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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 陳延平 | |
| dc.contributor.author | Hsin-Yan Lu | en |
| dc.contributor.author | 呂信諺 | zh_TW |
| dc.date.accessioned | 2021-06-08T05:18:32Z | - |
| dc.date.copyright | 2005-08-01 | |
| dc.date.issued | 2005 | |
| dc.date.submitted | 2005-07-30 | |
| dc.identifier.citation | 參考文獻
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Langmuir, 20, 2004, 5109-5113 Zhu, J., Liu, S., Plachiik, O., Koltypin Y., Gedanken, A., Shape-Controlled Synthesis of Silver Nanoparticles by Pulse Sonoelectrochemical Methods. Langmui. 2000, 16, 6396-6399 蘇至善，以批式超臨界反溶劑沉積法進行非類固醇抗發炎藥之再結晶研究，國立台灣大學化學工程學研究所碩士論文，2003 梁明在，水熱條件下形成奈米粉體之機制， 2003年超臨界流體技術應用與發展研討會暨設備展. 1.3.1-1.3.12，台北，台灣，2003 | |
| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/24208 | - |
| dc.description.abstract | 不同於超臨界水水熱結晶製備奈米金屬氧化物，本研究以超臨界水還原方法製備奈米金屬及金屬氧化物。本研究使用四種前驅物，分別為硫酸鐵，硫酸銅，硫酸銀及四氯化鉑，並以甲酸作為還原劑，合成奈米四氧化三鐵、奈米銅、奈米銀及奈米白金。本研究主要探討欲得到不同奈米金屬及奈米金屬氧化物所需還原劑之濃度，及所得產物之粒徑大小及其分佈。由各產物之TEM圖所測得之粒徑大小，奈米銅平均粒徑約為18奈米，奈米銀約為28奈米，奈米白金約為10奈米。除成功製備奈米金屬，本研究亦提出超臨界水還原反應方程式。 | zh_TW |
| dc.description.abstract | In this study, supercritical water reduction (SCWR) method was applied to prepare metal oxide and metal nanoparticles. Different from the supercritical water hydrothermal crystallization, reduction methods was used to obtain the nanoparticles. Four kinds of metal precursors, ferric sulfate, copper sulfate, and silver sulfate, were employed in this study to prepare Fe3O4, Cu, Ag, and Pt nanoparticles. The effect of reducing agent concentration was examined. TEM micrographs showed that average particle size of copper, silver, platinum are about 18nm, 28nm and 10nm, respectively. The reaction mechanism for supercritical water reduction was also proposed in this study. | en |
| dc.description.provenance | Made available in DSpace on 2021-06-08T05:18:32Z (GMT). No. of bitstreams: 1 ntu-94-R92524077-1.pdf: 2871012 bytes, checksum: a74a4fac458065aae8a202db46d9d159 (MD5) Previous issue date: 2005 | en |
| dc.description.tableofcontents | 目錄
摘要 Abstract Ⅰ Ⅱ 目錄 Ⅲ 表目錄 圖目錄 Ⅴ Ⅵ 第一章 序論 1 1-1 奈米級金屬氧化物之用途 1 1-2 奈米級金屬氧化物之傳統製程 2 1-3 超臨界流體技術及超臨界水之應用 3 1-3-1 超臨界流體技術 3 1-3-2 超臨界二氧化碳製備奈米粉體 5 1-3-3 超臨界水之應用 6 1-4 利用超臨界水製備奈米金屬氧化物之文獻回顧 7 1-5 本研究之研究動機 11 1-6 本論文之架構 14 第二章 實驗方法、步驟與分析 16 2-1 前言 16 2-2 實驗藥品 16 2-3 實驗儀器 17 2-4 實驗裝置 18 2-4-1 儀器組裝 18 2-4-2 儀器測試 20 2-5 實驗步驟 21 2-6 實驗分析 22 2-6-1 X光繞射分析 22 2-6-2 穿透式電子顯微鏡分析 23 2-6-3 粒徑分佈分析 24 2-6-4 pH量測判斷甲酸分解率 24 第三章 結果與討論 25 3-1 以硫酸鐵前驅物製備奈米四氧化三鐵. 25 3-2 以硫酸銅前驅物製備奈米銅 30 3-3 以硫酸銀前驅物製備奈米銀 35 3-4 以氯化鉑前驅物製備奈米白金 38 3-5 與文獻所生產之奈米金屬比較 40 第四章 結論 42 參考文獻 83 表目錄 Table. 1-1 Summary of metal oxide particles produced by supercritical water 43 Table. 1-2 Summary of metal nanopaticles produced by microemulsion, electrochemical and synthesis with silica or silica film method 44 Table. 3-1-1 Decomposition fraction of formic acid 45 Table. 3-1-2 Relation between Intensity ratio and weight percentage of Fe3O4 45 Table. 3-1-3 Relation between concentration of formic acid and the average particle size measurement from TEM 46 圖目錄 Fig. 1-1 Properties of water from standard state( 25℃, 1bar) to supercritical state 47 Fig. 1-2 Solubility behavior of PbO and CuO in sub- and supercritical water 47 Fig. 1-3 A schematic mechanism of CeO2 formation in sub- and supercritical water 48 Fig. 2-1 Experimental apparatus of continuous SCWR reaction 49 Fig. 3-1-1 JCPDS of (A)α-Fe2O3 and (B) Fe3O4 50 Fig. 3-1-2 XRD spectrum of α-Fe2O3 and Fe3O4 mixtures under: (A) [HCOOH]=0.0015M (B) [HCOOH]=0.015M 51 Fig. 3-1-3 XRD spectrum of α-Fe2O3 and Fe3O4 mixtures under: (C) [HCOOH] =0.15M (D) [HCOOH] =1.5M 52 Fig. 3-1-4 XRD spectrum of α-Fe2O3 and Fe3O4 mixtures under: (E) [HCOOH] =1.8M (F) [HCOOH] =2.4M 53 Fig. 3-1-5 XRD spectrum of α-Fe2O3 and Fe3O4 mixtures under: (G) [HCOOH] =3M (H) [HCOOH] =3.6M 54 Fig. 3-1-6 XRD spectrum of α-Fe2O3 and Fe3O4 mixtures under: (I) [HCOOH] =7.5M 55 Fig. 3-1-7 The relationship between intensity ratio and wt % of Fe3O4 56 Fig. 3-1-8 FTIR spectrum of the exhausting gases CO2 56 Fig. 3-1-9 TEM images of α-Fe2O3 and Fe3O4 mixtures under: (A) [HCOOH]=0.0015M (B) [HCOOH]=0.015M 57 Fig. 3-1-10 TEM images of α-Fe2O3 and Fe3O4 mixtures under: (C) [HCOOH]=0.15M (D) [HCOOH]=1.5M 58 Fig. 3-1-11 TEM images of α-Fe2O3 and Fe3O4 mixtures under: (E) [HCOOH]=1.8M (F) [HCOOH]=2.4M 59 Fig. 3-1-12 TEM images of α-Fe2O3 and Fe3O4 mixtures under: (G) [HCOOH]=3M (H) [HCOOH]=3.6M 60 Fig. 3-1-13 TEM images of α-Fe2O3 and Fe3O4 mixtures under: (I)[HCOOH]=7.5 M 61 Fig. 3-1-14 Particle size distribution diagram of α-Fe2O3and Fe3O4 mixtures under: (A) [HCOOH]=0.0015M (B) [HCOOH]=0.015M 62 Fig. 3-1-15 Particle size distribution diagram of α-Fe2O3and Fe3O4 mixtures under: [HCOOH]=0.15M (B) [HCOOH]=1.5M 63 Fig. 3-1-16 Particle size distribution diagram of α-Fe2O3and Fe3O4 mixtures under: (E) [HCOOH]=1.8M (F) [HCOOH]=2.4M 64 Fig. 3-1-17 Particle size distribution diagram of α-Fe2O3and Fe3O4 mixtures under: (G) [HCOOH]=3 M (H) [HCOOH]=3.6M 65 Fig. 3-1-18 Particle size distribution diagram of α-Fe2O3and Fe3O4 mixtures under: (I) [HCOOH]=7.5M 66 Fig. 3-2-1 JCPDS of (A) CuSO4•2Cu(OH)2 (B) CuSO4•3Cu(OH)2 67 Fig. 3-2-2 JCPDS of (C) Cu (D) Cu2O 68 Fig. 3-2-3 JCPDS of (E) CuO 69 Fig. 3-2-4 XRD spectrum of (A) Cu3(SO4)(OH)4 and Cu4(SO4)(OH)6xH2O (B) Cu, CuO and Cu2Omixtures under: (A) [HCOOH] =0M (B) [HCOOH]=0.003M 70 Fig. 3-2-5 XRD spectrum of Cu, CuO and Cu2O mixtures under: (C) [HCOOH] =0.15M (D) [HCOOH] =1.8M 71 Fig. 3-2-6 XRD spectrum of Cu under: (E) [HCOOH] =3.6M 72 Fig. 3-2-7 TEM images of Cu under 3.6M formic acid 73 Fig. 3-2-8 Particle size distribution diagram of Cu under 3.6M formic acid 74 Fig. 3-3-1 JCPDS of (A) Ag2SO4 (B) Ag 75 Fig. 3-3-2 XRD spectrum of (A) Ag2SO4 and (B) Ag under: (A) [HCOOH] =0M (B) [HCOOH] =0.015M 76 Fig. 3-3-3 TEM images of Ag under 0.015M formic acid 77 Fig. 3-3-4 Particle size distribution diagram of Ag under 0.015M formic acid 78 Fig. 3-4-1 JCPDS of (A) α-Fe2O3 (B) Pt 79 Fig. 3-4-2 XRD spectrum of (A) α-Fe2O3 (B) Pt under: (A)[HCOOH] =0M (B) [HCOOH] =0.015M 80 Fig. 3-4-3 TEM images of Pt under 0.015M formic acid 81 Fig. 3-4-4 Particle size distribution diagram of Pt under 0.015M formic acid 82 | |
| dc.language.iso | zh-TW | |
| dc.subject | 奈米銀 | zh_TW |
| dc.subject | 奈米銅 | zh_TW |
| dc.subject | 超臨界水 | zh_TW |
| dc.subject | 水熱結晶 | zh_TW |
| dc.subject | 米四氧化三鐵 | zh_TW |
| dc.subject | 奈米白金 | zh_TW |
| dc.subject | nanoparticles | en |
| dc.subject | supercritical water reduction | en |
| dc.subject | hydrothermal crystallization | en |
| dc.subject | Fe3O4 | en |
| dc.subject | Cu | en |
| dc.subject | Ag | en |
| dc.subject | Pt | en |
| dc.title | 利用超臨界水還原方法製備奈米金屬及奈米金屬氧化物粉體之研究 | zh_TW |
| dc.title | Synthesis of Metal and Metal Oxide Nanoparticles by Supercritical Water Reduction Method | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 93-2 | |
| dc.description.degree | 碩士 | |
| dc.contributor.oralexamcommittee | 陳立仁,萬本儒 | |
| dc.subject.keyword | 超臨界水,水熱結晶,米四氧化三鐵,奈米銅,奈米銀,奈米白金, | zh_TW |
| dc.subject.keyword | supercritical water reduction,hydrothermal crystallization,Fe3O4,Cu,Ag,Pt,nanoparticles, | en |
| dc.relation.page | 91 | |
| dc.rights.note | 未授權 | |
| dc.date.accepted | 2005-07-31 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 化學工程學研究所 | zh_TW |
| 顯示於系所單位： | 化學工程學系 | |
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