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http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/49256完整後設資料紀錄
| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 楊宗傑 | |
| dc.contributor.author | Chang-Yen Liu | en |
| dc.contributor.author | 劉昌彥 | zh_TW |
| dc.date.accessioned | 2021-06-15T11:21:04Z | - |
| dc.date.available | 2021-09-01 | |
| dc.date.copyright | 2016-09-01 | |
| dc.date.issued | 2016 | |
| dc.date.submitted | 2016-08-19 | |
| dc.identifier.citation | 1. McCabe, J.F., Soft lining materials: composition and structure. J Oral Rehabil, 1976. 3:273-8.
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Mese, A., Guzel, K.G.,Uysal, E., Effect of storage duration on tensile bond strength of acrylic or silicone-based soft denture liners to a processed denture base polymer. Acta Odontol Scand, 2005. 63:31-5. 34. McCabe, J.F., Carrick, T.E.,Kamohara, H., Adhesive bond strength and compliance for denture soft lining materials. Biomaterials, 2002. 23:1347-52. 35. Kutay, O., Comparison of tensile and peel bond strengths of resilient liners. J Prosthet Dent, 1994. 71:525-31. 36. Jepson, N.J., McCabe, J.F.,Storer, R., Age changes in the viscoelasticity of permanent soft lining materials. J Dent, 1993. 21:171-8. 37. Waters, M., Jagger, R., Williams, K.,Jerolimov, V., Dynamic mechanical thermal analysis of denture soft lining materials. Biomaterials, 1996. 17:1627-30. 38. Nikawa, H., Iwanaga, H., Hamada, T.,Yuhta, S., Effects of denture cleansers on direct soft denture lining materials. J Prosthet Dent, 1994. 72:657-62. 39. Mutluay, M.M.,Ruyter, I.E., Evaluation of bond strength of soft relining materials to denture base polymers. Dent Mater, 2007. 23:1373-81. 40. Meşe, A., Bond Strength of Soft Denture Liners Following Immersion of Denture Cleanser. Biotechnology & Biotechnological Equipment, 2014. 20:184-191. 41. Takahashi, J.M., Consani, R.L., Henriques, G.E., Nobilo, M.A.,Mesquita, M.F., Effect of accelerated aging on permanent deformation and tensile bond strength of autopolymerizing soft denture liners. J Prosthodont, 2011. 20:200-4. 42. Hong, G., Murata, H.,Hamada, T., Relationship between plasticizer content and tensile bond strength of soft denture liners to a denture base resin. Dent Mater J, 2004. 23:94-9. 43. Wright, P.S., Characterization of the Adhesion of Soft Lining Materials to Poly (Methyl-Methacrylate). J Dent Res, 1982. 61:1002-1005. 44. Wright, P.S., The success and failure of denture soft-lining materials in clinical use. J Dent, 1984. 12:319-27. 45. Braden, M.,Wright, P.S., Water absorption and water solubility of soft lining materials for acrylic dentures. J Dent Res, 1983. 62:764-8. 46. Kazanji, M.N.,Watkinson, A.C., Soft lining materials: their absorption of, and solubility in, artificial saliva. Br Dent J, 1988. 165:91-4. 47. Polyzois, G.L., Adhesion properties of resilient lining materials bonded to light-cured denture resins. J Prosthet Dent, 1992. 68:854-8. 48. Wright, P.S., Composition and properties of soft lining materials for acrylic dentures. J Dent, 1981. 9:210-23. 49. 黃千豈, 使用檸檬酸三丁酯、乙醯檸檬酸三丁酯及超分支聚酯提升組織調理材黏彈性質穩定性. 2015, 國立台灣大學: 台北市. 50. Mese, A.,Guzel, K.G., Effect of storage duration on the hardness and tensile bond strength of silicone- and acrylic resin-based resilient denture liners to a processed denture base acrylic resin. J Prosthet Dent, 2008. 99:153-9. 51. Kim, B.J., Yang, H.S., Chun, M.G.,Park, Y.J., Shore hardness and tensile bond strength of long-term soft denture lining materials. J Prosthet Dent, 2014. 112:1289-97. 52. Emmer, T.J., Jr., Emmer, T.J., Sr., Vaidynathan, J.,Vaidynathan, T.K., Bond strength of permanent soft denture liners bonded to the denture base. J Prosthet Dent, 1995. 74:595-601. 53. Dootz, E.R., Koran, A.,Craig, R.G., Physical property comparison of 11 soft denture lining materials as a function of accelerated aging. J Prosthet Dent, 1993. 69:114-9. 54. Craig, R.G.,Gibbons, P., Properties of resilient denture liners. J Am Dent Assoc, 1961. 63:382-90. 55. Sinobad, D., Murphy, W.M., Huggett, R.,Brooks, S., Bond strength and rupture properties of some soft denture liners. J Oral Rehabil, 1992. 19:151-60 | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/49256 | - |
| dc.description.abstract | 組織調理材(tissue conditioner)常用於活動義齒暫時墊底,可舒緩因其組 織接觸面(tissue surface)與口腔黏膜間的不密合所引起的不適感,目前臨床使 用上最大問題是組織調理材所含之酯類增塑劑及乙醇會釋出導致這類材料黏彈性 質(viscoelasticity)隨著口內使用時間拉長而快速喪失。
為延長組織調理材黏彈性質的維持時間及減少生物毒性成份的使用,先前本 研究團隊以無毒環保增塑劑—乙醯檸檬酸三丁酯(acetyl tributyl citrate, ATBC),另加入分子量較大之超分支聚酯(hyperbranched polyester, TAH)以減 少增塑劑的釋出,進而減少組織調理材料黏彈性質的喪失。結果顯示使用液劑為 78.3wt% ATBC、8.7wt% TAH 和 13wt%乙醇之新式組織調理材(NTU-TC),其複數剪 切模數(G*)的28天模擬口腔環境中,百分比變化量為所有組別中最小,故認為此 新式組織調理材(NTU-TC)有較長時間的黏彈性質穩定表現。 為使之臨床應用的可能,此類材料與活動義齒間使用後黏著失效的現象必須 要被進行探討。因此,組織調理材與活動義齒的黏著強度(bonding strength)是本 研究探討的重點:針對新式組織調理材(NTU-TC)及兩組市售組織調理材(Soft liner,GC; Lynal,Dentsply),與常用於活動義齒基底之材料:PMMA樹脂(Lucitone 199,Dentsply)進行樣品裝配,在分組給予不同天數(Day 0, 1, 3, 7, 14, 28)的 37°C水中浸泡後進行抗張黏著強度(Tensile bonding strength)測試,並觀察黏 著失效模式(Failure mode)。結果顯示,所有組別的抗張黏著強度均隨著浸泡時間 的增長而有增加的趨勢。除Day 0外,NTU-TC在Day 1到Day 28都保持穩定的黏著 強度;在黏著失效模式上,所有組別之樣品均呈現膠合面失效(adhesive failure)。 故本研究認為新式組織調理材(NTU-TC)在與活動義齒基底有合理之黏著性質。 | zh_TW |
| dc.description.abstract | Tissue conditioners are often used in edentulous patients to treat lesions of the alveolar mucosa caused by ill-fitted dentures. The main problem in clinical use is the rapid loss of viscoelasticity due to the leaching of ester plasticizer and ethanol.
For extending the life span of tissue conditioner and decrease the using of bio-toxic components, our research team had used acetyl tributyl citrate (ATBC), which are non- toxic and adding hyperbranched polyester (TAH) with large molecular weight to reduce the plasticizer leaching to oral cavity and the loss of viscoelastic property. The results showed that the viscoelasticity stability of new tissue conditioners using using ATBC 78.3%, TAH 8.7% and ethanol 13% as plasticizer was better than another conventional brands. The changes in the percentage of complex modulus (G*) with time for new tissue conditioner was the smallest of all the groups. Therefore, in this study, this new tissue conditioner is the most suitable combination for tissue conditioners. In order to explore the possibility of clinical using, the bonding failure from denture must be discussed. Our research point is the bonding strength between tissue conditioner and denture resin. We would assess the tensile bonding strength between tissue conditioners(NTU-TC, Lynal, Soft liner) in the simulations of oral cavity, immerse in 37°C distilled water, for several days(Day 0, 1, 3, 7, 14, 28). The bonding failure mode would be observed. The results showed the tensile bonding strength of all groups increase with immersion time. Except Day 0, NTU-TC had stable bonding value from Day 1 to Day 28. All samples of three tissue conditioners had adhesive failure mode. We think the new tissue conditioner(NTU-TC) had suitable bonding property with denture resin. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-15T11:21:04Z (GMT). No. of bitstreams: 1 ntu-105-R02422016-1.pdf: 4272484 bytes, checksum: e2cfd6568b1e26f706d391935314afee (MD5) Previous issue date: 2016 | en |
| dc.description.tableofcontents | 摘要 7
Abstract 8 第一章 前言 9 第二章 文獻回顧 10 2.1 組織調理材 10 2.1.1 功能 10 2.1.2 組成 11 2.1.3材料性質 11 2.1.4 增塑劑 12 2.1.5 塑化作用 12 2.1.6 衰退效應(Aging Effect) 13 2.2 組織調理材配方的改良 13 2.2.1 乙醇的添加 14 2.2.2 PMMA的作用 14 2.2.3 增塑劑的改變 15 2.3 黏著強度測試Bonding strength testing 17 2.3.1 ASTM D429 18 2.3.2 黏著失效(Bonding failure) 19 2.4 文獻回顧結論 20 第三章 實驗動機與目的 21 3.1 研究動機 21 3.2 研究目的 21 第四章 實驗材料與方法 22 摘要 7 Abstract 8 第一章 前言 9 第二章 文獻回顧 10 2.1 組織調理材 10 2.1.1 功能 10 2.1.2 組成 11 2.1.3材料性質 11 2.1.4 增塑劑 12 2.1.5 塑化作用 12 2.1.6 衰退效應(Aging Effect) 13 2.2 組織調理材配方的改良 13 2.2.1 乙醇的添加 14 2.2.2 PMMA的作用 14 2.2.3 增塑劑的改變 15 2.3 黏著強度測試Bonding strength testing 17 2.3.1 ASTM D429 18 2.3.2 黏著失效(Bonding failure) 19 2.4 文獻回顧結論 20 第三章 實驗動機與目的 21 3.1 研究動機 21 3.2 研究目的 21 第四章 實驗材料與方法 22 4.1實驗藥品 22 4.2實驗儀器 24 4.3實驗流程 25 4.4實驗樣品備製 26 4.4.1 合成超分支聚酯 TAH 26 4.4.2 活動義齒基底材料樹脂塊備製 27 4.4.3 新式組織調理材NTU-TC備製 29 4.5 樣品組裝 29 4.6模擬口腔環境 31 4.7抗張黏著強度測試 32 4.8黏著失效模式分析 33 4.9 統計分析 33 第五章 實驗結果 34 5.1 抗張黏著測試 34 5.2 黏著失效分析 41 5.2.1 肉眼觀察 41 5.2.2 不同倍率放大之觀察 43 5.2.3 同倍率不同區域之放大分析(31.25X) 47 5.3 統計分析 52 受試者間效應項的檢定 52 多重比較 53 第六章 討論 54 6.1.樹脂塊之製作與組織調理材之裝配 54 6.2 抗張黏著強度與增塑劑 55 6.3 抗張黏著強度與模擬口腔環境 57 摘要 7 Abstract 8 第一章 前言 9 第二章 文獻回顧 10 2.1 組織調理材 10 2.1.1 功能 10 2.1.2 組成 11 2.1.3材料性質 11 2.1.4 增塑劑 12 2.1.5 塑化作用 12 2.1.6 衰退效應(Aging Effect) 13 2.2 組織調理材配方的改良 13 2.2.1 乙醇的添加 14 2.2.2 PMMA的作用 14 2.2.3 增塑劑的改變 15 2.3 黏著強度測試Bonding strength testing 17 2.3.1 ASTM D429 18 2.3.2 黏著失效(Bonding failure) 19 2.4 文獻回顧結論 20 第三章 實驗動機與目的 21 3.1 研究動機 21 3.2 研究目的 21 第四章 實驗材料與方法 22 4.1實驗藥品 22 4.2實驗儀器 24 4.3實驗流程 25 4.4實驗樣品備製 26 4.4.1 合成超分支聚酯 TAH 26 4.4.2 活動義齒基底材料樹脂塊備製 27 4.4.3 新式組織調理材NTU-TC備製 29 4.5 樣品組裝 29 4.6模擬口腔環境 31 4.7抗張黏著強度測試 32 4.8黏著失效模式分析 33 4.9 統計分析 33 第五章 實驗結果 34 5.1 抗張黏著測試 34 5.2 黏著失效分析 41 5.2.1 肉眼觀察 41 5.2.2 不同倍率放大之觀察 43 5.2.3 同倍率不同區域之放大分析(31.25X) 47 5.3 統計分析 52 受試者間效應項的檢定 52 多重比較 53 第六章 討論 54 6.1.樹脂塊之製作與組織調理材之裝配 54 6.2 抗張黏著強度與增塑劑 55 6.3 抗張黏著強度與模擬口腔環境 57 6.4 黏著強度與黏彈性質 58 6.5 黏著失效之分析 61 6.6 臨床應用 64 第七章 結論 65 Reference 66 Fig 4 1 Experimental procedure 24 Fig 4 2 The chemical structure of TAH 25 Fig 4 3不鏽鋼模具 側視圖 26 Fig 4 4不鏽鋼模具實體 27 Fig 4 5取出之樹脂塊(含不鏽鋼螺絲) 27 Fig 4 6樣品組裝 側視圖 29 Fig 4 7樣品組裝實圖 29 Fig 4 8樣品組裝存放於獨立塑膠容器 30 Fig 4 9樣品上夾具及萬用測試儀 31 Fig 5 1 Day 0 Tensile bonding strength 33 Fig 5 2 Day 1 Tensile bonding strength 34 Fig 5 3 Day 3 Tensile bonding strength 35 Fig 5 4 Day 7 Tensile bonding strength 36 Fig 5 5 Day 14 Tensile bonding strength 37 Fig 5 6 Day 28 Tensile bonding strength 38 Fig 5 7 Day 0~ Day 28 Tensile bonding strength trend 39 Fig 5 8 黏著失效瞬間(NTU-TC，Day 28) 40 Fig 5 9 完整拉開之樹脂塊(NTU-TC，Day 28) 41 Fig 5 10 原始未經黏著樹脂塊表面(不同放大倍率) 42 Fig 5 11 Soft liner，Day 28組別，樹脂塊表面(不同放大倍率) 43 Fig 5 12 Lynal，Day 28組別樹脂塊表面(不同放大倍率) 44 Fig 5 13 NTU-TC，Day 28組別樹脂塊表面(不同放大倍率) 45 Fig 5 14 原始未經黏著樹脂塊表面(同放大倍率不同區域) 46 Fig 5 15 Soft liner，Day 28組別樹脂塊表面(同放大倍率不同區域) 47 Fig 5 16 Lynal，Day28組別樹脂塊表面(同放大倍率不同區域) 48 Fig 5 17 NTU-TC，Day 28組別樹脂塊表面(同放大倍率不同區域) 49 Fig 5 18 不同組別樹脂塊表面(同放大倍率中央區) 50 Fig 6 1 28天G’ G” G* 趨勢圖 58 Fig 6 2 0~28天G*變化百分比 59 Fig 6-3 Day 0 Area under curve 60 Fig 6-4 Day 28 Area under curve 61 Table 2 1 Properties of TBC, ATBC 15 Table 5 1 Two-way ANOVA分析 51 Table 5 2 One-way ANOVA分析 52 | |
| dc.language.iso | zh-TW | |
| dc.subject | 組織調理材 | zh_TW |
| dc.subject | 超分支聚酯 | zh_TW |
| dc.subject | 抗張黏著強度 | zh_TW |
| dc.subject | Tissue conditioner | en |
| dc.subject | Hyperbranched polyester | en |
| dc.subject | Tensile bonding strength | en |
| dc.title | 評估使用乙醯檸檬酸三丁酯及超分支聚酯之新式組織調理材的黏著強度 | zh_TW |
| dc.title | Evaluation of bonding strength of new tissue conditioner using acetyl tribute citrate and novel hyper branched polyester | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 104-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.coadvisor | 林立德,李伯訓 | |
| dc.contributor.oralexamcommittee | 鄭國忠 | |
| dc.subject.keyword | 組織調理材,抗張黏著強度,超分支聚酯, | zh_TW |
| dc.subject.keyword | Tissue conditioner,Tensile bonding strength,Hyperbranched polyester, | en |
| dc.relation.page | 69 | |
| dc.identifier.doi | 10.6342/NTU201603380 | |
| dc.rights.note | 有償授權 | |
| dc.date.accepted | 2016-08-19 | |
| dc.contributor.author-college | 醫學院 | zh_TW |
| dc.contributor.author-dept | 臨床牙醫學研究所 | zh_TW |
| 顯示於系所單位： | 臨床牙醫學研究所 | |
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