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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 吳茂昆(Maw-Kuen Wu),陳國慶(Maw-Kuen Wu Kuo-Ching Chen) | |
| dc.contributor.author | Wei-Hsiang Chao | en |
| dc.contributor.author | 趙偉祥 | zh_TW |
| dc.date.accessioned | 2021-06-16T23:34:03Z | - |
| dc.date.available | 2014-08-20 | |
| dc.date.copyright | 2012-08-01 | |
| dc.date.issued | 2012 | |
| dc.date.submitted | 2012-07-27 | |
| dc.identifier.citation | References of Chapter 0
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/65274 | - |
| dc.description.abstract | LiCu2O2是一個典型的準一維螺旋磁性材料，同時也是第一個被發現具有多鐵性質的銅氧化物。它在低溫環境下會形成磁有序行為，且自身擁有低維度量子自旋系統的幾何變動特性，這些不尋常的物理性質近來引起了廣泛的關注；有許多實驗皆證實了這個s=1/2的磁系統大約在22-24 K自旋有序溫度下擁有一個不對稱的螺旋磁性基態。在此論文的第一部份，我們成功地生長了一系列的LiδCu2O2 (LCO) 與 LiδTMxCu2-xO2 (LTCO, TM = 鈦、鎳、鋅) (δ = 1 - 1.2 與 x = 0 - 0.1)晶體，典型的LiCu2O2單晶具有ab面的特性，不僅呈現出高純度與高結晶度的X光繞射圖譜，同時也顯示出非雙晶的結構，沒有TM摻雜的晶體尺寸可達9×6 mm2。我們利用軟X射線偏振光的吸收光譜量測法來瞭解銅與TM在不同晶格結構時其價態與軌域的特性，同時隨著不同TM摻雜量成功地摻雜進入銅的位置，可以獲取不同TM摻雜量單晶的物理特性。
另一方面，近年來鐵基超導體是個熱門有趣的議題。自從具有層狀結構的鐵基氮磷族氧化物LaO1-xFxFeAs超導體被發現擁有相對高的超導轉變溫度26 K之後，從那時起，更多的鐵基超導體陸續被提出且轉變溫度甚至可高達56 K。而硒化鐵具有最簡單的晶體結構以及8K的超導轉變溫度，因此吸引了廣泛的注意；在鐵硫族化合物與鐵氮族化合物系統中有許多共同的物理特性可以被提供來瞭解高溫超導的超導機制。在論文的第二部份中，我們利用高壓合成技術成功獲得一系列的硒化鐵晶體並描述其生長條件與物理特性，硒化鐵晶體皆呈現(101)優選方向且擁有高結晶性，晶體的尺寸最大可達2×2 mm2，其中Fe1.03Se晶體藉由適當的熱處理後超導轉變溫度可達到9 K。相較於多晶的硒化鐵樣品，由磁化率的量測證實硒化鐵晶體無論在零場冷或場冷的量測曲線中都呈現出相對輕微的磁背景訊號，這些晶體具有相對高的純淨度將有助於研究超導機制的形成。 | zh_TW |
| dc.description.abstract | LiCu2O2 is a typical quasi-one dimensional helimagnetic material which also is the first member of the cuprate family found to be mutiferroics. Due to its unusual magnetic order at low temperature and low dimensional quantum spin systems with geometric frustration. Therefore, it has recently attracted a great deal of attention. More experiments clearly demonstrated that this s=1/2 magnetic system possess an incommensurate helimagnetic ground state during the spin ordering temperature about 22-24 K. In first part of this thesis, a systematic investigation of LiδCu2O2 (LCO) and LiδTMxCu2-xO2 (LTCO, TM = Ti, Ni and Zn) (δ = 1 - 1.2 and x = 0 - 0.1) were undertaken to determine growth parameters and crystal properties. Typical LiCu2O2 crystals with ab-plane habit not only show a clean X-ray diffraction pattern without impurities and high crystalinity but also exhibit untwined structure. A typical size of large single crystals LiCu2O2 was 9×6 mm2. The orbital character of the valence states of Cu and TM ions on different sites were investigated by polarization-dependent soft X-ray absorption (XAS) spectroscopy measurement with in- and out-of-plane X-ray E vectors. These crystals exhibit varied physical properties owing to successful incorporation of TM dopants.
On the other hand, in recent years the iron-based superconductors are well received by everyone interested in the issues. With layer structure iron-based quaternary oxypnictides, LaO1-xFxFeAs superconductors were found with its superconductivity transition TC ~ 26 K which is a relatively high transition temperature. Since then, more iron-based superconductors have been discovered and the transition temperature TC up to 56 K. The FexSe arouse the majority of interest because of its simplest crystal structure and with superconducting transition around 8 K without any carrier doping. In the iron-chacogenides system, excluding arsenic but with iron-pnictides have many common physical characteristics which can provide important information to understand the superconducting mechanism of high-temperature superconductors. In the second part we reported the growth and characterization of FexSe single crystals. High-pressure cubic-anvil technique successfully obtained FexSe single crystals of a size up to 2 × 2 mm2 at an optimum growth pressure of 2.8 GPa. As-grown crystals showed a characteristic of (101) crystal orientation with good out-of-plane and in-plane crystallinity. The maximum TC = 9 K in Fe1.03Se crystal was reached after appropriate heat treatment. The crystals exhibit more slight magnetic background both in ZFC and FZ curves in the normal state corroborate by susceptibility measurement. Such crystals have significantly purer quality compared to the polycrystalline samples and are promising for future investigation of superconductivity. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-16T23:34:03Z (GMT). No. of bitstreams: 1 ntu-101-D94543002-1.pdf: 14172006 bytes, checksum: f2adabfae899170747c32df158ab9012 (MD5) Previous issue date: 2012 | en |
| dc.description.tableofcontents | Table of Contents
ACKNOWLEDGMENT i ABSTRACT (CHINESE) iii ABSTRACT v TABLE OF CONTENTS vii LIST OF FIGURES xii LIST OF TABLES xix Chapter 0 Introduction 1 References of Chapter 0 3 Part 1 Multiferroic LiCu2O2 4 Chapter 1 Survey of Multiferroic Cuprate 4 1.1 Multiferroic cuprate 4 1.2 Overview of LiCu2O2 5 1.3 Motivation 11 References of Chapter 1 18 Chapter 2 Theoretical Background of Multiferroic Material 22 2.1 Multiferroic 22 2.1.1 Magnetoelectric effect (ME effect) 23 2.2 Magnetism 28 2.2.1 Paramagnetism 29 2.2.2 Diamagnetism 30 2.2.3 Ferromagnetism, ferrimagnetism, and antiferromagnetism 32 2.2.4 Spin-glass 34 2.3 X-ray absorption spectroscopy 37 References of Chapter 2 47 Chapter 3 Experiment Details 49 3.1 Crystal growth 49 3.1.1 Traveling solvent floating zone (TSFZ) method 49 3.2 Sample characterizations 53 3.2.1 Structure 53 3.2.2 Chemical composition 54 3.2.3 Electrical transport 55 3.2.4 DC susceptibility 56 3.2.5 X-ray photoelectron spectroscopy (XPS) 58 3.2.6 X-ray absorption spectroscopy (XAS) 59 References of Chapter 3 62 Chapter 4 Crystal Growth and Physical Properties of Transition-Metal-Doped LiCu2O2 64 4.1 Crystal growth 64 4.2 Chemical composition and structure of crystals 65 4.3 Magnetic properties 72 4.4 Specific heat 75 4.5 Dielectric constant 76 4.6 Near edge X-ray absorption spectroscopy of LCO and LTCO 77 4.7 Summary 85 References of Chapter 4 98 Part 2 Iron-based Superconductors 100 Chapter 5 Survey of Fe-based Superconductor 100 5.1 Overview of high temperature superconductors 100 5.2 The discovery of Fe-based superconductors 104 5.3 Motivation 108 References of Chapter 5 113 Chapter 6 Theoretical Background of Superconductivity 118 6.1 Superconductivity 118 References of Chapter 6 128 Chapter 7 Experiment Details 129 7.1 Crystal growth by high-pressure cubic-anvil technique 129 7.2 Chemical composition 132 7.3 Orientation dependence of DC susceptibility 133 References of Chapter 7 135 Chapter 8 Study on Crystal Growth and Physical Properties of FexSe Superconductor 136 8.1 Crystal growth FexSe 136 8.2 Crystal morphology and structure identification 138 8.3 Chemical composition determination 141 8.4 Magnetic and resistive properties 143 8.5 Near edge X-ray absorption spectroscopy of FexSe 149 8.5.1 Experimental 150 8.5.2 K-edge XAS spectroscopy of Fe and Se 151 8.5.3 The electronic correlation of the Fe 3d 156 8.5.4 Temperature dependence of FexSe XANES 159 8.6 Summary 161 References of Chapter 8 181 Chapter 9 Conclusion 185 | |
| dc.language.iso | en | |
| dc.subject | 晶體生長 | zh_TW |
| dc.subject | 高壓法 | zh_TW |
| dc.subject | 多鐵性 | zh_TW |
| dc.subject | 浮動區法 | zh_TW |
| dc.subject | 鐵基超導體 | zh_TW |
| dc.subject | crystal growth | en |
| dc.subject | mutiferroics | en |
| dc.subject | floating-zone method | en |
| dc.subject | high pressure method | en |
| dc.subject | iron-based superconductor | en |
| dc.title | 多鐵性LiCu2O2與鐵基超導體之晶體成長與物性分析之研究 | zh_TW |
| dc.title | Investigation of Crystal Growth and Characterization in Multiferroic LiCu2O2 and Fe-based Superconductor | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 100-2 | |
| dc.description.degree | 博士 | |
| dc.contributor.oralexamcommittee | 齊正中(Cheng-Chung Chi),陳洋元(Yang-Yuan Chen),王明杰(Ming-JyeWang) | |
| dc.subject.keyword | 晶體生長,多鐵性,浮動區法,高壓法,鐵基超導體, | zh_TW |
| dc.subject.keyword | crystal growth,mutiferroics,floating-zone method,high pressure method,iron-based superconductor, | en |
| dc.relation.page | 187 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2012-07-27 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 應用力學研究所 | zh_TW |
| 顯示於系所單位： | 應用力學研究所 | |
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