biodiesel in this study. To clarify the effects of crude glycerol addition on biogas production and wastewater treatment, different ratios (2, 4, and 8%, v/v) of crude glycerol from the previous experiment were mixed with dairy wastewater and inoculated with anaerobic dairy sludge. The mixture was then incubated at 35℃ for 14 days. Although 8% group showed the highest total methane production, low pH resulted from volatile fatty acid (VFA) accumulation decreased the removal efficiency of chemical oxygen demand (COD), biochemical oxygen demand (BOD), and suspended solids (SS). Addition of 2 and 4% of crude glycerol increased total methane production up to 177 and 226% compared to the control group, respectively. Moreover, both of them didn’t show negative effects on COD, BOD, and SS removal efficiency. Additionally, addition of crude glycerol decreased removal efficiency of total solids (TS) and volatile solids (VS) regardless of the volume added. In conclusion, slaughterhouse sludge cake has been proven to be a feedstock for producing bioenergy through transesterification and anaerobic co-digestion technical platform. | en |
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| dc.description.tableofcontents | 謝誌 II
摘要 IV Abstract V 目錄 VII 圖目錄 X 表目錄 XII 第壹章、前言 1 一、 研究動機及目的 1 第貳章、文獻回顧 2 一、 廢水處理 2 (一) 污水、廢水處理設施 2 (二) 國內及國外畜牧業廢水處理設施 2 (三) 廢水處理系統之污泥及污泥處理系統 5 (四) 國內及國外污泥處理方式 8 二、 生質柴油 8 (一) 生質柴油之起源 8 (二) 生質柴油的定義 9 (三) 生質柴油之特點 9 (四) 製作生質柴油之原料 10 (五) 生質柴油產製方式 12 (六) 影響轉酯化反應之因素 14 (七) 各國及國內之生質柴油生產、使用現況及政策 17 (八) 污泥產製生質柴油相關文獻探討 19 三、 粗甘油厭氧共消化 23 (一) 厭氧消化 23 (二) 厭氧消化步驟 23 (三) 影響厭氧消化之因子 24 (四) 沼氣之介紹及應用 26 (五) 厭氧共消化 27 (六) 粗甘油 27 (七) 粗甘油厭氧共消化相關文獻探討 29 第參章、材料與方法 31 一、 生質柴油 31 (一) 原料收集與製備 31 (二) 試驗設計 31 (三) 統計分析 31 (四) 生質柴油產製流程 32 (五) 脂肪酸甲酯 (Fatty acid methyl ester, FAME) 含量及組成分分析 34 二、 粗甘油與養牛廢水厭氧共消化 35 (一) 原料收集與製備 35 (二) 試驗設計 35 (三) 統計分析 36 (四) 厭氧共消化反應槽設計 36 (五) 厭氧共消化實驗流程 37 (六) 化學需氧量 (COD) 之檢測 38 (七) 生化需氧量 (BOD) 之檢測 39 (八) 懸浮固形物 (SS) 之檢測 41 (九) 總固形物 (TS) 及揮發性固形物 (VS) 之檢測 42 (十) pH值之檢測 43 (十一) 揮發性脂肪酸 (Volatile Fatty Acids, VFAs) 之檢測 43 (十二) 沼氣氣體組成之分析 44 第肆章、結果與討論 45 一、 屠宰場污泥餅轉酯化產製生質柴油試驗 45 (一) 污泥餅性質分析 45 (二) 以濃硫酸作為催化劑轉酯化試驗結果 45 (三) 以鹽酸作為催化劑轉酯化試驗結果 52 (四) 以濃硫酸及鹽酸作為轉酯化反應催化劑之比較 58 (五) 與各文獻結果之比較與討論 58 二、 粗甘油與養牛廢水厭氧共消化產製沼氣試驗 62 (一) 原料基本性質分析 62 (二) 沼氣產量分析 62 (三) 甲烷濃度分析 66 (四) 甲烷產量分析 67 (五) pH值分析 69 (六) 揮發性脂肪酸(Volatile fatty acids, VFAs)分析 70 (七) 沼氣生產效率分析 74 (八) 總固形物 (TS) 及揮發性固形物 (VS) 去除效率分析 75 (九) 單位揮發性固形物產沼氣效率 (Specific biogas production) 分析 77 (十) 水質分析 79 (十一) 與各文獻結果之比較與討論 83 第伍章、結論與未來研究方向 86 第陸章、參考文獻 87 附錄 96 | |
| dc.language.iso | zh-TW | |
| dc.subject | 脂肪酸甲酯 | zh_TW |
| dc.subject | 沼氣 | zh_TW |
| dc.subject | 生質柴油 | zh_TW |
| dc.subject | 轉酯化 | zh_TW |
| dc.subject | 污泥 | zh_TW |
| dc.subject | 厭氧共消化 | zh_TW |
| dc.subject | 粗甘油 | zh_TW |
| dc.subject | Biogas | en |
| dc.subject | Transesterification | en |
| dc.subject | Biodiesel | en |
| dc.subject | FAME | en |
| dc.subject | Crude glycerol | en |
| dc.subject | Anaerobic co-digestion | en |
| dc.subject | Sludge | en |
| dc.title | 屠宰場污泥餅轉酯化及其副產物粗甘油進行厭氧共消化產製生質能源之研究 | zh_TW |
| dc.title | Research of bioenergy production by transesterification of slaughterhouse sludge cake and anaerobic co-digestion of its processing by-product crude glycerol | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 105-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 徐世勳,周楚洋 | |
| dc.subject.keyword | 污泥,轉酯化,生質柴油,脂肪酸甲酯,粗甘油,厭氧共消化,沼氣, | zh_TW |
| dc.subject.keyword | Sludge,Transesterification,Biodiesel,FAME,Crude glycerol,Anaerobic co-digestion,Biogas, | en |
| dc.relation.page | 98 | |
| dc.identifier.doi | 10.6342/NTU201701654 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2017-07-19 | |
| dc.contributor.author-college | 生物資源暨農學院 | zh_TW |
| dc.contributor.author-dept | 動物科學技術學研究所 | zh_TW |
| 顯示於系所單位： | 動物科學技術學系 | |
文件中的檔案：
| 檔案 | 大小 | 格式 | |
|---|---|---|---|
| ntu-106-1.pdf 未授權公開取用 | 5.16 MB | Adobe PDF |
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