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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/61029完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 劉貴生(Guey-Sheng Liou) | |
| dc.contributor.author | Shih-Han Chen | en |
| dc.contributor.author | 陳詩涵 | zh_TW |
| dc.date.accessioned | 2021-06-16T10:42:19Z | - |
| dc.date.available | 2018-08-01 | |
| dc.date.copyright | 2013-08-28 | |
| dc.date.issued | 2013 | |
| dc.date.submitted | 2013-08-13 | |
| dc.identifier.citation | CHAPTER 1
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/61029 | - |
| dc.description.abstract | 本論文分成四個章節， 第一章為總體序論。第二章節包含了以
1-(2-(4-(bis(4-aminophenyl)amino)phenoxy)ethyl)-1'-ethyl-[4,4'-bipyridine] hexafluorophosphate, 4,4'-diamino-4'-methoxytriphenylamine 和 N,N'-bis(4-aminophenyl)-N,N'-di(4-methoxylphenyl)-1,4-phenylenediamine為主體與 間苯二甲醯氯利用低溫聚合法合成出一系列新型含三苯胺帶有紫精側鍊之陽極/ 陰極芳香族聚醯胺。第三章是以 1-(2-(4-(bis(4-aminophenyl)amino)phenoxy)ethyl)-1'-ethyl-[4,4'-bipyridine] hexafluorophosphate為主體與兩種不同的二酸酐合成出另一系列新型含三苯胺之 芳香族聚醯亞胺。第四章節為結論。這五個新型三苯胺帶有紫精側鍊之芳香族高 分子之合成與基本特性、電化學及電致變色性質已被研究與比較。所有的高分子 在極性非質子型溶劑中有好的溶解性，出色的薄膜成形能力，在空氣下高的碳殘 餘量，機械性質，較低的HOMO值。在利用電化學與光譜電化學的方法下，大部 分的高分子也展現出色可逆的電致變色特性。此外，在第二章我們比較了同聚物 與共聚物, 結果顯示若加入含有紫精基團醚鏈單元進入高分子鍊段並不影響其 氧化電位。另外在第三章的部分，兩個芳香族聚醯亞胺不論在氧化或還原上都顯 示了高顏色對比。 | zh_TW |
| dc.description.abstract | This study has been separated into four chapters. Chapter 1 is general introduction.
Chapter 2 includes a series of novel ambipolar aramids derived from three diamine monomers,1-(2-(4-(bis(4-aminophenyl)amino)phenoxy)ethyl)-1'-ethyl-[4,4'-bipyridin e] hexafluorophosphate, 4,4'-diamino-4'-methoxytriphenylamine, and N,N'-bis(4-aminophenyl)-N,N'-di(4-methoxylphenyl)-1,4-phenylenediamine with diacid chloride IPC via low-temperature polycondensation reaction. Chapter 3 describes the other series of novel aromatic polyimides derived from 1-(2-(4-(bis(4-aminophenyl)amino)phenoxy)ethyl)-1'-ethyl-[4,4'-bipyridine] hexafluorophosphate and various commercially available tetracarboxylic dianhydrides by thermal imidization. Chapter 4 is conclusions. The synthesis, basic characterization, electrochemical and electrochromic properties of these novel triphenylamine-containing aromatic polymers with viologen pendant groups were investigated and compared. All polymers had good solubility in many polar aprotic solvents, and exhibited excellent thin-film-forming ability. In addition to high char yield in air flow, mechanical properties, and lower HOMO energy levels, most of the obtained polymers also revealed excellent reversibility of electrochromic characteristics by the electrochemical and spectroelectrochemical methods. Furthermore, in chapter 2 we compared homopolymer and copolymers, and the results showed that adding ether linkage with viologen moiety did not make influence on polymer backbone. Besides, two polyimides showed interesting electrochromic behavior with high contrast both in oxidation and reduction in chapter 3. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-16T10:42:19Z (GMT). No. of bitstreams: 1 ntu-102-R00549017-1.pdf: 6702664 bytes, checksum: ae8234379c11c7166f1fbbba04a2d1c9 (MD5) Previous issue date: 2013 | en |
| dc.description.tableofcontents | CHAPTER 1
General Introduction 1.1 HIGH PERFORMANCE POLYMERS ............................................................... 2 1.1.1 Preparation of Aromatic Polyamides ........................................................ 4 Direct polycondensation................................................................................ 5 Low-temperature solution methods .............................................................. 7 1.1.2 Preparation of Aromatic Polyimides ......................................................... 7 1.1.3 Modification of Aromatic Polyamides and Polyimides .......................... 10 1.2 EVOLUTION OF ELECTROCHROMISM ..................................................... 14 1.3 ELECTROCHROMIC SYSTEMS .................................................................... 18 1.3.1 Transition-metal Oxides ........................................................................... 18 Tungsten Trioxide (WO3) ............................................................................ 18 Iridium Oxide (IrO2) ................................................................................... 19 1.3.2 Coordination Complexes .......................................................................... 20 Prussian blue (PB) ...................................................................................... 20 Phthalocyanines .......................................................................................... 21 1.3.3 Conducting Polymers ................................................................................ 22 1.3.4 Arylamine-based Polymers ...................................................................... 25 1.4 VIOLOGENS ....................................................................................................... 29 1.4.1 Reduction Behavior .................................................................................. 29 1.4.2 Electrochemical Behavior of Viologen in Organic System .................... 31 1.4.3 Development of Viologen in Electrochromic device ............................... 32 1.4.4. Combination between Polymer and Viologens ...................................... 33 1.5 RESEARCH MOTIVATION .............................................................................. 37 REFERENCES AND NOTES ................................................................................... 39 CHAPTER 2 Synthesis, Electrochemical and Electrochromic Properties of Ambipolar Triphenylamine-containing Aramids with Pendant Viologen Moieties ABSTRACT OF CHAPTER 2 .................................................................................. 53 2.1 INTRODUCTION ................................................................................................ 54 2.2 EXPERIMENTAL SECTION ............................................................................ 56 2.2.1 Materials .................................................................................................... 56 2.2.2 Monomer Synthesis ................................................................................... 56 1-ethyl-4-(4-pyridinyl)pyridinium bromide (1)........................................... 56 4,4'-dinitro-4'-(2-bromoethoxy)triphenylamine (3) .................................. 57 1-(2-(4-(bis(4-nitrophenyl)amino)phenoxy)ethyl)-1'-ethyl-[4,4'-bipyridine] hexafluorophosphate (4) ............................................................................. 57 1-(2-(4-(bis(4-aminophenyl)amino)phenoxy)ethyl)-1'-ethyl-[4,4'-bipyridin e] hexafluorophosphate (5) ......................................................................... 58 2.2.3 Polymer Synthesis ..................................................................................... 59 2.2.4 Preparation of the Polyamide Films ........................................................ 60 2.2.5 Measurements............................................................................................ 60 2.3 RESULTS AND DISCUSSION ........................................................................... 62 2.3.1 Monomer Synthesis ................................................................................... 62 2.3.2 Polymer Synthesis ..................................................................................... 71 2.3.3 Polymer Properties ................................................................................... 75 Basic Characterization ................................................................................ 75 Electrochemical Properties ......................................................................... 78 Spectroelectrochemistry and Electrochromic Properties ........................... 83 Measurement of n-Electrons Polyamide, TPA-cPA ................................... 88 2.4 SUMMARY .......................................................................................................... 90 REFERENCES AND NOTES ................................................................................... 91 CHAPTER 3 Novel Triphenylamine-based Electrochromic Aromatic Polyimides With Pendant Viologen Moieties ABSTRACT OF CHAPTER 3 .................................................................................. 94 3.1 INTRODUCTION ................................................................................................ 95 3.2 EXPERIMENTAL SECTION ............................................................................ 97 3.2.1 Materials .................................................................................................... 97 3.2.2 Polymer Synthesis ..................................................................................... 97 3.2.3 Preparation of the Polyimide Films ......................................................... 98 3.2.4 Measurements ........................................................................................... 99 3.3 RESULTS AND DISCUSSION ......................................................................... 101 3.3.1 Polymer Synthesis ................................................................................... 101 3.3.2 Polymer Properties ................................................................................. 105 Basic Characterization .............................................................................. 105 Electrochemical Properties ....................................................................... 108 Spectroelectrochemistry and Electrochromic Properties ........................ 113 3.4 SUMMARY ........................................................................................................ 117 REFERENCES AND NOTES ................................................................................. 118 | |
| dc.language.iso | en | |
| dc.subject | 聚醯胺 | zh_TW |
| dc.subject | 聚醯亞胺 | zh_TW |
| dc.subject | 紫精 | zh_TW |
| dc.subject | 三苯胺 | zh_TW |
| dc.subject | 電致變色 | zh_TW |
| dc.subject | triphenylamine | en |
| dc.subject | viologen | en |
| dc.subject | polyamide | en |
| dc.subject | polyimide | en |
| dc.subject | electrochromism | en |
| dc.title | 新型含紫精側鏈之三苯胺芳香族高分子合成與電化學及電致變色特性之研究 | zh_TW |
| dc.title | Synthesis, Electrochemical and Electrochromic Properties of Triphenylamine-containing Novel Aromatic Polymers with Pendant Viologen Moieties | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 101-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 蕭勝輝(Sheng-Huei Hsiao),陳燿騰(Yaw-Terng Chern),陳志堅(Jyh-Chien Chen) | |
| dc.subject.keyword | 三苯胺,紫精,聚醯胺,聚醯亞胺,電致變色, | zh_TW |
| dc.subject.keyword | triphenylamine,viologen,polyamide,polyimide,electrochromism, | en |
| dc.relation.page | 122 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2013-08-13 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 高分子科學與工程學研究所 | zh_TW |
| 顯示於系所單位： | 高分子科學與工程學研究所 | |
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