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| DC 欄位 | 值 | 語言 |
|---|---|---|
| dc.contributor.advisor | 段維新(Wei-Hsing Tuan) | |
| dc.contributor.author | Yuan-Liang Chin | en |
| dc.contributor.author | 靳元良 | zh_TW |
| dc.date.accessioned | 2021-05-20T21:09:34Z | - |
| dc.date.available | 2013-04-01 | |
| dc.date.available | 2021-05-20T21:09:34Z | - |
| dc.date.copyright | 2011-06-01 | |
| dc.date.issued | 2011 | |
| dc.date.submitted | 2011-03-29 | |
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| dc.identifier.uri | http://tdr.lib.ntu.edu.tw/jspui/handle/123456789/10201 | - |
| dc.description.abstract | 為了改善陶瓷材料先天的脆性，在過往二、三十年陶瓷基複合材料研究當中，起初添加金屬強化相作為研究，但因金屬材料的熔點較低而限制了其應用面。在陶瓷韌化材方面，一般添加強度、硬度較高的顆粒、鬚晶及板晶等，但韌性的提升效果有限。本研究主要為提供一個新的陶瓷韌化概念，以強度相較於基地相較低，但含有弱介面之層狀陶瓷韌化材作為第二相，利用其層間弱介面的特性，使得脆性的陶瓷材料在破壞時破壞能量由此韌化材的層間弱介面吸收而產生韌化。
本研究使用三種材料系統，分別以氧化鋁與硼矽酸鹽玻璃基低溫共燒陶瓷（LTCC）作為基材，添加積層陶瓷電容（MLCC）以及碳化鈦矽（Ti3SiC2）層狀陶瓷作為韌化相進行無壓或熱壓燒結成試樣，進行強度與韌性的量測，確立強韌化機制，並輔以理論計算。此外，也以X光與奈米壓痕技術分析試樣內部的應力對於強度韌性之影響。有別於一般陶瓷基複合材料在基地相與第二相間的裂縫轉折或架橋，此一特殊的韌化機制的設計使得裂縫在含有弱介面的第二相內部產生轉折而吸收破壞能，可更進一步的改善陶瓷材料的韌性。 | zh_TW |
| dc.description.abstract | Since ceramic materials have various advantages to demonstrate their functions, they can be applied in many areas. However, ceramics are brittle and show catastrophic failure. The objective of many researches on structural ceramics is the development of materials with high reliability. Low-cost ceramic composite materials that exhibit excellent mechanical properties have attracted considerable interest for advanced engineering applications. For such materials, toughening remains one of the most important issues in enhancing the reliability.
In the present study, three different kinds of ceramic-matrix composites are used as model systems to demonstrate the feasibility of using toughening agents with weak interfaces as a new approach. The reinforcements, such as BaTiO3 platelet containing weak interfaces and Ti3SiC2 compound can be incorporated to toughen the composite. The material selection is based on the higher thermal expansion coefficient and the lower elastic modulus of the reinforcement than those of the matrix. The toughening mechanism and the energy dissipation during crack propagation are investigated via different skills, such as residual stress analysis and nano-indentation. The role of the shape of the reinforcement and the effect of pullout during toughening is also discussed with theoretical calculation. | en |
| dc.description.provenance | Made available in DSpace on 2021-05-20T21:09:34Z (GMT). No. of bitstreams: 1 ntu-100-D94527004-1.pdf: 3752225 bytes, checksum: 724dc5895e5018c34742300fa98ac44a (MD5) Previous issue date: 2011 | en |
| dc.description.tableofcontents | 摘要 I
Abstract II List of Tables VI List of Figures VII Chapter 1: Objective and Outline 1 Chapter 2: General Theory 4 2.1 Biomimetic concept 4 2.2 Toughening mechanisms of ceramic-matrix composites 7 2.3 Fracture toughness measurement 11 2.3.1 Single edge notched beam (SENB) method 13 2.3.2 Single edge V-notched beam (SEVNB) method 15 2.3.3 Indentation method 19 2.4 X-ray residual stress analysis [30] 19 2.4.1 Introduction of residual stress 19 2.4.2 Principles of X-ray stress measurement 21 Chapter 3: Feasibility Study of Using Multilayer Platelet as Toughening Agent 27 3.1 Introduction 27 3.2 Experimental Procedures 28 3.2.1 Raw material 29 3.2.2 Al2O3/BaTiO3-platelet composite 29 3.3 Results 32 3.4 Discussion 39 3.5 Conclusions 44 Chapter 4: Crack Extension Resistance Behaviour in Lamellae Inclusions Toughened Ceramic-Matrix Composite 46 4.1 Introduction 46 4.2 Experimental Procedures 47 4.2.1 Raw material 47 4.2.2 LTCC/BaTiO3-platelet composite 47 4.3 Results 48 4.4 Discussion 50 4.5 Conclusions 59 Chapter 5: Toughening Alumina with Layered Ti3SiC2 Inclusions 61 5.1 Introduction 61 5.2 Experimental Procedures 65 5.2.1 Samples preparation 65 5.2.2 Phase and structure analysis 65 5.2.3 Bulk mechanical properties 66 5.2.4 Nanoindentation tests 67 5.2.5 Crack-extension-resistance behaviour(R-curve) tests 69 5.3 Results 70 5.3.1 Phase analysis and physical properties 70 5.3.2 Mechanical properties 72 5.3.3 Residual stress analysis 78 5.3.4 Nanoindentation results 82 5.3.5 R-curve measurements 90 5.4 Discussion 93 5.4.1 Strengthening mechanism 93 5.4.2 Toughening mechanism 94 5.4.3 Contribution of plastic deformation of Ti3SiC2 to the crack deflection in the Al2O3/Ti3SiC2 composites 98 5.4.4 Contribution of crack-deflection-induced pullouts to the toughening effect in Al2O3/Ti3SiC2 composite 105 5.5 Conclusions 115 Chapter 6: Conclusions 119 Chapter 7: Future Work 122 References 124 Curriculum Vitae 136 | |
| dc.language.iso | en | |
| dc.title | 以含有弱介面之韌化相韌化脆性陶瓷之研究 | zh_TW |
| dc.title | Study on Toughening Brittle Ceramic by Using Reinforcements with Weak Interfaces | en |
| dc.type | Thesis | |
| dc.date.schoolyear | 99-2 | |
| dc.description.degree | 博士 | |
| dc.contributor.oralexamcommittee | 黃肇瑞(Jow-Lay Huang),謝宗霖(Tzong-Lin Shieh),郭錦龍(Chin-Lung Kuo),林博文(Bor-Wen Lin) | |
| dc.subject.keyword | 陶瓷基複合材料,弱介面,韌化機制,破壞能, | zh_TW |
| dc.subject.keyword | Weak interface,BaTiO3 platelet,Ti3SiC2,Residual stress,Nano-indentation,Pullout, | en |
| dc.relation.page | 137 | |
| dc.rights.note | 同意授權(全球公開) | |
| dc.date.accepted | 2011-03-30 | |
| dc.contributor.author-college | 工學院 | zh_TW |
| dc.contributor.author-dept | 材料科學與工程學研究所 | zh_TW |
| 顯示於系所單位： | 材料科學與工程學系 | |
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