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完整後設資料紀錄
DC 欄位 | 值 | 語言 |
---|---|---|
dc.contributor.advisor | 段維新(Wei-Hsing Tuan) | |
dc.contributor.author | Chuang-Ching Huang | en |
dc.contributor.author | 黃莊敬 | zh_TW |
dc.date.accessioned | 2021-06-13T02:10:53Z | - |
dc.date.available | 2012-07-03 | |
dc.date.copyright | 2007-07-03 | |
dc.date.issued | 2007 | |
dc.date.submitted | 2007-06-25 | |
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dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/30637 | - |
dc.description.abstract | 本實驗主要研究氧化鋁/鉬錳層接合之微結構與機械性質,純氧化鋁利用鉬錳法 (Moly – Manganese process) 製成三明治試片 (sandwich specimen),此一製程為利用網版印刷的方式將氧化鋁表面塗佈上鉬錳膏;其主要的成分包含有金屬鉬、金屬錳、玻璃粉末以及黏結劑。接著將試片在還原氣氛中燒結後,陶瓷層間會產生由金屬-玻璃混合物所組成之界面。
本實驗配製了兩種不同成分之鉬錳膏,在1100℃至1470℃溫度區間接合,所使用之氣氛為95%N2-5%H2,以四點彎曲來量測界面強度,進而探討在不同接合溫度下,鉬錳層之微結構與界面的生成相對強度之影響。本實驗利用SEM/EDS、XRD以及EPMA來做微結構觀察與相分析。 實驗結果顯示,當使用無添加鈦之鉬錳膏接合時,在氧化鋁與鉬之間會發現一層MnAl2O4,此反應層的出現可幫助接著點強度之提升。然而,當使用含有微量鈦的鉬錳膏接合時 其界面強度主要與鉬錳層之微結構有關,強度的提升主要是來自於鉬顆粒的緻密化。 | zh_TW |
dc.description.provenance | Made available in DSpace on 2021-06-13T02:10:53Z (GMT). No. of bitstreams: 1 ntu-96-R94527032-1.pdf: 136798499 bytes, checksum: 15a787a8fb76e7d4b379796c1f56008f (MD5) Previous issue date: 2007 | en |
dc.description.tableofcontents | Chapter 1: Introduction..............................................1
Chapter 2: Literature survey..............................3 2.1 Joining of ceramics...................................3 2.1.1 Mechanical joining..................................5 2.1.2 Adhesive bonding....................................5 2.1.3 Diffusion bonding...................................6 2.1.4 Brazing.............................................8 2.2 Fracture of metal/ceramic interfaces.................20 2.2.1 Four-point bending test............................25 2.2.2 Double cantilever beam test........................28 2.2.3 Double cleavage drilled compressive test...........29 2.2.4 Laser spallation technique.........................31 2.2.5 Bulge and blister test.............................33 Chapter 3: Experiments...................................35 3.1 Materials and test specimen..........................35 3.1.1 Alumina............................................35 3.1.2 Mo-Mn paste........................................35 3.2 Density measurement..................................36 3.3 Thermogravimetric analysis...........................37 3.4 Wetting test.........................................37 3.5 Joining process......................................37 3.6 Four-point bending test..............................40 3.7 XRD..................................................41 3.8 SEM..................................................41 3.9 Experimental flow chart..............................41 Chapter 4: Results.......................................43 4.1 Density..............................................43 4.2 Thermogravimetric analysis of Mo-Mn pastes...........44 4.3 Wetting behavior of glass............................46 4.4 Phase analysis.......................................48 4.5 Microstructure observation...........................52 4.5.1 Alumina substrate..................................52 4.5.2 Cross-section observation..........................53 4.5.3 Fracture surface characterization..................60 4.6 Adhesion strength....................................61 Chapter 5: Discussion....................................63 5.1 Microstructure.......................................63 5.1.1 The specimens of A group...........................63 5.1.2 The specimens of B group...........................64 5.2 Load-displacement curves.............................69 5.2.1 Mechanics approach.................................69 5.2.2 Energy approach....................................74 5.3 Adhesion strength....................................76 Chapter 6: Conclusions...................................86 References...............................................88 | |
dc.language.iso | en | |
dc.title | 氧化鋁與鉬錳之界面強度 | zh_TW |
dc.title | Adhesion Strength of Al2O3/Mo-Mn Interfaces | en |
dc.type | Thesis | |
dc.date.schoolyear | 95-2 | |
dc.description.degree | 碩士 | |
dc.contributor.oralexamcommittee | 楊聰仁,陳榮志 | |
dc.subject.keyword | 氧化鋁,界面,硬焊,接合,金屬化,四點彎曲測試, | zh_TW |
dc.subject.keyword | Al2O3,Interface,Brazing,Joining,Metallization,Four-point bending test, | en |
dc.relation.page | 97 | |
dc.rights.note | 有償授權 | |
dc.date.accepted | 2007-06-26 | |
dc.contributor.author-college | 工學院 | zh_TW |
dc.contributor.author-dept | 材料科學與工程學研究所 | zh_TW |
顯示於系所單位: | 材料科學與工程學系 |
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